DE6823C - Method of making wine beautiful and clarifying spirits - Google Patents
Method of making wine beautiful and clarifying spiritsInfo
- Publication number
- DE6823C DE6823C DENDAT6823D DE6823DA DE6823C DE 6823 C DE6823 C DE 6823C DE NDAT6823 D DENDAT6823 D DE NDAT6823D DE 6823D A DE6823D A DE 6823DA DE 6823 C DE6823 C DE 6823C
- Authority
- DE
- Germany
- Prior art keywords
- clarifying
- spirits
- beautiful
- making wine
- oxygen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 235000014101 wine Nutrition 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title description 2
- 235000015096 spirit Nutrition 0.000 title description 2
- 229910001882 dioxygen Inorganic materials 0.000 claims description 3
- 238000005352 clarification Methods 0.000 claims description 2
- 235000020094 liqueur Nutrition 0.000 claims description 2
- 239000007788 liquid Substances 0.000 description 6
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- ZJRXSAYFZMGQFP-UHFFFAOYSA-N Barium peroxide Chemical compound [Ba+2].[O-][O-] ZJRXSAYFZMGQFP-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- QVQLCTNNEUAWMS-UHFFFAOYSA-N Barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L Barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
- 229910001864 baryta Inorganic materials 0.000 description 2
- 229910052601 baryte Inorganic materials 0.000 description 2
- 239000010428 baryte Substances 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L cacl2 Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 2
- 239000001110 calcium chloride Substances 0.000 description 2
- 229910001628 calcium chloride Inorganic materials 0.000 description 2
- 238000005530 etching Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- -1 chlorine-calcium Chemical compound 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/12—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages without precipitation
- C12H1/14—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages without precipitation with non-precipitating compounds, e.g. sulfiting; Sequestration, e.g. with chelate-producing compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Description
PATENTSCHRIFTPATENT LETTERING
Klasse 6.Grade 6.
ALFRED CORDS in BERLIN. Verfahren, Wein zu schönen und Spiritus zu klären.ALFRED CORDS in BERLIN. Method of making wine beautiful and clarifying spirits.
Patentirt im Deutschen Reiche vom 5. December 1878 ab.Patented in the German Empire on December 5, 1878.
Die Schönung von Weinen und Klärung von Spiritus und Liqueuren bewirke ich durch Sättigung genannter Flüssigkeiten mit Sauerstoffgas.I bring about the fining of wines and the clarification of alcohol and liqueurs through saturation named liquids with oxygen gas.
Das zu erwähntem Zwecke nothwendige Gas entwickele ich auf folgende Weise:I develop the gas necessary for the above-mentioned purpose in the following way:
Ich nehme ein Rohr aus Eisen, Chamotte, Schmelztiegelmasse etc., welches an einem Ende einen gasdichten Hahn hat, schiebe in dieses eine stählerne oder Platinschale mit Aetzbaryt, erhitze nun das Rohr bis zur Rothglut, öffne dann den Hahn und führe mittelst eines vor das andere Ende des Rohres gelegten Aspirators Luft hindurch. I take a pipe made of iron, chamotte, crucible mass, etc., which is at one end has a gas-tight tap, insert a steel or platinum bowl with caustic soda into it, Now heat the pipe until it burns red, then open the tap and use one to bring it out the other end of the tube put air through the aspirator.
Die atmosphärische Luft, welche mittelst Kalilauge gewaschen und durch Chlorkalcium getrocknet worden ist, wird nun durch das glühende Rohr geführt, spaltet sich naturgemäfs, der Aetzbaryt absorbirt den frei gewordenen Sauerstoff-und wandelt sich in Baryumsuperoxyd um, während die anderen Bestandtheile der Luft, wie Stickstoff etc., durch den Aspirator abgezogen werden.The atmospheric air, washed with potassium hydroxide and dried with calcium chloride is now passed through the glowing pipe, splits naturally, the etching barite absorbs what has become free Oxygen and converts to barium peroxide, while the other components the air, such as nitrogen etc., can be withdrawn through the aspirator.
Wenn man nun annehmen kann, dafs die Umwandlung des Aetzbaryts in Baryumsuperoxyd eine vollständige ist, wird der schon früher erwähnte Hahn geschlossen, der Aspirator abgenommen und an seiner Stelle eine Trommel mit Chlorealciumfüllung vorgelegt. Das Feuer des Ofens, durch welches das Rohr mit der Barytschale geführt ist, wird nun verstärkt bis zur Weifsglut, das Baryumsuperoxyd giebt dann seinen Sauerstoff ab und wandelt sich wieder in Aetzbaryt um; der entweichende Sauerstoff wird durch die Trommel mit Chlorcalcium geführt, woselbst er die etwa noch vorhandene Kohlensäure oder das Ammoniak abgiebt und sodann durch ein Rohr bis auf den Boden des Gefäfses, welches mit der zu schönenden oder zu klärenden Flüssigkeit gefüllt ist, geleitet. Die qualificirte Flüssigkeit sättigt sich nunmehr mit dem chemisch reinen Sauerstoffgas.If one can now assume that the conversion of the etching barite into barium superoxide is complete, the valve mentioned earlier is closed and the aspirator is removed and in its place a drum filled with chlorine-calcium. The fire of the furnace, through which the pipe with the baryta shell is passed, is now reinforced up to to the white glow, the barium superoxide then gives off its oxygen and changes again in caustic soda; the escaping oxygen is fed through the drum with calcium chloride, where it releases any remaining carbonic acid or ammonia and then through a pipe down to the bottom of the vessel, which is connected to the or liquid to be clarified is filled. The qualified liquid is now saturated with it the chemically pure oxygen gas.
Der Procefs ist als vollendet zu betrachten, wenn überschüssiger Sauerstoff vorhanden, was man leicht durch ein Probirröhrchen, welches durch die obere Wandung des nicht vollständig gefüllten Gefäfses geführt wird, constatiren kann, wenn man einen glimmenden Spahn an die äufsere Mündung hält und dieser sich dann entzündet.The process is to be regarded as complete when there is excess oxygen, what one easily through a test tube, which through the upper wall of the not completely when the vessel is filled, it can be established if a smoldering spahn is touched to the outer mouth holds and this then ignites.
Durch den Zutritt des Sauerstoffes zu den erwähnten Flüssigkeiten werden die an dieselben gebundenen schleimigen Substanzen etc. gefällt. ■ . 'Through the admission of oxygen to the liquids mentioned, they become the same bound slimy substances etc. like. ■. '
Um zu vermeiden, dafs die Flüssigkeiten bei einem plötzlichen Nachlassen der Gasentwickelung bis in das Rohr mit der Barytschale steigen, wird in das Gefäfs, in welchem sich die zu klärende Flüssigkeit befindet, von oben ein Glasrohr (Sicherheitsrohr) bis zu drei Viertel der Höhe eingeführt.In order to avoid that the liquids flow in the event of a sudden cessation of the evolution of gas as far as the tube with the baryta bowl, will go into the vessel in which the liquid to be clarified is up to three quarters of a glass tube (safety tube) from above the height introduced.
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE6823C true DE6823C (en) |
Family
ID=284856
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT6823D Active DE6823C (en) | Method of making wine beautiful and clarifying spirits |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE6823C (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1134466B (en) * | 1961-08-08 | 1962-08-09 | Zentralinstitut Schweiss | Method and device for welding hollow bodies, in particular pipes, made of foils of high-alloy steel |
| US5172846A (en) * | 1990-12-20 | 1992-12-22 | Mitsubishi Jukogyo Kabushiki Kaisha | Butting device for joining running steel sheets |
-
0
- DE DENDAT6823D patent/DE6823C/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1134466B (en) * | 1961-08-08 | 1962-08-09 | Zentralinstitut Schweiss | Method and device for welding hollow bodies, in particular pipes, made of foils of high-alloy steel |
| US5172846A (en) * | 1990-12-20 | 1992-12-22 | Mitsubishi Jukogyo Kabushiki Kaisha | Butting device for joining running steel sheets |
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