DK201783A - Fremgangsmaade til fjernelse af nitrogen fra naturgas - Google Patents

Fremgangsmaade til fjernelse af nitrogen fra naturgas Download PDF

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Publication number
DK201783A
DK201783A DK201783A DK201783A DK201783A DK 201783 A DK201783 A DK 201783A DK 201783 A DK201783 A DK 201783A DK 201783 A DK201783 A DK 201783A DK 201783 A DK201783 A DK 201783A
Authority
DK
Denmark
Prior art keywords
nitrogen
natural gas
heat pump
pressure
methane
Prior art date
Application number
DK201783A
Other languages
Danish (da)
English (en)
Other versions
DK201783D0 (da
Inventor
James Willers Pervier
Harvey Lewis Vines
Iii Vincent Marano
Michael Andrew Patterson
Original Assignee
Air Prod & Chem
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Prod & Chem filed Critical Air Prod & Chem
Publication of DK201783D0 publication Critical patent/DK201783D0/da
Publication of DK201783A publication Critical patent/DK201783A/da

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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0209—Natural gas or substitute natural gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0233—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of CnHm with 1 carbon atom or more
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0257—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/02—Processes or apparatus using separation by rectification in a single pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/50—Processes or apparatus using separation by rectification using multiple (re-)boiler-condensers at different heights of the column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/72—Refluxing the column with at least a part of the totally condensed overhead gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/02—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum
    • F25J2205/04—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum in the feed line, i.e. upstream of the fractionation step
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00—Processes characterised by the type or other details of the feed stream
    • F25J2210/06—Splitting of the feed stream, e.g. for treating or cooling in different ways
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2240/00—Processes or apparatus involving steps for expanding of process streams
    • F25J2240/02—Expansion of a process fluid in a work-extracting turbine (i.e. isentropic expansion), e.g. of the feed stream
    • F25J2240/12—Expansion of a process fluid in a work-extracting turbine (i.e. isentropic expansion), e.g. of the feed stream the fluid being nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/04—Internal refrigeration with work-producing gas expansion loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/12—External refrigeration with liquid vaporising loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/60—Closed external refrigeration cycle with single component refrigerant [SCR], e.g. C1-, C2- or C3-hydrocarbons
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/66—Closed external refrigeration cycle with multi component refrigerant [MCR], e.g. mixture of hydrocarbons
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00—Refrigeration
    • Y10S62/927—Natural gas from nitrogen

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DK201783A 1982-05-10 1983-05-05 Fremgangsmaade til fjernelse af nitrogen fra naturgas DK201783A (da)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/376,365 US4411677A (en) 1982-05-10 1982-05-10 Nitrogen rejection from natural gas

Publications (2)

Publication Number Publication Date
DK201783D0 DK201783D0 (da) 1983-05-05
DK201783A true DK201783A (da) 1983-11-11

Family

ID=23484730

Family Applications (1)

Application Number Title Priority Date Filing Date
DK201783A DK201783A (da) 1982-05-10 1983-05-05 Fremgangsmaade til fjernelse af nitrogen fra naturgas

Country Status (7)

Country Link
US (1) US4411677A (fr)
EP (1) EP0094062B1 (fr)
AT (1) ATE31578T1 (fr)
CA (1) CA1195231A (fr)
DE (1) DE3375044D1 (fr)
DK (1) DK201783A (fr)
NO (1) NO158478C (fr)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
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US4767428A (en) * 1982-03-10 1988-08-30 Flexivol, Inc. Nitrogen removal system
US4496382A (en) * 1983-03-21 1985-01-29 Air Products And Chemicals, Inc. Process using serpentine heat exchange relationship for condensing substantially single component gas streams
US4504295A (en) * 1983-06-01 1985-03-12 Air Products And Chemicals, Inc. Nitrogen rejection from natural gas integrated with NGL recovery
US4501600A (en) * 1983-07-15 1985-02-26 Union Carbide Corporation Process to separate nitrogen from natural gas
US4592767A (en) * 1985-05-29 1986-06-03 Union Carbide Corporation Process for separating methane and nitrogen
US4662919A (en) * 1986-02-20 1987-05-05 Air Products And Chemicals, Inc. Nitrogen rejection fractionation system for variable nitrogen content natural gas
US4710212A (en) * 1986-09-24 1987-12-01 Union Carbide Corporation Process to produce high pressure methane gas
US4732598A (en) * 1986-11-10 1988-03-22 Air Products And Chemicals, Inc. Dephlegmator process for nitrogen rejection from natural gas
US4761167A (en) * 1986-12-12 1988-08-02 Air Products And Chemicals, Inc. Hydrocarbon recovery from fuel gas
FR2644160B1 (fr) * 1989-03-09 1991-05-10 Air Liquide Procede et installation de recuperation des hydrocarbures les plus lourds d'un melange gazeux
US4948404A (en) * 1989-08-03 1990-08-14 Phillips Petroleum Company Liquid nitrogen by-product production in an NGL plant
US5051120A (en) * 1990-06-12 1991-09-24 Union Carbide Industrial Gases Technology Corporation Feed processing for nitrogen rejection unit
US5375422A (en) * 1991-04-09 1994-12-27 Butts; Rayburn C. High efficiency nitrogen rejection unit
FR2764972B1 (fr) * 1997-06-24 1999-07-16 Inst Francais Du Petrole Procede de liquefaction d'un gaz naturel a deux etages interconnectes
US5802871A (en) * 1997-10-16 1998-09-08 Air Products And Chemicals, Inc. Dephlegmator process for nitrogen removal from natural gas
US6214258B1 (en) 1998-08-13 2001-04-10 Air Products And Chemicals, Inc. Feed gas pretreatment in synthesis gas production
MY117066A (en) 1998-10-22 2004-04-30 Exxon Production Research Co Process for removing a volatile component from natural gas
MY114649A (en) 1998-10-22 2002-11-30 Exxon Production Research Co A process for separating a multi-component pressurized feed stream using distillation
US6978638B2 (en) 2003-05-22 2005-12-27 Air Products And Chemicals, Inc. Nitrogen rejection from condensed natural gas
JP4763039B2 (ja) * 2005-03-30 2011-08-31 フルオー・テクノロジーズ・コーポレイシヨン Ｌｎｇ再ガス化の精製および発電との統合
EP1734027B1 (fr) * 2005-06-14 2012-08-15 Toyo Engineering Corporation Procédé et appareil pour la séparation d'hydrocarbures de gaz naturel liquifié
US9243842B2 (en) 2008-02-15 2016-01-26 Black & Veatch Corporation Combined synthesis gas separation and LNG production method and system
CA2734853A1 (fr) * 2008-10-07 2010-04-15 Exxonmobil Upstream Research Company Recuperation de l'helium dans le gaz naturel integree a la recuperation du lgn
US10113127B2 (en) 2010-04-16 2018-10-30 Black & Veatch Holding Company Process for separating nitrogen from a natural gas stream with nitrogen stripping in the production of liquefied natural gas
WO2012075266A2 (fr) 2010-12-01 2012-06-07 Black & Veatch Corporation Récupération de ngl à partir de gaz naturel à l'aide d'un mélange de réfrigérants
US20120324943A1 (en) * 2011-06-21 2012-12-27 Butts Rayburn C Two Step Nitrogen and Methane Separation Process
US10139157B2 (en) * 2012-02-22 2018-11-27 Black & Veatch Holding Company NGL recovery from natural gas using a mixed refrigerant
EA201491790A1 (ru) * 2012-03-30 2015-01-30 Эксонмобил Апстрим Рисерч Компани Способ образования сжиженного природного газа
MX2015006658A (es) * 2013-01-24 2015-08-10 Exxonmobil Upstream Res Co Produccion de gas natural licuado.
GB201306342D0 (en) * 2013-04-08 2013-05-22 Costain Oil Gas & Process Ltd Process and apparatus for separation of hydrocarbons and nitrogen
US10563913B2 (en) 2013-11-15 2020-02-18 Black & Veatch Holding Company Systems and methods for hydrocarbon refrigeration with a mixed refrigerant cycle
US9574822B2 (en) 2014-03-17 2017-02-21 Black & Veatch Corporation Liquefied natural gas facility employing an optimized mixed refrigerant system
US9816754B2 (en) 2014-04-24 2017-11-14 Air Products And Chemicals, Inc. Integrated nitrogen removal in the production of liquefied natural gas using dedicated reinjection circuit
US9945604B2 (en) * 2014-04-24 2018-04-17 Air Products And Chemicals, Inc. Integrated nitrogen removal in the production of liquefied natural gas using refrigerated heat pump
US20150308737A1 (en) * 2014-04-24 2015-10-29 Air Products And Chemicals, Inc. Integrated Nitrogen Removal in the Production of Liquefied Natural Gas Using Intermediate Feed Gas Separation
CA2855383C (fr) 2014-06-27 2015-06-23 Rtj Technologies Inc. Procede et disposition pour produire du methane liquefie a partir de diverses sources de gaz
US9816752B2 (en) 2015-07-22 2017-11-14 Butts Properties, Ltd. System and method for separating wide variations in methane and nitrogen
CA2903679C (fr) 2015-09-11 2016-08-16 Charles Tremblay Procede et systeme de controle du debit massique de methane pour la production de methane liquefie
US10520250B2 (en) 2017-02-15 2019-12-31 Butts Properties, Ltd. System and method for separating natural gas liquid and nitrogen from natural gas streams
US11686528B2 (en) 2019-04-23 2023-06-27 Chart Energy & Chemicals, Inc. Single column nitrogen rejection unit with side draw heat pump reflux system and method
US11378333B2 (en) 2019-12-13 2022-07-05 Bcck Holding Company System and method for separating methane and nitrogen with reduced horsepower demands
US11650009B2 (en) 2019-12-13 2023-05-16 Bcck Holding Company System and method for separating methane and nitrogen with reduced horsepower demands
CN114777416B (zh) * 2022-04-22 2023-02-07 杭州特盈能源技术发展有限公司 一种绿电高效转化低能耗空分储能工艺

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US3238735A (en) * 1962-12-05 1966-03-08 Chevron Res Distillation of low-boiling components
DE1939114B2 (de) * 1969-08-01 1979-01-25 Linde Ag, 6200 Wiesbaden Verflüssigungsverfahren für Gase und Gasgemische, insbesondere für Erdgas
DE2022954C3 (de) * 1970-05-12 1978-05-18 Linde Ag, 6200 Wiesbaden Verfahren zur Zerlegung von stickstoffhaltigem Erdgas
DE2734080A1 (de) * 1977-07-28 1979-02-15 Linde Ag Verfahren zum abtrennen von methan aus einem methanhaltigen rohgas

Also Published As

Publication number Publication date
ATE31578T1 (de) 1988-01-15
NO158478C (no) 1988-09-14
NO831636L (no) 1983-11-11
DK201783D0 (da) 1983-05-05
EP0094062A3 (en) 1985-01-30
US4411677A (en) 1983-10-25
NO158478B (no) 1988-06-06
EP0094062A2 (fr) 1983-11-16
EP0094062B1 (fr) 1987-12-23
DE3375044D1 (en) 1988-02-04
CA1195231A (fr) 1985-10-15

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