DE2701054C3 - Procedure for the determination of defects in materials with high ultrasound scattering - Google Patents

Procedure for the determination of defects in materials with high ultrasound scattering

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Publication number
DE2701054C3
DE2701054C3 DE2701054A DE2701054A DE2701054C3 DE 2701054 C3 DE2701054 C3 DE 2701054C3 DE 2701054 A DE2701054 A DE 2701054A DE 2701054 A DE2701054 A DE 2701054A DE 2701054 C3 DE2701054 C3 DE 2701054C3
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Germany
Prior art keywords
defects
determination
procedure
materials
frequency
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Expired
Application number
DE2701054A
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German (de)
Other versions
DE2701054B2 (en
DE2701054A1 (en
Inventor
Klaus Dr.Rer.Nat. 6600 Saarbruecken Goebbels
Siegfried Dipl.-Ing. 6605 Friedrichsthal Kraus
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Fraunhofer Gesellschaft zur Forderung der Angewandten Forschung eV
Original Assignee
Fraunhofer Gesellschaft zur Forderung der Angewandten Forschung eV
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Priority to DE2701054A priority Critical patent/DE2701054C3/en
Priority to AU33908/78A priority patent/AU515483B2/en
Publication of DE2701054A1 publication Critical patent/DE2701054A1/en
Publication of DE2701054B2 publication Critical patent/DE2701054B2/en
Application granted granted Critical
Publication of DE2701054C3 publication Critical patent/DE2701054C3/en
Expired legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00Use of ingredients characterised by shape
    • C08K7/22Expanded, porous or hollow particles
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F299/00Macromolecular compounds obtained by interreacting polymers involving only carbon-to-carbon unsaturated bond reactions, in the absence of non-macromolecular monomers
    • C08F299/02Macromolecular compounds obtained by interreacting polymers involving only carbon-to-carbon unsaturated bond reactions, in the absence of non-macromolecular monomers from unsaturated polycondensates
    • C08F299/04Macromolecular compounds obtained by interreacting polymers involving only carbon-to-carbon unsaturated bond reactions, in the absence of non-macromolecular monomers from unsaturated polycondensates from polyesters
    • C08F299/0442Catalysts
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/04Analysing solids
    • G01N29/11Analysing solids by measuring attenuation of acoustic waves
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/22Details, e.g. general constructional or apparatus details
    • G01N29/26Arrangements for orientation or scanning by relative movement of the head and the sensor
    • G01N29/27Arrangements for orientation or scanning by relative movement of the head and the sensor by moving the material relative to a stationary sensor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/34Generating the ultrasonic, sonic or infrasonic waves, e.g. electronic circuits specially adapted therefor
    • G01N29/348Generating the ultrasonic, sonic or infrasonic waves, e.g. electronic circuits specially adapted therefor with frequency characteristics, e.g. single frequency signals, chirp signals
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/01Indexing codes associated with the measuring variable
    • G01N2291/011Velocity or travel time
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/04Wave modes and trajectories
    • G01N2291/044Internal reflections (echoes), e.g. on walls or defects
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/10Number of transducers
    • G01N2291/102Number of transducers one emitter, one receiver
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/249921Web or sheet containing structurally defined element or component
    • Y10T428/249994Composite having a component wherein a constituent is liquid or is contained within preformed walls [e.g., impregnant-filled, previously void containing component, etc.]
    • Y10T428/249995Constituent is in liquid form
    • Y10T428/249997Encapsulated liquid

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Acoustics & Sound (AREA)
  • Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)

Description

Die Erfindung betrifft ein Verfahren gemäß dem Oberbegriff des Anspruchs. Die zunehmende Anwendung austenitischer Werkstoffe, insbesondere solcher höherer Wandstärken, wirft bei der Ultraschall-Fehlerprüfung große Probleme auf. Die Nutzanzeigen sind von Streuanzeigen aus dem Gefüge begleitet Die Amplituden dieser Interferenzstruktur können, je nach Größe des zu detektierenden Fehlers, die Amplitude des Nutzsignals erreichen oder gar übersteigen.The invention relates to a method according to the preamble of the claim. The increasing application Austenitic materials, especially those of higher wall thicknesses, throw up in the ultrasonic flaw test big problems. The useful displays are accompanied by scatter displays from the structure The amplitudes this interference structure can, depending on the size of the error to be detected, the amplitude of the Reach or even exceed the useful signal.

Inn Verlauf früherer Untersuchungen wurde versucht, das Nutzsignal mit Hilfe von Methoden der Nachrichtentechnik gegenüber dem StreuuntergruH anzuheben. Dies sind die Korrelation und die inverse Filterung. Bei der Korrelation kann ein bekanntes Nutzsignal gegenüber einem weißen Rauschen angehoben werden, bei der inversen Filterung werden sich zeitlich überlagernde Signale nach Ankunftszeit und Amplitude getrenntIn the course of previous investigations it was attempted to increase the useful signal with the help of communication technology methods compared to the scattered background. These are the correlation and the inverse filtering. A known useful signal are increased compared to white noise, with inverse filtering it is time-dependent overlapping signals separated according to arrival time and amplitude

Beide Verfahren lieferten keinen wesentlichen Erfolg, da das Gefügerauschen ein kohärentes Rauschen ist, d. h. den gleichen Frequenzinhalt wie das Nutzsignal hatBoth methods did not provide any significant success because the structural noise is a coherent noise, d. H. has the same frequency content as the useful signal

Ultraschall-StreuungUltrasonic scattering

Gibt man einen Ultraschall-Impuls in eine metallische Probe, so wird die Energie der Welle mit zunehmendem Laufweg durch Absorption und Streuung verbraucht. Im vom Schallstrahl erfaßten Gefügebereich werden die Kristallite zu Schwingungen angeregt die einander überlagern und sich nach allen Seiten ausbreiten. Die gestreute Energie kann somit auch vom sendenden Prüfkopf als Funktion der Zeit empfangen werden.If you put an ultrasonic pulse into a metallic sample, the energy of the wave increases with Path used up by absorption and scattering. In the structural area covered by the sound beam, the Crystallites stimulated to vibrations that overlap and spread out in all directions. the Scattered energy can thus also be received by the sending probe as a function of time.

Die bei der Gefügebestimmung mittels Ultraschall-Streuung übliche Meßanordnung und den allgemeinen Verlauf der gewonnenen Kurven ist in DE-PS 25 11 750 beschrieben.The measurement setup and the general ones that are customary when determining the structure by means of ultrasonic scattering The course of the curves obtained is in DE-PS 25 11 750 described.

MeBaufbauMeasurement structure

Die zur Durchführung der Messungen benutzten Apparaturen sind in F i g. I und 2 als Blockschaltbild-Dia dargestellt. Fig. 1 zeigt den allgemeinen Grundaufbau. Die Sende-Empfangseinheit mit dem Prüfkopf PK ist über eine Impedanzanpassung mit demThe apparatuses used to carry out the measurements are shown in FIG. I and 2 shown as a block diagram slide. Fig. 1 shows the general basic structure. The transceiver unit with the test head PK is via an impedance matching with the

Datenverarbeitungssystem verbunden. Die Analogsignale werden in einem AD-Wandler ADC mit maximal 100 MHz Wandelrate digitalisiert und in einem Mittelwertrechner aufsummiertData processing system connected. The analog signals are digitized in an AD converter ADC with a maximum conversion rate of 100 MHz and added up in an average value computer

Das resultierende Signal kann in der digitalisierten Form auf Lochstreifen gebracht oder über eine Teletype ausgelesen werden. Weiterhin besteht die Möglichkeit, das Signal nochmals analog abzugreifen und über einen X-Y-Schreiber darzustellen oder, nach erneutem Digitalisieren, im angeschlossenen Rechner zu verarbeiten.The resulting signal can be digitized in the Form can be put on punched tape or read out via a teletype. Furthermore there is the possibility to pick up the signal again in analog form and to display it using an X-Y recorder or, after digitizing again, to be processed in the connected computer.

Bei der Ortsmittlung wird ein Ultraschallimpulsgerät mit Analogausgängen für das Signal in Hochrrequenz- und gleichgerichteter Darstellung benutzt Die Probe wird hierbei unter dem Prüfkopf über einen Schrittmotor-gesteuerten Schlitten bewegtIn the case of location averaging, an ultrasonic pulse device with analog outputs for the signal in high-frequency The sample is used under the test head via a stepper motor-controlled Slide moves

Bei der Frequenzmittelung wird in einem Frequenzgenerator eine Sinusspannung erzeugt, deren Frequenz im angegliederten Wobbler in vorwählbaren Schrittweiten um die eingestellte Mittenfrequenz variiert wird. Ober den nachgeschalteten Burstgenerator, Leistungsverstärker und Prüfkopf gelangt der Ultraschall-Impuls in die Probe, die in diesem Falle fixiert ist Von dem Empfangsverstärker werden die Signale in das oben skizzierte Datenverarbeitungssystems eingespeistThe frequency averaging is done in a frequency generator a sinusoidal voltage is generated, the frequency of which in the attached wobbler in preselectable steps is varied by the set center frequency. Above the downstream burst generator, power amplifier and probe, the ultrasonic pulse reaches the sample, which in this case is fixed by the Receiving amplifiers are fed the signals into the data processing system outlined above

Bestimmen der VersuchsbedingungenDetermine the experimental conditions

Ein zentrales Problem stellt die Wahl der geeigneten Versuchsparameter dar. Bei der Ortsmittelung muß die Prüfkopfposition über dem interessierenden Reflektor variiert werden; bei der Frequenzmittelung hingegen ist die Anregungsfrequenz um die Mittenfrequenz geeignet zu verändern.A central problem is the choice of suitable test parameters. When averaging the location, the Probe position can be varied over the reflector of interest; in the case of frequency averaging, however, is to change the excitation frequency to suit the center frequency.

Die Parameter — Höhe Ar des Hubes, Ay des Winkels bzw. Breite Afae.% Frequenzintervalls — können aus den entsprechenden Echodynamikkurven gewonnen werden (F i g. 3).The parameters - height Ar of the stroke, Ay of the angle or width Afae.% Frequency interval - can be obtained from the corresponding echo dynamics curves (FIG. 3).

Aufgetragen ist der Nutzsignalabfall in Abhängigkeit von der Prüfkopfposition relativ zur Fehlermitte bzw. der Anregungsfrequenz bzw. vom Einschallwinkel.The useful signal drop is plotted as a function of the probe position relative to the center of the error or the excitation frequency or the angle of incidence.

Betrachtet man die möglichen Oszillationsbreiten, z. B. bei 6 dB Abfall, so ist zusätzlich die Abhängigkeit der Hubhöhe von der Fehlertiefe zu beachten. Wie durch die Schallfeldstruktur vorgegeben, ist die Hubhöhe für die geringere Fehlertiefe kleiner als für den Fehler größerer Tiefenlage.If one considers the possible ranges of oscillation, e.g. B. at 6 dB drop, there is also the dependency the height of lift from the depth of the defect. As given by the sound field structure, the Lifting height for the shallower defect depth is smaller than for the defect of greater depth.

Ganz analog sind die Zusammenhänge bei der Frequenzmittelung. Hier kommt als zusätzlicher Parameter noch die Breite des Anregungsimpulses hinzu; mit zunehmender Pulsbreite werden die Dynamikkurven immer enger.The relationships in frequency averaging are very similar. Here comes as an additional parameter add the width of the excitation pulse; with increasing pulse width, the dynamic curves getting closer.

MessungenMeasurements

Der Darstellung der Meßergebnisse bei der Ortsmittelung zeigt Fig.4 für das Prüfen grobkörniger austenitischer Werkstoffe.The representation of the measurement results for the location averaging is shown in Fig. 4 for the testing of coarse grains austenitic materials.

Die nur durch Aufsummieren der Interferenzmuster bei zwei verschiedenen Prüfkopfpositionen ermittelte Kurve ist noch identisch mit der ersten Displayanzeige. Ein vierfaches Aufsummieren zeigt auch noch keine wesentlichen Verbesserungen. Geht man jedoch zu 32facher oder 64facher Summation über, so ist die Rückwandechofolge bereits bis zum 4. Echo deutlich darstellbar.Which was only determined by adding up the interference patterns at two different probe positions The curve is still identical to the first display. A fourfold addition does not show any either significant improvements. However, if one goes over to 32-fold or 64-fold summation, this is Back wall echo sequence can already be clearly displayed up to the 4th echo.

Hierzu 4 Blatt ZeichnungenFor this purpose 4 sheets of drawings

Claims (1)

Patentanspruch:Claim: 27 Ol 05427 Ol 054 Verfahren zur Fehlerermittlung in Werkstoffen mit hoher Ultraschall-Streuung mittels Messung der Schalldruckamplitude in Abhängigkeit von der Laufzeit der Schallwellen in der Probe und Verbesserung des Signals-Gefügerauschverhältnisses, dadurch gekennzeichnet, daß das Interferenzmuster des kohärenten Streuuntergrundes durch örtliche Änderung und/oder Einschallwinkeländerung des Schallgebers und/oder Änderung der Einschallfrequenz geändert wird und die einander entsprechenden Werte der laufzeitabhängigen Schalldruckamplituden von mindestens zwei der so geänderten Interferenzmuster summiert werden.Procedure for the determination of defects in materials with high ultrasound scattering by measuring the Sound pressure amplitude as a function of the travel time of the sound waves in the sample and Improvement of the signal-structure-noise ratio, characterized in that the Interference pattern of the coherent scattering background due to local changes and / or changes in the angle of incidence of the sounder and / or change of the sound frequency is changed and the corresponding values of the propagation time-dependent sound pressure amplitudes of at least two of the interference pattern changed in this way are summed up.
DE2701054A 1977-01-12 1977-01-12 Procedure for the determination of defects in materials with high ultrasound scattering Expired DE2701054C3 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
DE2701054A DE2701054C3 (en) 1977-01-12 1977-01-12 Procedure for the determination of defects in materials with high ultrasound scattering
AU33908/78A AU515483B2 (en) 1977-01-12 1978-03-07 Latent curing system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2701054A DE2701054C3 (en) 1977-01-12 1977-01-12 Procedure for the determination of defects in materials with high ultrasound scattering

Publications (3)

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DE2701054A1 DE2701054A1 (en) 1978-07-13
DE2701054B2 DE2701054B2 (en) 1979-04-05
DE2701054C3 true DE2701054C3 (en) 1979-12-06

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DE (1) DE2701054C3 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3331468A1 (en) * 1983-08-29 1985-03-07 Mannesmann AG, 4000 Düsseldorf METHOD FOR DESTRUCTION-FREE TESTING WITH GUIDED SHAFTS
AU672353B3 (en) * 1996-01-15 1996-09-26 Budd Company, The Adhesive bonding apparatus and method using non-compressible beads
DE102009047318A1 (en) * 2009-05-15 2010-11-18 Intelligendt Systems & Services Gmbh Apparatus and method for ultrasound examination

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DE2701054B2 (en) 1979-04-05
AU3390878A (en) 1979-09-13
DE2701054A1 (en) 1978-07-13
AU515483B2 (en) 1981-04-09

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