DE60203335D1 - Process for the preparation of microcapsules by interfacial polycondensation between polyoxyalkylene amine and acid chloride - Google Patents
Process for the preparation of microcapsules by interfacial polycondensation between polyoxyalkylene amine and acid chlorideInfo
- Publication number
- DE60203335D1 DE60203335D1 DE60203335T DE60203335T DE60203335D1 DE 60203335 D1 DE60203335 D1 DE 60203335D1 DE 60203335 T DE60203335 T DE 60203335T DE 60203335 T DE60203335 T DE 60203335T DE 60203335 D1 DE60203335 D1 DE 60203335D1
- Authority
- DE
- Germany
- Prior art keywords
- microcapsules
- acid chloride
- preparation
- organic phase
- interfacial polycondensation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/06—Making microcapsules or microballoons by phase separation
- B01J13/14—Polymerisation; cross-linking
- B01J13/16—Interfacial polymerisation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2984—Microcapsule with fluid core [includes liposome]
- Y10T428/2985—Solid-walled microcapsule from synthetic polymer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Medicinal Preparation (AREA)
Abstract
The present invention relates to a process of obtaining microcapsules, comprising mainly the following stages:preparing a scarcely water-soluble organic phase containing a determined amount of acid chlorides,forming an emulsion of said organic phase in an aqueous phase,adding to the aqueous emulsion an amount of at least one polyoxyalkylene polyamine,reacting the monomers containing the amine and acid chloride functions so as to form a polyamide membrane around the emulsified organic phase,recovering the microcapsules obtained.The present invention also relates to a microcapsule.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0105674 | 2001-04-27 | ||
FR0105674A FR2823994B1 (en) | 2001-04-27 | 2001-04-27 | PROCESS FOR THE MANUFACTURE OF MICROCAPSULES BY INTERFACIAL POLYCONDENSATION WITH POLYOXYALKYNEAMINE AND ACID CHLORIDES |
Publications (2)
Publication Number | Publication Date |
---|---|
DE60203335D1 true DE60203335D1 (en) | 2005-04-28 |
DE60203335T2 DE60203335T2 (en) | 2006-02-09 |
Family
ID=8862758
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE60203335T Expired - Lifetime DE60203335T2 (en) | 2001-04-27 | 2002-04-12 | Process for the preparation of microcapsules by interfacial polycondensation between polyoxyalkylene amine and acid chloride |
Country Status (5)
Country | Link |
---|---|
US (1) | US6706397B2 (en) |
EP (1) | EP1254701B1 (en) |
AT (1) | ATE291488T1 (en) |
DE (1) | DE60203335T2 (en) |
FR (1) | FR2823994B1 (en) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1360259A1 (en) * | 2001-02-07 | 2003-11-12 | Institut Francais Du Petrole | Method for making a quasi-incompressible phase-change material, shear-thinned and with low heat conductivity |
EP1640063A1 (en) * | 2004-09-22 | 2006-03-29 | Cognis IP Management GmbH | Polyamide Microcapsules |
US20070244211A1 (en) * | 2004-11-22 | 2007-10-18 | Phelan John C | Crosslinkable poly(oxyalkylene)-containing polyamide prepolymers |
CN102002771B (en) * | 2010-10-21 | 2012-06-06 | 大连工业大学 | Phase-change microcapsule heat storage and temperature adjustment polyacrylonitrile fiber and wet spinning preparation method thereof |
ES2436268T3 (en) | 2010-12-21 | 2013-12-30 | Procter & Gamble International Operations Sa | Encapsulated |
MX2016013034A (en) | 2014-04-11 | 2017-02-15 | Novozymes As | Detergent composition. |
US20170044468A1 (en) * | 2014-05-02 | 2017-02-16 | Novozymes A/S | Detergent Composition |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1091141A (en) * | 1963-12-13 | 1967-11-15 | Wallace & Tiernan Inc | Encapsulating liquids or solids by interfacial polymerisation |
BE795421A (en) * | 1972-02-14 | 1973-05-29 | Fuji Photo Film Co Ltd | PROCESS FOR THE PRODUCTION OF MICROCAPSULES HAVING STRONG CELLULAR WALLS |
JPS5813212B2 (en) * | 1973-07-17 | 1983-03-12 | 富士写真フイルム株式会社 | Microcapsules |
US5322862A (en) * | 1990-05-22 | 1994-06-21 | Nippon Kayaku Kabushiki Kaisha | Resin molding composition for preventing gnawing damage by animals |
-
2001
- 2001-04-27 FR FR0105674A patent/FR2823994B1/en not_active Expired - Fee Related
-
2002
- 2002-04-12 AT AT02290917T patent/ATE291488T1/en not_active IP Right Cessation
- 2002-04-12 DE DE60203335T patent/DE60203335T2/en not_active Expired - Lifetime
- 2002-04-12 EP EP02290917A patent/EP1254701B1/en not_active Expired - Lifetime
- 2002-04-24 US US10/128,280 patent/US6706397B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
US6706397B2 (en) | 2004-03-16 |
US20020158356A1 (en) | 2002-10-31 |
EP1254701A1 (en) | 2002-11-06 |
DE60203335T2 (en) | 2006-02-09 |
FR2823994B1 (en) | 2003-05-30 |
EP1254701B1 (en) | 2005-03-23 |
FR2823994A1 (en) | 2002-10-31 |
ATE291488T1 (en) | 2005-04-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8327 | Change in the person/name/address of the patent owner |
Owner name: IFP ENERGIES NOUVELLES, RUEIL-MALMAISON, FR |
|
8328 | Change in the person/name/address of the agent |
Representative=s name: VONNEMANN, KLOIBER & KOLLEGEN, 81667 MUENCHEN |