DE1907672A1 - Rotating anode for X-ray tubes - Google Patents
Rotating anode for X-ray tubesInfo
- Publication number
- DE1907672A1 DE1907672A1 DE19691907672 DE1907672A DE1907672A1 DE 1907672 A1 DE1907672 A1 DE 1907672A1 DE 19691907672 DE19691907672 DE 19691907672 DE 1907672 A DE1907672 A DE 1907672A DE 1907672 A1 DE1907672 A1 DE 1907672A1
- Authority
- DE
- Germany
- Prior art keywords
- tungsten
- ray tubes
- rotating anode
- rhenium
- graphite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J35/00—X-ray tubes
- H01J35/02—Details
- H01J35/04—Electrodes ; Mutual position thereof; Constructional adaptations therefor
- H01J35/08—Anodes; Anti cathodes
- H01J35/10—Rotary anodes; Arrangements for rotating anodes; Cooling rotary anodes
- H01J35/108—Substrates for and bonding of emissive target, e.g. composite structures
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J2235/00—X-ray tubes
- H01J2235/08—Targets (anodes) and X-ray converters
- H01J2235/083—Bonding or fixing with the support or substrate
- H01J2235/084—Target-substrate interlayers or structures, e.g. to control or prevent diffusion or improve adhesion
Description
Dipl.-Ing. ' " ;·..-- .Dipl.-Ing. '"; · ..--.
.... Augsburg, den 13» Februar I969Augsburg, February 13, 1969
Po.tf.A242 1907672 A 3228/68 .Po.tf. A242 1907672 A 3228/68.
5290/16 Th/Sch5290/16 Th / Sch
- PATENTANMELDUNG- PATENT APPLICATION
Metallwerk Plansee AG, Reutte/Tirol,Metallwerk Plansee AG, Reutte / Tyrol,
; Ö STERRlS ICH-; Ö STERRlS I-
Drehanode für RöntgenröhrenRotating anode for X-ray tubes
Ais Werkstoff für Anoden von Röntgenröhren hat »ich wegen öeiner hohen Dichte, seiner hohenAis material for anodes of X-ray tubes I have because of its high density, its high
. Ordnungszahl im Periodensystem und nicht zuletzt ' wegen seines hohen Schmelzpunktes-■ Wolfram hervorragend bewährt. Die guten Eigenschaften des Wolframs, für diesen Zweck konnten durch1 Zusätze von anderen hochachmelzenden Metallen mit höher Dichte und hohen OrdnungSlahlen, wie Rhenium* Osmium, Iridium usw., "teilweise noch verbessert werden. Man hat auch gefundön, daß es für Röntgenröhren mit Drehanöden keines-, wegs notwendig .ist, die Anoden durchgehend aus Wolfram oder einer Wolframlegierxing herzustellen; es bietet. Ordinal number in the periodic table and not least because of its high melting point ■ tungsten has proven to be excellent. The good properties of tungsten, for this purpose could by 1 additions of other hochachmelzenden metals with higher density and high OrdnungSlahlen such as rhenium * osmium, iridium, etc., "partially improved. It has also gefundön that for X-ray tubes with Drehanöden It is by no means necessary to manufacture the anodes entirely from tungsten or a tungsten alloy; it offers
K4,sogar erhebliche Vorteile, für den Grundkörper der ( Drehanode einen Werkstoff mit geringem spez. Gewicht ; zu verwenden und lediglich an den AuftreffstellenK 4 , even considerable advantages, for the base body of the (rotating anode a material with a low specific weight; to be used and only at the points of impact
, '( für die Elektronen Auflagen aus Wolfram bzw. einer-., '(for the electron pads made of tungsten or a-.
' Wolframlegierung vorzusehen. - '■ ·. 'Provide tungsten alloy. - '■ ·.
Als Werkstoff für den Grundköfper hat »ich bis- ] her Molybdän gut bewährt. Versuchet den Grundkörper , ; aus Graphit herzuetelleü, stießen zunächst auf die VSchwierigkeit, daß <!er Graphit iait den.aufgebrachten ..- Wolframs chi eh te κ reagiert * wobei · spröde Zwischen-As a material for the basic body, “I have [] so far, molybdenum has proven its worth. Attempts t the base body; made from graphite, initially encountered the difficulty that <! he graphite reacts with the applied ..- tungsten chi eh te κ * whereby brittle intermediate
echichtan; »ntstahen.. Ss hat sich niiii gaeeigt« daß die,echichtan; "Ntstahen .. Ss has niiii admitted" that the
8Q3.8i6VQ5iJ4 . ; ^Kyü·. 8Q3.8i6VQ5iJ4. ; ^ Kyü ·.
529O/I6 Th/Sch - 2 - 13« Februar I969 j529O / I6 Th / Sch - 2 - 13 «February I969 j
Bildung dieser spröden. Zwischenschichten stark verzögert wird, wenn auf einen Graphit-Grundkörper&±n& ; > Auflage aus einer Wolfram-Rhenium-Legierung angeord- ; net wird, weil der ßhsmlufiSBuaats di· Kayteidbilduag - ) erschwert» Um diese Anoden hoch weiter zu verbessern, wurde gemäß einem noch nicht veröffentlichtem Vorschlag die Anweisung gegeben, zwischen dem Graphitkörper und V der aufgebrachten Wolfram-Rhenium-Legierung »Pch eine Zwischenschicht aus unlegiertem Rhenium abzuordnene Eine derartige Zwischenschicht würde die Diffusion des Kohlenstoffes'aus dem Graphit in die aus einer ' Wolfram-Rhenium-Legierung bestehenden Auflage praktisch ■ vollkommen unterdrücken. Ea hat sich nun gezeigt, daß die Anordnung einer Zwischenschicht aus Rhenium auf einem Grundkörper aus Graphit sich auch dann ausgezeichnet bewährt, wenn die an den Auftreffstellen für die Elektronen vorgesehen® Auflage nicht aus einer Wolfram-Rhenium-Legierung, sondern aus reinem Wolfram oder Wolframlegierungen, die z.B. Osmium odsr Iridium enthalten, besteht. Diese Erkenntnisse bilden die Grundlage für die vorliegende Erfindung,Formation of these brittle. Interlayers is greatly retarded when & ± n & ; > Support made of a tungsten-rhenium alloy arranged; net is because the ßhsmlufiSBuaats di · Kayteidbilduag - ) made more difficult »In order to further improve these anodes, according to a proposal that has not yet been published, the instruction was given to create an intermediate layer between the graphite body and the applied tungsten-rhenium alloy» P ch seconded unalloyed rhenium e such an intermediate layer would completely suppress the graphite practically ■ in the group consisting of a 'tungsten-rhenium alloy support the diffusion of the Kohlenstoffes'aus. It has now been shown that the arrangement of an intermediate layer made of rhenium on a base body made of graphite is also extremely effective when the support provided at the point of impact for the electrons is not made of a tungsten-rhenium alloy, but of pure tungsten or tungsten alloys that contain, for example, osmium or iridium. These findings form the basis for the present invention,
Die Erfindung betrifft eine Drehanode mit einem , Grundkörper aus Graphit und einer Auflage aus Wolfram bzw« einer Wolframlegierung. Die Erfindung besteht darin, daß zwischen dem Grundkörper aus Graphit und ·.The invention relates to a rotating anode with a, Base body made of graphite and a support made of tungsten or a tungsten alloy. The invention consists in that between the base body made of graphite and ·.
^%,der aus Wolfram oder einer Wolframlegierung becrtehenV"; . den Auflage eine Zwischenschicht aus Rhenium arigsprd-.-.^% of tungsten or a tungsten alloy because of "; . the support an intermediate layer of rhenium arigsprd -.-.
« net ist. Durch diese als Sperrschicht wirkende Zwi- . schenschicht wird eine Diffusion des Kohlenstoffes ·ν au.s dem Graphitkörper in die aus Wolfram oder einer : Wolframlegierung bestehende Auflage auch« dann yer- . hindert, trenn in dieser Rhenium nicht enthalten ist...;«Is not. Through this acting as a barrier layer between. layer becomes a diffusion of carbon · ν except for the graphite body in the one made of tungsten or one of: Tungsten alloy existing edition also «then yer-. prevents separating in this rhenium is not contained ...;
Zur Aufbringung der Rfcenium-ZwiaehansehichtFor the application of the Rfcenium-Zwiaehansehicht
und dar Wolfraa haltigen Auflage konnea an sich be- ■'·■'and the edition containing Wolfraa could actually be ■ '· ■'
5290/16 Th/Sch - 3 - / 13« Februar 19695290/16 Th / Sch - 3 - / 13 «February 1969
kannte Verfahren, wie elektrolytische Abscheidung, Aufspritzen mittels einer Plasmapistole oder Abscheidung aus der Gasphase, verwendet werden. An Hand' •in·· Au«führungsb*iepi·!·· wird di· Erfindung noch näher erläutert. Die in der Abbildung dargestellte Drehanode besteht aus einem scheibenförmig ausgebil- ' deten Grundkörper (1) aus Graphit, auf dem eine dünne Rheniumschicht (2) und darüber eine Wolframauflage (3) aufgebracht sind· Für die Wirksamkeit der Rhenium-Zwischenschicht ist bereits eine Stärke von wenigen Mikronen ausreichend, sodaß der Verbrauch ah Rhenium für die erfindungsgemäße Drehanode klein gehalten werden kann. Die Wolframauflage muß etwas stärker ■ ausgebildet sein und sie soll eine Mindeststärke von Q1I mm aufweisen. Ah Stelle von reinem Wolfram können auch Legierungen des Wolframs mit anderen hochschmelzenden Metallen, wie Osmium oder Iridium, verwendet · werden. . .Known methods such as electrolytic deposition, spraying using a plasma gun or deposition from the gas phase can be used. On hand '• ·· in Au "führungsb * IEPI ·! ·· di · invention will be explained in more detail. The rotating anode shown in the figure consists of a disk-shaped base body (1) made of graphite, on which a thin rhenium layer (2) and a tungsten layer (3) are applied.For the effectiveness of the rhenium intermediate layer is already a strength of a few microns is sufficient so that the consumption of rhenium for the rotary anode according to the invention can be kept small. The tungsten layer must be made somewhat thicker and it should have a minimum thickness of Q 1 mm. Instead of pure tungsten, alloys of tungsten with other refractory metals, such as osmium or iridium, can also be used. . .
" Die Herstellung der dargestellten Drehanode ■kann am einfachsten durch Abscheiden der .einzelnen Schien e aus der Gasphase vorgenommen werden. Geeignet hierau sind Fluoride und Halogenide der abzuscheidenden Metalle. Man kann dabei so vorgehen, daß zunächst durch thermische Zersetzung eines Gemisches von Wasserstoff und Rheiiiunr-Hexaf luorid die Rhenium-W^schicht und anschließend aus einem Gemisch aus Wasserstoff und Wolfram-Hexafluorid die Wolframschicht ab- . geschieden wird. Das .Aufbringen der beiden Schichten kann in einem einzigen Arbeitsprozeß vorgenommen wer* den, denn es muß bei der Abscheidung der verschiedenen Schichten-lediglich die Gaszusammensetzung geändert. . werden·The easiest way to manufacture the rotating anode shown is by depositing the individual Seemed to be made from the gas phase. Fluorides and halides of the to be deposited are suitable for this Metals. One can proceed in such a way that initially by thermal decomposition of a mixture of hydrogen and rhenium-hexafluoride the rhenium-W ^ layer and then from a mixture of hydrogen and tungsten hexafluoride, the tungsten layer from. being divorced. The application of the two layers can be done in a single work process * den, because it must be used in the separation of the various Layers-only changed the gas composition. . will·
' ■ -■■■/"■ .■■'.. - 4 V 909846/0504 . '■ - ■■■ / "■. ■■' .. - 4 V 909846/0504.
- Patentansprüche- Claims
Claims (3)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT322868A AT281215B (en) | 1968-04-03 | 1968-04-03 | Rotating anode for X-ray tubes |
Publications (1)
Publication Number | Publication Date |
---|---|
DE1907672A1 true DE1907672A1 (en) | 1969-11-13 |
Family
ID=3547354
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE19691907672 Pending DE1907672A1 (en) | 1968-04-03 | 1969-02-15 | Rotating anode for X-ray tubes |
Country Status (5)
Country | Link |
---|---|
AT (1) | AT281215B (en) |
DE (1) | DE1907672A1 (en) |
FR (1) | FR2005418A1 (en) |
GB (1) | GB1247244A (en) |
NL (1) | NL6905038A (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3013441A1 (en) * | 1980-04-05 | 1981-10-08 | Philips Patentverwaltung Gmbh, 2000 Hamburg | ANODE PLATE FOR A TURNING ANODE TUBE AND METHOD FOR THE PRODUCTION THEREOF |
FR2625033A1 (en) * | 1987-12-22 | 1989-06-23 | Thomson Cgr | Method of manufacturing an anode for an X-ray tube and anode obtained by this method |
EP0323366A1 (en) * | 1987-12-30 | 1989-07-05 | General Electric Cgr S.A. | Manufacturing method of a rotating anode of an X-ray tube |
EP0513830A1 (en) * | 1991-05-17 | 1992-11-19 | Sumitomo Electric Industries, Limited | Rotary anode for X-ray tube and method for manufacturing the same |
DE102010041532A1 (en) * | 2010-09-28 | 2012-01-05 | Siemens Aktiengesellschaft | Composite component, has connector arranged between internal component and outer component, where inner component is connected with external component by thermal bonding process using connector |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4119879A (en) * | 1977-04-18 | 1978-10-10 | General Electric Company | Graphite disc assembly for a rotating x-ray anode tube |
AT376064B (en) * | 1982-02-18 | 1984-10-10 | Plansee Metallwerk | X-RAY TUBE ROTATING ANODE |
US5204891A (en) * | 1991-10-30 | 1993-04-20 | General Electric Company | Focal track structures for X-ray anodes and method of preparation thereof |
JP2014506377A (en) * | 2010-12-16 | 2014-03-13 | コーニンクレッカ フィリップス エヌ ヴェ | Anode disk device with high melting point interlayer and VPS focal track |
JP2013098168A (en) * | 2011-10-28 | 2013-05-20 | Gamc Biotec Development Co Ltd | Transmission type x-ray tube and reflection type x-ray tube |
-
1968
- 1968-04-03 AT AT322868A patent/AT281215B/en not_active IP Right Cessation
-
1969
- 1969-02-15 DE DE19691907672 patent/DE1907672A1/en active Pending
- 1969-02-27 GB GB1043969A patent/GB1247244A/en not_active Expired
- 1969-03-10 FR FR6906586A patent/FR2005418A1/fr not_active Withdrawn
- 1969-04-01 NL NL6905038A patent/NL6905038A/xx unknown
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3013441A1 (en) * | 1980-04-05 | 1981-10-08 | Philips Patentverwaltung Gmbh, 2000 Hamburg | ANODE PLATE FOR A TURNING ANODE TUBE AND METHOD FOR THE PRODUCTION THEREOF |
FR2625033A1 (en) * | 1987-12-22 | 1989-06-23 | Thomson Cgr | Method of manufacturing an anode for an X-ray tube and anode obtained by this method |
EP0323366A1 (en) * | 1987-12-30 | 1989-07-05 | General Electric Cgr S.A. | Manufacturing method of a rotating anode of an X-ray tube |
FR2625606A1 (en) * | 1987-12-30 | 1989-07-07 | Thomson Cgr | METHOD FOR MANUFACTURING ROTATING ANODE FOR X-RAY TUBE, AND ROTATING ANODE OBTAINED ACCORDING TO SAID METHOD |
EP0513830A1 (en) * | 1991-05-17 | 1992-11-19 | Sumitomo Electric Industries, Limited | Rotary anode for X-ray tube and method for manufacturing the same |
DE102010041532A1 (en) * | 2010-09-28 | 2012-01-05 | Siemens Aktiengesellschaft | Composite component, has connector arranged between internal component and outer component, where inner component is connected with external component by thermal bonding process using connector |
Also Published As
Publication number | Publication date |
---|---|
NL6905038A (en) | 1969-10-07 |
AT281215B (en) | 1970-05-11 |
GB1247244A (en) | 1971-09-22 |
FR2005418A1 (en) | 1969-12-12 |
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