DE723492C - Process for the production of preparations by mixing aqueous solutions of cellulose ether carboxylic acids with aluminum salt solutions - Google Patents

Process for the production of preparations by mixing aqueous solutions of cellulose ether carboxylic acids with aluminum salt solutions

Info

Publication number
DE723492C
DE723492C DEI63145D DEI0063145D DE723492C DE 723492 C DE723492 C DE 723492C DE I63145 D DEI63145 D DE I63145D DE I0063145 D DEI0063145 D DE I0063145D DE 723492 C DE723492 C DE 723492C
Authority
DE
Germany
Prior art keywords
solutions
cellulose ether
ether carboxylic
carboxylic acids
preparations
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DEI63145D
Other languages
German (de)
Inventor
Franz Nestelberger
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IG Farbenindustrie AG
Original Assignee
IG Farbenindustrie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IG Farbenindustrie AG filed Critical IG Farbenindustrie AG
Priority to DEI63145D priority Critical patent/DE723492C/en
Application granted granted Critical
Publication of DE723492C publication Critical patent/DE723492C/en
Expired legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03Polysaccharides or derivatives thereof
    • D06M15/05Cellulose or derivatives thereof
    • D06M15/09Cellulose ethers

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Description

Verfahren zur Herstellung von Zubereitungen durch Mischen von wässerigen Lösungen von Celluloseäthercarbonsäuren mit Aluminiumsalzlösungen Aus Lösungen von CelI:uloseäth ercarbonsäuren oder denen Salzen, wie sie beispielsweise nach Patent 33z 203 oder Patent 712 666 hergestellt werden können, werden die Celluloseät'hercarb:onsäuren durch Zusatz von Aluminiumsalzen mehr oder weniger als Aluminiumsalze ausgefällt. Diese Ausfällung macht die technische Anwendung der viscosen Lösungen in Gegenwart von Aluminiumsalzen unmöglich,.The method for producing preparations by mixing aqueous solutions of cellulose ether carboxylic acids having from aluminum salt solutions from solutions of Celi: ercarbonsäuren uloseäth or to which salts, such as may be prepared for example according to 33z 203 or Patent 712,666, the Celluloseät'hercarb are: onic acids by the addition of Aluminum salts more or less precipitated than aluminum salts. This precipitation makes the technical application of the viscous solutions in the presence of aluminum salts impossible.

Es wurde nun gefunden, daß die oben beschriebene Ausfällung von Aluminiumsalzen der Cellulos:eätlzercarbonsäuren bei Anwesenheit von wasserlöslichen aliphatischen Oxycarbonsäuren, z. B. Glykol-, Milch-, Wein-, Citronen- und Apfelsäure, ferner von Äth@ercarbonsäuren, z. B. Methoxyessigsäure und Diglykolsäure, von Thioäthercarbonsäuren, z. B. Thiodiglykolsäure, sowie von Ameisensäure nicht eintritt. Der Zusatz der Säuren erfolgt am besten entweder zur Lösung des Ahiminiumsalzes .oder zur wässerigen Lösung der Celluloseäthercarb:onsäuren vor dem Mischen der Lösungen. Man setzt die Säuren in Mengen von mindestens 2o% der angewandten Celluloseäthercarbonsäuren hinzu. Das vorliegende Verfahren kann beispielsweise im Zeugdruck oder bei Appreturverfahren angewendet werden.It has now been found that the above-described precipitation of aluminum salts Cellulose: ether carboxylic acids in the presence of water-soluble aliphatic ones Oxycarboxylic acids, e.g. B. glycolic, lactic, tartaric, citric and malic acid, also of Äth @ ercarbonsäuren, z. B. methoxyacetic acid and diglycolic acid, of thioether carboxylic acids, z. B. thiodiglycolic acid, as well as formic acid does not occur. The addition of acids is best done either to the solution of the ammonium salt. or to the aqueous solution the cellulose ether carb: onic acids before mixing the solutions. You set the acids in amounts of at least 2o% of the cellulose ether carboxylic acids used. That The present process can be, for example, in fabric printing or in finishing processes be applied.

Claims (1)

P<1TRNTANSPRUC H Verfahren zur Herstellung von Zubereitungen durch Mischen von wässerigen Lösungen von Cell.uloseätli!ercarbonsäuren mit Aluminiumsalzlösungen, dadurch gekennzeichnet, daß man eine der beiden Lösungen vor dem Vermischen mit wasserlöslichen Oxycarbonsäuren, Äthern derselben, fihioäthercarb:onsäuren oder Ameisensäure in Mengen von mindesüens 2o % der angewandten Celluloseäthercarbonsäure versetzt. ,P <1TRNTANSPRUC H Process for the manufacture of preparations by Mixing of aqueous solutions of cellulose ether carboxylic acids with aluminum salt solutions, characterized in that one of the two solutions before mixing with water-soluble oxycarboxylic acids, ethers thereof, fihioäthercarb: onsäuren or Formic acid in amounts of at least 20% of the cellulose ether carboxylic acid used offset. ,
DEI63145D 1938-12-13 1938-12-13 Process for the production of preparations by mixing aqueous solutions of cellulose ether carboxylic acids with aluminum salt solutions Expired DE723492C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEI63145D DE723492C (en) 1938-12-13 1938-12-13 Process for the production of preparations by mixing aqueous solutions of cellulose ether carboxylic acids with aluminum salt solutions

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEI63145D DE723492C (en) 1938-12-13 1938-12-13 Process for the production of preparations by mixing aqueous solutions of cellulose ether carboxylic acids with aluminum salt solutions

Publications (1)

Publication Number Publication Date
DE723492C true DE723492C (en) 1942-08-05

Family

ID=7195843

Family Applications (1)

Application Number Title Priority Date Filing Date
DEI63145D Expired DE723492C (en) 1938-12-13 1938-12-13 Process for the production of preparations by mixing aqueous solutions of cellulose ether carboxylic acids with aluminum salt solutions

Country Status (1)

Country Link
DE (1) DE723492C (en)

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