DE69309942D1 - Verfahren zur herstellung von adipic säure und anderen aliphatischen dibasischen säuren - Google Patents

Verfahren zur herstellung von adipic säure und anderen aliphatischen dibasischen säuren

Info

Publication number
DE69309942D1
DE69309942D1 DE69309942T DE69309942T DE69309942D1 DE 69309942 D1 DE69309942 D1 DE 69309942D1 DE 69309942 T DE69309942 T DE 69309942T DE 69309942 T DE69309942 T DE 69309942T DE 69309942 D1 DE69309942 D1 DE 69309942D1
Authority
DE
Germany
Prior art keywords
adipic acid
dibasic acids
aliphatic dibasic
producing adipic
producing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69309942T
Other languages
English (en)
Other versions
DE69309942T2 (de
Inventor
John Kollar
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Redox Technologies Inc
Original Assignee
Redox Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Redox Technologies Inc filed Critical Redox Technologies Inc
Publication of DE69309942D1 publication Critical patent/DE69309942D1/de
Application granted granted Critical
Publication of DE69309942T2 publication Critical patent/DE69309942T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69309942T 1992-09-25 1993-09-13 Verfahren zur herstellung von adipic säure und anderen aliphatischen dibasischen säuren Expired - Fee Related DE69309942T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US95174392A 1992-09-25 1992-09-25
US08/053,791 US5321157A (en) 1992-09-25 1993-04-26 Process for the preparation of adipic acid and other aliphatic dibasic acids
PCT/EP1993/002470 WO1994007833A1 (en) 1992-09-25 1993-09-13 A process for the preparation of adipic acid and other aliphatic dibasic acids

Publications (2)

Publication Number Publication Date
DE69309942D1 true DE69309942D1 (de) 1997-05-22
DE69309942T2 DE69309942T2 (de) 1997-09-04

Family

ID=26732250

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69309942T Expired - Fee Related DE69309942T2 (de) 1992-09-25 1993-09-13 Verfahren zur herstellung von adipic säure und anderen aliphatischen dibasischen säuren

Country Status (10)

Country Link
US (1) US5321157A (de)
EP (1) EP0662942B1 (de)
JP (1) JPH08502247A (de)
CN (1) CN1086804A (de)
AU (1) AU4959893A (de)
CA (1) CA2145307A1 (de)
DE (1) DE69309942T2 (de)
MX (1) MX9305612A (de)
TW (1) TW243444B (de)
WO (1) WO1994007833A1 (de)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5455375A (en) * 1993-04-09 1995-10-03 Asahi Kasei Kogyo Kabushiki Kaisha Process for preparing adipic acid
FR2722783B1 (fr) * 1994-07-21 1996-08-30 Rhone Poulenc Chimie Procede de preparation d'acide adipique par oxydattion directe du cyclohexane et recyclage du catalyseur
US5505920A (en) * 1994-10-04 1996-04-09 Bayer Aktiengesellschaft Process for treatment of waste gas from a cyclohexane oxidation reactor
WO1996040610A1 (en) * 1995-06-07 1996-12-19 Twenty-First Century Research Corp. Methods and devices for making intermediate oxidation products by controlling conversions and temperatures in an atomized liquid
US5883292A (en) * 1996-01-17 1999-03-16 Twenty-First Century Research Corporation Reaction control by regulating internal condensation inside a reactor
US5801282A (en) * 1995-06-07 1998-09-01 Twenty-First Century Research Corporation Methods of making intermediate oxidation products by controlling pre-coalescing temperature and transient temperature difference in an atomized liquid
US5580531A (en) * 1995-06-07 1996-12-03 Twenty-First Century Research Corporation Devices for making reaction products by controlling transient conversion in an atomized liquid
US5654475A (en) * 1996-03-25 1997-08-05 Twenty-First Century Research Corporation Methods of making intermediate oxidation products by controlling oxidation rates in an atomized liquid
US5558842A (en) * 1995-06-07 1996-09-24 Twenty-First Century Research Corporation Devices for making reaction products by controlling pre-coalescing temperature and transient temperature difference in an atomized liquid
US5502245A (en) * 1995-06-07 1996-03-26 Twenty-First Century Research Corporation Methods of making intermediate oxidation products by controlling transient conversion in an atomized liquid
US6337051B1 (en) 1996-06-24 2002-01-08 Rpc Inc. Device for detecting formation of a second liquid phase
US5922908A (en) * 1996-06-24 1999-07-13 Twenty-First Century Research Corporation Methods for preparing dibasic acids
US6039902A (en) * 1996-06-24 2000-03-21 Rpc Inc. Methods of recycling catalyst in oxidations of hydrocarbons
US6143927A (en) 1996-06-24 2000-11-07 Rpc Inc. Methods for removing catalyst after oxidation of hydrocarbons
US6288270B1 (en) 1996-06-24 2001-09-11 Rpc Inc. Methods for controlling the reaction rate of a hydrocarbon to an acid by making phase-related adjustments
US20010053864A1 (en) * 1996-08-21 2001-12-20 Decoster David C. Devices for controlling the reaction rate and/or reactivity of hydrocarbon to an intermediate oxidation product by adjusting the oxidant consumption rate
EP0923524A1 (de) 1996-08-21 1999-06-23 Twenty-First Century Research Corporation Verfahren und vorrichtungen zur steuerung einer reaktion durch einstellung des oxydationsmittelverbrauchs
US5801273A (en) 1996-08-21 1998-09-01 Twenty-First Century Research Corporation Methods and devices for controlling the reaction rate of a hydrocarbon to an intermediate oxidation product by pressure drop adjustments
US6103933A (en) * 1996-11-07 2000-08-15 Rpc Inc. Methods for controlling the oxidation rate of a hydrocarbon by adjusting the ratio of the hydrocarbon to a rate-modulator
US5817868A (en) * 1996-11-12 1998-10-06 Twenty-First Century Research Corporation Method and devices for controlling the oxidation of a hydrocarbon to an acid by regulating temperature/conversion relationship in multi-stage arrangements
US5824819A (en) * 1996-12-18 1998-10-20 Twenty-First Century Research Corporation Methods of preparing an intermediate oxidation product from a hydrocarbon by utilizing an activated initiator
US6037491A (en) * 1997-07-25 2000-03-14 Rpc Inc. Methods and devices for controlling hydrocarbon oxidations to respective acids by adjusting the solvent to hydrocarbon ratio
US5929277A (en) * 1997-09-19 1999-07-27 Twenty-First Century Research Corporation Methods of removing acetic acid from cyclohexane in the production of adipic acid
US5908589A (en) * 1997-12-08 1999-06-01 Twenty-First Century Research Corporation Methods for separating catalyst from oxidation mixtures containing dibasic acids
BR9907687A (pt) 1998-02-09 2000-11-14 Rpc Inc Processo para o tratamento de catalisador cobalto em misturas de oxidação de hidrocarbonetos a ácidos dibásicos
BR9907998A (pt) * 1998-02-19 2000-10-24 Rpc Inc Processos e dispositivos para a separação de catalisador de misturas de oxidação
US6433220B1 (en) 1998-07-02 2002-08-13 Rpc Inc. Methods of extracting catalyst from a reaction mixture in the oxidation of cyclohexane to adipic acid
US6340420B1 (en) 1998-07-06 2002-01-22 Rpc Inc. Methods of treating the oxidation mixture of hydrocarbons to respective dibasic acids
EP1101753A4 (de) * 1998-07-30 2002-09-11 Sumitomo Chemical Co Verfahren zur herstellung von adipinsäure
US6417128B1 (en) 1999-04-20 2002-07-09 Rpc, Inc. Methods and replacing water and cyclohexanone with acetic acid in aqueous solutions of catalyst
US6235932B1 (en) 1999-06-18 2001-05-22 Chemintel (India) Private Ltd. Process for preparation of adipic acid
FR2838122B1 (fr) * 2002-04-08 2004-05-21 Rhodia Polyamide Intermediates Procede de fabrication d'acides carboxyliques
FR2846652B1 (fr) * 2002-10-30 2006-09-22 Rhodia Polyamide Intermediates Procede de fabrication d'acides carboxyliques
FR2939052B1 (fr) * 2008-12-01 2010-12-10 Rhodia Operations Installation de cristallisation d'acide adipique
CN103288626B (zh) 2013-06-21 2014-12-10 湘潭大学 一种联产己二酸和硝基环己烷的方法
CN112939765B (zh) 2021-02-22 2022-08-09 湘潭大学 一种由环己烷联产己二酸和环己酮肟的方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2223493A (en) * 1938-07-12 1940-12-03 Du Pont Oxidation of cyclic compounds
US2589648A (en) * 1950-05-26 1952-03-18 Pan American Refining Corp Cycloalkane oxidation
US3231608A (en) * 1961-08-28 1966-01-25 Gulf Research Development Co Preparation of dibasic acids
US3390174A (en) * 1964-06-17 1968-06-25 Gulf Research Development Co Process for the preparation of adipic acid
GB1304855A (de) * 1969-08-05 1973-01-31
US3657334A (en) * 1969-12-04 1972-04-18 Inst Francais Du Petrole Process for producing adipic acid
US4105856A (en) * 1970-09-29 1978-08-08 El Paso Products Company Recovery process for aqueous waste streams in adipic acid systems
US4032569A (en) * 1975-07-14 1977-06-28 Gulf Research & Development Company Process for converting cyclohexane to adipic acid
US4158739A (en) * 1978-03-20 1979-06-19 Gulf Research & Development Company Process for converting cyclopentane to glutaric acid
EP0021118B1 (de) * 1979-06-06 1983-12-14 Mitsui Petrochemical Industries, Ltd. Katalytische Ko-Oxidation in flüssiger Phase von ungesättigten Verbindungen und Aldehyden oder Ketonen
US4263453A (en) * 1979-12-10 1981-04-21 Gulf Research & Development Company Process for converting cyclohexane to adipic acid
DE3468861D1 (en) * 1983-06-02 1988-02-25 New Japan Chem Co Ltd Process for preparing carboxylic acid
US4902827A (en) * 1988-05-03 1990-02-20 Eastman Kodak Company Process for the preparation of adipic acid
US5221800A (en) * 1989-09-05 1993-06-22 Amoco Corporation One step air oxidation of cyclohexane to produce adipic acid

Also Published As

Publication number Publication date
CN1086804A (zh) 1994-05-18
EP0662942B1 (de) 1997-04-16
MX9305612A (es) 1994-03-31
CA2145307A1 (en) 1994-04-14
TW243444B (de) 1995-03-21
AU4959893A (en) 1994-04-26
US5321157A (en) 1994-06-14
EP0662942A1 (de) 1995-07-19
WO1994007833A1 (en) 1994-04-14
JPH08502247A (ja) 1996-03-12
DE69309942T2 (de) 1997-09-04

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee