EP0000918A3 - Process and apparatus for the preparation of linear, high molecular polyesters - Google Patents

Process and apparatus for the preparation of linear, high molecular polyesters Download PDF

Info

Publication number
EP0000918A3
EP0000918A3 EP78100670A EP78100670A EP0000918A3 EP 0000918 A3 EP0000918 A3 EP 0000918A3 EP 78100670 A EP78100670 A EP 78100670A EP 78100670 A EP78100670 A EP 78100670A EP 0000918 A3 EP0000918 A3 EP 0000918A3
Authority
EP
European Patent Office
Prior art keywords
linear
preparation
high molecular
molecular polyesters
polyesters
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP78100670A
Other versions
EP0000918B1 (en
EP0000918A2 (en
Inventor
Hans-Josef Dr. Sterzel
Kasimir Von Dziembowski
Hans Dr. Pirzer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25772598&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP0000918(A3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from DE19772738093 external-priority patent/DE2738093B1/en
Priority claimed from DE19782803530 external-priority patent/DE2803530A1/en
Application filed by BASF SE filed Critical BASF SE
Publication of EP0000918A2 publication Critical patent/EP0000918A2/en
Publication of EP0000918A3 publication Critical patent/EP0000918A3/en
Application granted granted Critical
Publication of EP0000918B1 publication Critical patent/EP0000918B1/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/785—Preparation processes characterised by the apparatus used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00121—Controlling the temperature by direct heating or cooling
    • B01J2219/0013—Controlling the temperature by direct heating or cooling by condensation of reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00168—Controlling or regulating processes controlling the viscosity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyesters Or Polycarbonates (AREA)
EP78100670A 1977-08-24 1978-08-16 Process for the preparation of linear, high molecular polyesters Expired EP0000918B1 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE2738093 1977-08-24
DE19772738093 DE2738093B1 (en) 1977-08-24 1977-08-24 Process and device for the production of linear high molecular weight polyesters
DE2803530 1978-01-27
DE19782803530 DE2803530A1 (en) 1978-01-27 1978-01-27 Linear high mol. wt. polyester prepn. - by precondensate after-condensn. under reduced pressure while progressively decreasing process temp. opt. continuously

Publications (3)

Publication Number Publication Date
EP0000918A2 EP0000918A2 (en) 1979-03-07
EP0000918A3 true EP0000918A3 (en) 1979-04-04
EP0000918B1 EP0000918B1 (en) 1982-03-17

Family

ID=25772598

Family Applications (1)

Application Number Title Priority Date Filing Date
EP78100670A Expired EP0000918B1 (en) 1977-08-24 1978-08-16 Process for the preparation of linear, high molecular polyesters

Country Status (5)

Country Link
US (2) US4214072A (en)
EP (1) EP0000918B1 (en)
JP (1) JPS5443997A (en)
DE (1) DE2861668D1 (en)
IT (1) IT1097584B (en)

Families Citing this family (48)

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Publication number Priority date Publication date Assignee Title
DE3820362A1 (en) * 1988-06-15 1990-03-15 Basf Ag METHOD FOR THE CONTINUOUS PRODUCTION OF LINEAR THERMOPLASTIC POLYESTERS
US5238740A (en) * 1990-05-11 1993-08-24 Hoechst Celanese Corporation Drawn polyester yarn having a high tenacity and high modulus and a low shrinkage
US5869011A (en) * 1994-02-01 1999-02-09 Lee; Jing Ming Fixed-bed catalytic reactor
US5520891A (en) * 1994-02-01 1996-05-28 Lee; Jing M. Cross-flow, fixed-bed catalytic reactor
JP3001181B2 (en) * 1994-07-11 2000-01-24 株式会社クボタ Reaction tube for ethylene production
DE19509551A1 (en) * 1995-03-16 1996-09-19 Basf Ag Process for the continuous production of thermoplastic polyesters
DE19615886C1 (en) * 1996-04-22 1997-07-31 Huels Chemische Werke Ag Increasing yield in crude di:methyl terephthalate prodn.
US6194609B1 (en) * 1997-06-30 2001-02-27 Bp Amoco Corporation Crystallization in a plate heat exchanger
DE19929791A1 (en) * 1999-06-29 2001-02-01 Basf Ag Process for the continuous production of polybutylene terephthalate from terephthalic acid and butanediol
FR2811789B1 (en) * 2000-07-13 2003-08-15 France Etat Ponts Chaussees METHOD AND DEVICE FOR CLASSIFYING VEHICLES INTO SILHOUETTE CATEGORIES AND FOR DETERMINING THEIR SPEED, FROM THEIR ELECTROMAGNETIC SIGNATURE
US6906164B2 (en) 2000-12-07 2005-06-14 Eastman Chemical Company Polyester process using a pipe reactor
AU2002243291A1 (en) 2000-12-07 2002-06-18 Eastman Chemical Company Low cost polyester process using a pipe reactor
US7135541B2 (en) 2003-06-06 2006-11-14 Eastman Chemical Company Polyester process using a pipe reactor
US7074879B2 (en) 2003-06-06 2006-07-11 Eastman Chemical Company Polyester process using a pipe reactor
DE102004001914A1 (en) 2004-01-14 2005-08-04 Sms Eumuco Gmbh Coupling device for a mechanical press, scissors or punching device
US7332548B2 (en) 2004-03-04 2008-02-19 Eastman Chemical Company Process for production of a polyester product from alkylene oxide and carboxylic acid
DE102004019810A1 (en) * 2004-04-23 2005-03-24 Zimmer Ag Production of thermoplastic polyester for use e.g. in fibres, film or bottles, involves precondensation by passing an esterification product downwards under reduced pressure through a column with structured packing
US20060251547A1 (en) * 2005-05-05 2006-11-09 Windes Larry C Family of stationary film generators and film support structures for vertical staged polymerization reactors
US7557243B2 (en) * 2005-05-19 2009-07-07 Eastman Chemical Company Enriched terephthalic acid composition
US20060264664A1 (en) * 2005-05-19 2006-11-23 Parker Kenny R Esterification of an exchange solvent enriched composition
US7919652B2 (en) * 2005-05-19 2011-04-05 Eastman Chemical Company Process to produce an enriched composition through the use of a catalyst removal zone and an enrichment zone
US7880031B2 (en) * 2005-05-19 2011-02-01 Eastman Chemical Company Process to produce an enrichment feed
US7432395B2 (en) 2005-05-19 2008-10-07 Eastman Chemical Company Enriched carboxylic acid composition
US7741516B2 (en) * 2005-05-19 2010-06-22 Eastman Chemical Company Process to enrich a carboxylic acid composition
US20060264662A1 (en) * 2005-05-19 2006-11-23 Gibson Philip E Esterification of an enriched composition
US20060264656A1 (en) * 2005-05-19 2006-11-23 Fujitsu Limited Enrichment process using compounds useful in a polyester process
US7897809B2 (en) * 2005-05-19 2011-03-01 Eastman Chemical Company Process to produce an enrichment feed
US7884231B2 (en) * 2005-05-19 2011-02-08 Eastman Chemical Company Process to produce an enriched composition
US7834208B2 (en) 2005-05-19 2010-11-16 Eastman Chemical Company Process to produce a post catalyst removal composition
US7304178B2 (en) * 2005-05-19 2007-12-04 Eastman Chemical Company Enriched isophthalic acid composition
US7888529B2 (en) * 2006-03-01 2011-02-15 Eastman Chemical Company Process to produce a post catalyst removal composition
US7649109B2 (en) 2006-12-07 2010-01-19 Eastman Chemical Company Polyester production system employing recirculation of hot alcohol to esterification zone
US7943094B2 (en) 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
US7863477B2 (en) 2007-03-08 2011-01-04 Eastman Chemical Company Polyester production system employing hot paste to esterification zone
US7829653B2 (en) 2007-07-12 2010-11-09 Eastman Chemical Company Horizontal trayed reactor
US7868129B2 (en) 2007-07-12 2011-01-11 Eastman Chemical Company Sloped tubular reactor with spaced sequential trays
US7872089B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Multi-level tubular reactor with internal tray
US7847053B2 (en) 2007-07-12 2010-12-07 Eastman Chemical Company Multi-level tubular reactor with oppositely extending segments
US7842777B2 (en) 2007-07-12 2010-11-30 Eastman Chemical Company Sloped tubular reactor with divided flow
US7872090B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Reactor system with optimized heating and phase separation
US7868130B2 (en) 2007-07-12 2011-01-11 Eastman Chemical Company Multi-level tubular reactor with vertically spaced segments
US7858730B2 (en) 2007-07-12 2010-12-28 Eastman Chemical Company Multi-level tubular reactor with dual headers
US9944615B2 (en) 2014-05-08 2018-04-17 Eastman Chemical Company Purifying crude furan 2,5-dicarboxylic acid by hydrogenation and a purge zone
US10010812B2 (en) 2014-05-08 2018-07-03 Eastman Chemical Company Furan-2,5-dicarboxylic acid purge process
US9604202B2 (en) 2014-05-08 2017-03-28 Eastman Chemical Company Furan-2,5-dicarboxylic acid purge process
US20190023838A1 (en) 2017-07-20 2019-01-24 Eastman Chemical Company Production of polyethylene furanoate in a retrofitted pet plant
US10344011B1 (en) 2018-05-04 2019-07-09 Eastman Chemical Company Furan-2,5-dicarboxylic acid purge process
US10526301B1 (en) 2018-10-18 2020-01-07 Eastman Chemical Company Production of purified dialkyl-furan-2,5-dicarboxylate (DAFD) in a retrofitted DMT plant

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1545487A (en) * 1966-11-30 1968-11-08 Bemberg Spa Continuous process for the production of polymethylene terephthalate with a high degree of polymerization, the product thus obtained and fibers made therefrom
DE1920954A1 (en) * 1968-04-24 1969-11-06 Asahi Chemical Ind Process and apparatus for the production of polymers
DE1959455A1 (en) * 1968-11-26 1970-06-11 Rhodiaceta Method and device for the production of polyesters
US3640962A (en) * 1968-05-08 1972-02-08 Hoechst Ag Polyester polycondensation process under decreasing temperatures

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US401685A (en) * 1889-04-16 Ments
US1200996A (en) * 1912-10-14 1916-10-10 Techno Chemical Lab Ltd Method of evaporation, &c.
US1327599A (en) * 1914-05-25 1920-01-06 Andrew M Hunt Apparatus for cooling and scrubbing gases
DE517176C (en) * 1927-01-10 1931-01-31 Karl Fried Dr Device for evaporating and thickening liquids
FR702279A (en) * 1929-12-10 1931-04-03 gas and smoke purifier
US2689839A (en) * 1951-08-22 1954-09-21 Du Pont Dispersion of delusterants in polyamides
US2994724A (en) * 1958-08-14 1961-08-01 Exxon Research Engineering Co Cyclodiene dimer vapor phase cracking method and furnace
NL130338C (en) * 1963-06-11 1900-01-01
GB1101348A (en) * 1964-06-16 1968-01-31 Ici Ltd Improvements in sodium bicarbonate manufacture by the ammonia-soda process
US3499873A (en) * 1967-06-22 1970-03-10 Vickers Zimmer Ag Preparation of polyethylene terephthalate by means of free falling films
NL6809754A (en) * 1968-04-11 1969-10-14
DE1920945C3 (en) * 1969-04-24 1973-11-08 Polysius Ag, 4723 Neubeckum Device for cooling pourable material
DE2514116C3 (en) * 1975-03-29 1983-03-17 Basf Ag, 6700 Ludwigshafen Process for the continuous production of linear, high molecular weight polybutylene terephthalates
DE2557580A1 (en) * 1975-12-20 1977-06-30 Dynamit Nobel Ag PROCESS AND DEVICE FOR PRODUCING POLYCONDENSATE

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1545487A (en) * 1966-11-30 1968-11-08 Bemberg Spa Continuous process for the production of polymethylene terephthalate with a high degree of polymerization, the product thus obtained and fibers made therefrom
DE1920954A1 (en) * 1968-04-24 1969-11-06 Asahi Chemical Ind Process and apparatus for the production of polymers
US3640962A (en) * 1968-05-08 1972-02-08 Hoechst Ag Polyester polycondensation process under decreasing temperatures
DE1959455A1 (en) * 1968-11-26 1970-06-11 Rhodiaceta Method and device for the production of polyesters

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
CHEMICAL ABSTRACTS, vol. 73, no. 12, 21 sept 1970, Columbus, Ohio, (USA) FISYUK, L.T. GRAIZEL, L.A.: "Intensification of the poly condensation stage during the production of poly (ethylene terephtphalate), Seite 39, 1e Spalte, Zusammenfassung 57003q, KHIM. VOLOKNA 1970, (3) 70-1 *

Also Published As

Publication number Publication date
US4214072A (en) 1980-07-22
US4235844A (en) 1980-11-25
EP0000918B1 (en) 1982-03-17
JPS5443997A (en) 1979-04-06
DE2861668D1 (en) 1982-04-15
EP0000918A2 (en) 1979-03-07
IT7826342A0 (en) 1978-07-31
IT1097584B (en) 1985-08-31

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