DE547987C - Process for the preparation of derivatives of high molecular weight aliphatic amines - Google Patents

Process for the preparation of derivatives of high molecular weight aliphatic amines

Info

Publication number
DE547987C
DE547987C DE1930547987D DE547987DA DE547987C DE 547987 C DE547987 C DE 547987C DE 1930547987 D DE1930547987 D DE 1930547987D DE 547987D A DE547987D A DE 547987DA DE 547987 C DE547987 C DE 547987C
Authority
DE
Germany
Prior art keywords
aliphatic amines
derivatives
preparation
molecular weight
high molecular
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE1930547987D
Other languages
German (de)
Inventor
Dr Winfrid Hentrich
Dr Karl Ott
Dr Heribert Schuessler
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IG Farbenindustrie AG
Original Assignee
IG Farbenindustrie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IG Farbenindustrie AG filed Critical IG Farbenindustrie AG
Application granted granted Critical
Publication of DE547987C publication Critical patent/DE547987C/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/14Derivatives of phosphoric acid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00Sulfonic acids; Halides, esters, or anhydrides thereof
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/04Sulfonates or sulfuric acid ester salts derived from polyhydric alcohols or amino alcohols or derivatives thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)

Description

DEUTSCHES REICHGERMAN EMPIRE

AUSGEGEBEN AM
1. APRIL 1932
ISSUED ON
APRIL 1, 1932

REICHSPATENTAMTREICH PATENT OFFICE

PATENTSCHRIFTPATENT LETTERING

JVl 547987 KLASSE 12 q GRUPPEJVl 547987 CLASS 12 q GROUP

Patentiert im Deutschen Reiche vom 7. Mai 1930 abPatented in the German Empire on May 7, 1930

Es wurde gefunden, daß man durch Umsetzung von primären oder sekundären aliphatischen Aminen als solche oder im Gemisch, welche mindestens einen Kohlenstoffrest mit mehr als 8 Kohlenstoffatomen enthalten, mit Alkylhalogeniden der allgemeinen FormelIt has been found that by reacting primary or secondary aliphatic Amines as such or in a mixture, which contain at least one carbon radical with more than 8 carbon atoms, with alkyl halides of the general formula

,- R2
X.RX-N<
, - R 2
XR X -N <

worin X ein Halogen ist und R1, R2 und R3 gleiche oder verschiedenartige aliphatische Reste bedeuten, Substanzen erhalten kann, die saponinartige Eigenschaften besitzen. Die neuen Verbindungen lösen sich in Form ihrer Salze in Wasser auf und bilden seifenartige, stark schäumende Lösungen. Infolge ihrer außerordentlich hohen Schaumkraft eignenwherein X is a halogen and R 1 , R 2 and R 3 are identical or different aliphatic radicals, substances can be obtained which have saponin-like properties. The new compounds dissolve in the form of their salts in water and form soap-like, strongly foaming solutions. Due to their extraordinarily high foaming power, they are suitable

ao sich die Produkte zur Erzeugung eines beständigen Schaumes, ferner auch als Textilhilfsprodukte, wie z. B. als Emulgierungs-, Wasch- und Reinigungsmittel, insbesondere für die tierische Faser.ao the products for the production of a permanent foam, also as textile auxiliary products, such as B. as emulsifying agents, detergents and cleaning agents, especially for animal fibers.

chlorids und Heptadecylamin unter Rühren ι Stunde auf 150 bis i8o°. Das Reaktionsprodukt stellt eine fast farblose wachsartige Masse dar, die sich in Wasser löst. An Stelle des Diäthylaminoäthylchlorids kann man auch die entsprechende Dimethylverbindung oder andere Alkylchloride verwenden, welche basische Gruppen enthalten. An Stelle des Heptadecylamins können dessen am Stickstoff monoalkylsubstituierte Derivate Anwendung finden.chloride and heptadecylamine with stirring for ι hour to 150 to 180 °. The reaction product is an almost colorless, waxy mass that dissolves in water. Instead of diethylaminoethyl chloride you can also use the corresponding dimethyl compound or other alkyl chlorides, which contain basic groups. Instead of the heptadecylamine, its monoalkyl-substituted on the nitrogen can be used Derivatives are used.

Claims (1)

Patentanspruch :Claim: Verfahren zur Darstellung von Derivaten hochmolekularer aliphatischer Amine, dadurch gekennzeichnet, daß man primäre oder sekundäre aliphatische Amine oder ein Gemisch von ihnen, \velche wenigstens einen Kohlenstoffrest mit mehr als 8 Kohlenstoffatomen enthalten, mit Alkylhalogeniden der allgemeinen FormelProcess for the preparation of derivatives of high molecular weight aliphatic Amines, characterized in that primary or secondary aliphatic Amines, or a mixture of them, should have at least one carbon residue containing more than 8 carbon atoms, with alkyl halides of the general formula X-R1-N^XR 1 -N ^ worin X ein Halogen ist und R1, R2 und R3 gleiche oder verschiedenartige aliphatische Reste bedeuten, umsetzt.in which X is a halogen and R 1 , R 2 and R 3 are identical or different aliphatic radicals. Beispielexample Man erhitzt äquimolekulare Mengen des salzsauren Salzes des Diäthylaminoäthyl-Equimolecular amounts of the hydrochloric acid salt of diethylaminoethyl- *) Von dem Patentsucher sind als die Erfinder angegeben worden:*) The patent seeker indicated the following as the inventors: Dr. Winfrid Hentrich in Erlangen, Dr. Karl Ott in Leverkusen und Dr. Heribert Schüßler in Köln-Deuts.Dr. Winfrid Hentrich in Erlangen, Dr. Karl Ott in Leverkusen and Dr. Heribert Schüßler in Cologne-Deuts. BERLIN. GEDBUCKT IN DER REICHSDBUCKERElBERLIN. PRINTED IN THE REICHSDBUCKEREl
DE1930547987D 1930-05-07 1930-05-07 Process for the preparation of derivatives of high molecular weight aliphatic amines Expired DE547987C (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE547987T 1930-05-07

Publications (1)

Publication Number Publication Date
DE547987C true DE547987C (en) 1932-04-01

Family

ID=6561771

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1930547987D Expired DE547987C (en) 1930-05-07 1930-05-07 Process for the preparation of derivatives of high molecular weight aliphatic amines

Country Status (2)

Country Link
DE (1) DE547987C (en)
FR (1) FR714029A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2742504A (en) * 1953-03-23 1956-04-17 Nepera Chemical Co Inc Heptadecyl amine compound
DE1024977B (en) * 1953-02-25 1958-02-27 Nepera Chemical Co Inc Process for the production of tertiary diamines
US2908714A (en) * 1956-09-20 1959-10-13 Ciba Pharm Prod Inc Process for the preparation of a diamine
US3079436A (en) * 1955-11-25 1963-02-26 Rohm & Haas Bis-quaternary ammonium compounds

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1024977B (en) * 1953-02-25 1958-02-27 Nepera Chemical Co Inc Process for the production of tertiary diamines
US2742504A (en) * 1953-03-23 1956-04-17 Nepera Chemical Co Inc Heptadecyl amine compound
US3079436A (en) * 1955-11-25 1963-02-26 Rohm & Haas Bis-quaternary ammonium compounds
US2908714A (en) * 1956-09-20 1959-10-13 Ciba Pharm Prod Inc Process for the preparation of a diamine

Also Published As

Publication number Publication date
FR714029A (en) 1931-11-06

Similar Documents

Publication Publication Date Title
DE547987C (en) Process for the preparation of derivatives of high molecular weight aliphatic amines
DE2004154A1 (en) Lubricating or fuel oil
DE1300291B (en) Process for the production of high molecular weight, water-soluble organosiloxane copolymers
DE223695C (en)
DE977288C (en) Process for the production of solid, non-ionized surfactants
DE552268C (en) Process for the preparation of higher molecular oxyalkylamines
DE505928C (en) Process for making an engine fuel
AT165059B (en) Process for the preparation of new water-soluble, higher molecular weight acyl biguanides
DE1050543B (en) Process for the production of basic color-leveling and dispersing polyglycol ethers
EP0076471B1 (en) Stabilisation of polyether or polyester moulding compounds against premature reaction
DE664309C (en) Process for the preparation of amides of higher molecular weight carboxylic acids
DE676049C (en) Process for the preparation of monourethanes of the alkylenediamines
DE763310C (en) Process for the production of quaternary ammonium compounds
DE801991C (en) Process for the preparation of carboxylic ester sulfonic acids
DE258393C (en)
DE521035C (en) Process for the preparation of quaternary ammonium salts suitable as wetting agents, foaming agents, dispersing agents and emulsifying agents
DE639079C (en) Wetting and cleaning agents
DE637670C (en) Process for the production of quaternary ammonium compounds from cyclic amidines not substituted on nitrogen
DE551257C (en) Process for the preparation of aminosulfonic acids
DE741891C (en) Process for the preparation of water-soluble nitrogen-containing condensation products
DE844450C (en) Process for the production of higher molecular weight nitrogenous primary or secondary phosphoric acid esters
DE623906C (en) Process for improving mercerising liquors
DE907298C (en) Process for the preparation of compounds with an analgesic effect
DE646932C (en) Process for the production of diamino alcohols of the fatty aromatic series
DE639508C (en) Process for the stabilization of carbamic acid chloride or its alkyl substitution products