DE3123064C2 - - Google Patents

Info

Publication number
DE3123064C2
DE3123064C2 DE19813123064 DE3123064A DE3123064C2 DE 3123064 C2 DE3123064 C2 DE 3123064C2 DE 19813123064 DE19813123064 DE 19813123064 DE 3123064 A DE3123064 A DE 3123064A DE 3123064 C2 DE3123064 C2 DE 3123064C2
Authority
DE
Germany
Prior art keywords
mill
chemisorption
chemisorbent
steam jet
hydrated lime
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE19813123064
Other languages
German (de)
Other versions
DE3123064A1 (en
Inventor
Heinz Dipl.-Ing. 4390 Gladbeck De Hoelter
Heinz Ing.(Grad.) 4600 Dortmund De Gresch
Heinrich Ing.(Grad.) Igelbuescher
Heribert Ing.(Grad.) 4390 Gladbeck De Dewert
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to DE19813123064 priority Critical patent/DE3123064A1/en
Publication of DE3123064A1 publication Critical patent/DE3123064A1/en
Application granted granted Critical
Publication of DE3123064C2 publication Critical patent/DE3123064C2/de
Granted legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Treating Waste Gases (AREA)
  • Gas Separation By Absorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Description

Die Erfindung betrifft ein Verfahren zur besseren Nutzung von Chemisorptionsmitteln in Chemisorptions­ anlagen, bei dem das anteilmäßig rückgeführte Chemi­ sorptionsmittel durch eine Mühle zerkleinert wird.The invention relates to a method for better Use of chemisorbents in chemisorbents plants in which the proportionally recycled Chemi sorbent is crushed by a grinder.

Eine solche Rückführung ist aus der DD-Z.: "Chem. Techn.", 19. Jg., Heft 9, September 1967, Seiten 553 bis 556, in der Weise bekannt, daß das vom Emittenten kommende Rauch- bzw. Abgas einer Luftstrommühle zuge­ führt wird. Kalkstein gelangt aus dem Vorratssilo über einen Zuteiler ebenfalls in die Mühle, wird zerkleinert und gelangt in innigen Kontakt mit der gasförmigen Phase. Ein Teil des nach Durchlauf eines Sichters und eines Zyklons vom Ventilator zum nachgeschalteten Staubfilter strömenden Gases wird zum Mühleneintritt und -austritt zurückgeführt. Gleichermaßen werden die im Sichter von der Luft­ strommühle kommenden Grieße in die Mühle zurück­ transportiert, während das Feinmehl in die Zyklone weitergefördert wird. Die Luftstrommühle dient da­ bei als Kalkstein-Mahltrocknungsanlage. Such a return is from the DD-Z .: "Chem. Techn. ", 19th vol., Issue 9, September 1967, pages 553 to 556, known in such a way that the issuer Coming smoke or exhaust gas from an airflow mill leads. Limestone comes out of the storage silo into the mill via an allocator crushed and comes into intimate contact with the gaseous phase. Part of the after run a classifier and a cyclone from the fan to the downstream dust filter of flowing gas is returned to the mill inlet and outlet. Likewise, those in the classifier are from the air stream mill coming greetings back into the mill transported while the fine flour is in the cyclones is promoted. The airflow mill serves there at as a limestone mill drying plant.  

Ferner ist aus der DE-OS 29 36 839 ein Verfahren zur Reinigung von Wasser mit Aktivkohle bekannt, bei dem die mit den Verunreinigungen beladene Ak­ tivkohle von einem wasserdampfhaltigen Gas mit einer Temperatur von etwa 750°C durchströmt und auf diese Weise regeneriert wird.Furthermore, from DE-OS 29 36 839 is a method known for cleaning water with activated carbon, where the Ak loaded with the impurities activated carbon from a gas containing water vapor Temperature of about 750 ° C flows through and on this Way is regenerated.

Es ist Aufgabe der vorliegenden Erfindung, ein Ver­ fahren anzugeben, bei dem die eingesetzten Chemi­ sorptionsmittel besser genutzt werden können.It is an object of the present invention to provide a ver drive to indicate where the Chemi sorbent can be used better.

Zur Lösung dieser Aufgabe wird vorgeschlagen, daß das Chemisorptionsmittel in einer Dampf­ strahlmühle aufgemahlen und gleichzeitig befeuchtet wird.To solve this problem, it is proposed that the chemisorbent in a steam jet mill ground and moistened at the same time becomes.

Das Chemisorptionsmittel, das bereits einmal den Chemisorptionsreaktor oder die Chemisorptionskon­ taktstrecke und den Chemisorptionsfilter durch­ laufen hat, besteht z. B. aus Kalkhydrat und soll mechanisch oder pneumatisch zu der Chemisorptions­ kontaktstrecke zurückgefördert werden. Allerdings reicht eine Rückführung ohne Behandlung des Chemi­ sorptionsmittels nicht aus, da dieses bereits an der Oberfläche mit SO2, HCl, HF und zum Teil auch mit CO2 reagiert hat und inaktiv ist. Jedoch ist der Innenkern des Chemisorptionsmittels noch aktiv und kann erfindungsgemäß dadurch nutzbar gemacht werden, daß es mittels einer Dampfstrahlmühle auf­ gemahlen und gleichzeitig durch den expandierenden Dampf befeuchtet wird. Hierdurch ergibt sich The chemisorbent, which has already run through the chemisorption reactor or the Chemisorptionskon contact route and the chemisorption filter, consists, for. B. from hydrated lime and should be mechanically or pneumatically conveyed back to the chemisorption contact section. However, recycling without treatment of the chemi sorbent is not sufficient, since it has already reacted on the surface with SO 2 , HCl, HF and partly also with CO 2 and is inactive. However, the inner core of the chemisorbent is still active and can be used according to the invention in that it is ground by means of a steam jet mill and at the same time moistened by the expanding steam. This results in

  • a) eine neue Oberfläche durch den Dampfstrahlprall- und Mahleffekt unda) a new surface due to the steam jet impact and grinding effect and
  • b) durch das Befeuchten der neugebildeten Oberfläche ein erhöhter Nutzungsgrad.b) by moistening the newly formed surface an increased degree of utilization.

Insgesamt kann durch Anwendung des erfindungsge­ mäßen Verfahrens der Chemisorptionsmittelverbrauch wesentlich gesenkt werden, da das Chemisorptions­ mittel in der Regel zwei- und mehrfach stöchiome­ trisch zur Summe aller Schadstoffe in die Trocken­ chemisorptionsstufe aufgegeben werden kann.Overall, by using the fiction method of chemisorbent consumption can be significantly reduced since the chemisorption usually two or more stoichiomas to the sum of all pollutants in the dry chemisorption can be abandoned.

In der Zeichnung ist das erfindungsgemäße Verfahren dargestellt, es werden bezeichnet
mit (1) die Kontaktstrecke, in der das Chemisorptions­ mittel, z. B. Kalkhydrat, mit dem Rohgas, das mit HCl, HF, SO2, CO2 und weiteren Schad­ stoffen z. B. angereichert ist, kontaktiert wird;
mit (2) das Chemisorptionsfilter;
mit (3) die Kalkhydratrückführung in die Kontakt­ strecke durch Zwischenschalten einer Dampf­ strahlmühle (4);
mit (5) das Einführen von frischem Kalkhydrat in die Chemisorptionsstrecke;
mit (6) Teilmengenabführung aus dem rückläufigen, bereits reagierten Kalkhydrat;
mit (7) die Dampfzuführung;
mit (8) der Rohgaseintritt;
mit (9) der Reingasaustritt;
mit (10) der Eintrag des reaktivierten Kalks.
In the drawing, the method according to the invention is shown, it will be referred to
with ( 1 ) the contact distance in which the chemisorption medium, for. As hydrated lime, with the raw gas containing substances such as HCl, HF, SO 2 , CO 2 and other harmful substances. B. is enriched, is contacted;
with ( 2 ) the chemisorption filter;
with ( 3 ) the hydrated lime return into the contact section by interposing a steam jet mill ( 4 );
with ( 5 ) introducing fresh hydrated lime into the chemisorption line;
with ( 6 ) partial discharge from the declining, already reacted hydrated lime;
with ( 7 ) the steam supply;
with ( 8 ) the raw gas inlet;
with ( 9 ) the clean gas outlet;
with ( 10 ) the entry of the reactivated lime.

Claims (1)

Verfahren zur besseren Nutzung von Chemisorptions­ mitteln in Chemisorptionsanlagen, bei dem das an­ teilmäßig rückgeführte Chemisorptionsmittel durch eine Mühle zerkleinert wird, dadurch gekennzeichnet, daß das Chemisorptionsmittel in einer Dampf­ strahlmühle aufgemahlen und gleichzeitig befeuchtet wird.Process for better use of chemisorbents in chemisorption systems, in which the partially recycled chemisorbent is crushed by a mill, characterized in that the chemisorbent is ground in a steam jet mill and simultaneously moistened.
DE19813123064 1981-06-11 1981-06-11 "Method for improved utilisation of chemisorbents in gas purification plants" Granted DE3123064A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE19813123064 DE3123064A1 (en) 1981-06-11 1981-06-11 "Method for improved utilisation of chemisorbents in gas purification plants"

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19813123064 DE3123064A1 (en) 1981-06-11 1981-06-11 "Method for improved utilisation of chemisorbents in gas purification plants"

Publications (2)

Publication Number Publication Date
DE3123064A1 DE3123064A1 (en) 1983-01-05
DE3123064C2 true DE3123064C2 (en) 1990-02-22

Family

ID=6134388

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19813123064 Granted DE3123064A1 (en) 1981-06-11 1981-06-11 "Method for improved utilisation of chemisorbents in gas purification plants"

Country Status (1)

Country Link
DE (1) DE3123064A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4101439A1 (en) * 1990-01-18 1991-08-01 Mitsubishi Heavy Ind Ltd Combustion gas desulphurisation within furnace - followed by wet desulphurisation of off-gas

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH671523A5 (en) * 1985-03-13 1989-09-15 Von Roll Ag
BR9713138A (en) * 1996-11-25 2000-02-08 Armstrong Medical Limited Carbon dioxide absorber for use in anesthesiology, and its preparation process.

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2936839A1 (en) * 1979-09-12 1981-04-16 CEAG Verfahrenstechnik GmbH, 4714 Selm Water-purification with active carbon - regenerated in solid bed by passage of hot steam-contg. gas

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4101439A1 (en) * 1990-01-18 1991-08-01 Mitsubishi Heavy Ind Ltd Combustion gas desulphurisation within furnace - followed by wet desulphurisation of off-gas

Also Published As

Publication number Publication date
DE3123064A1 (en) 1983-01-05

Similar Documents

Publication Publication Date Title
US4590049A (en) Method for dry desulfurization of exhaust gas
US4613487A (en) Flue gas desulfurization process
US6303083B1 (en) Method and system for SO2 and SO3 control by dry sorbent/reagent injection and wet scrubbing
US4604269A (en) Flue gas desulfurization process
KR890000512B1 (en) Process for removal of nitrogen oxides and sulfur oxides from waste gases
US4645652A (en) Method for scrubbing sulfur oxides and nitrogen oxides in a flue gas duct
SE8203933D0 (en) PROCEDURES AND DEVICES FOR GAS PURIFICATION CONTAINING SOLID AND GAS POLLUTANTS
US5965095A (en) Flue gas humidification and alkaline sorbent injection for improving vapor phase selenium removal efficiency across wet flue gas desulfurization systems
US4026992A (en) Method for removing nitrogen oxides from combustion exhaust gases
US4600568A (en) Flue gas desulfurization process
US4670238A (en) Recycled sorbent flue gas desulfurization
DE3123064C2 (en)
US5820831A (en) Method and apparatus for preparing calcium carbonate for scrubbing sulfur oxides from combustion effluents
DE3526857C2 (en)
US5817283A (en) Method for removing sulfur dioxide and nitrogen oxides from combustion gases
US5112588A (en) Method of and apparatus for the removal of gaseous contaminants from flue gas or reduction of the content of gaseous contaminants in a flue gas
JPS6136969B2 (en)
DE3235020C2 (en)
DE69403638T2 (en) METHOD AND DEVICE FOR PURIFYING EXHAUST GAS
CH642866A5 (en) METHOD FOR REMOVING POLLUTANTS, ESPECIALLY ACID COMPONENTS, FROM EXHAUST GAS.
DE3225716C1 (en) Process for flue gas desulphurisation
JPH08131764A (en) Wet type exhaust gas treatment method and apparatus
EP0226863A1 (en) Method for scrubbing sulfur oxides and nitrogen oxides in a flue gas duct
DE3313522C2 (en)
EP0292012A1 (en) Process for reducing the ammonia content of the dust particles set free by combustion plants, and apparatus for carrying out the process

Legal Events

Date Code Title Description
8101 Request for examination as to novelty
8105 Search report available
8105 Search report available
8110 Request for examination paragraph 44
D2 Grant after examination
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee