DE1137548B - Process for the production of laminated safety glass - Google Patents

Process for the production of laminated safety glass

Info

Publication number
DE1137548B
DE1137548B DES69631A DES0069631A DE1137548B DE 1137548 B DE1137548 B DE 1137548B DE S69631 A DES69631 A DE S69631A DE S0069631 A DES0069631 A DE S0069631A DE 1137548 B DE1137548 B DE 1137548B
Authority
DE
Germany
Prior art keywords
laminated safety
production
glass plates
plates
safety glass
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DES69631A
Other languages
German (de)
Inventor
Henri Rhety
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhone Poulenc SA
Original Assignee
Rhone Poulenc SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhone Poulenc SA filed Critical Rhone Poulenc SA
Publication of DE1137548B publication Critical patent/DE1137548B/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/10Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/1055Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer
    • B32B17/10761Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer containing vinyl acetal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/08Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of cellulosic plastic substance or gelatin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/10Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/10009Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets
    • B32B17/10036Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets comprising two outer glass sheets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/10Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/10807Making laminated safety glass or glazing; Apparatus therefor
    • B32B17/10816Making laminated safety glass or glazing; Apparatus therefor by pressing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/10Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/10807Making laminated safety glass or glazing; Apparatus therefor
    • B32B17/10972Degassing during the lamination

Landscapes

  • Joining Of Glass To Other Materials (AREA)
  • Laminated Bodies (AREA)
  • Lining Or Joining Of Plastics Or The Like (AREA)

Description

DEUTSCHESGERMAN

PATENTAMTPATENT OFFICE

S69631X/39a3 S69631X / 39a 3

ANMELDETAG: 27. JULI 1960REGISTRATION DATE: JULY 27, 1960

BEKANNTMACHUNG
DER ANMELDUNG
UNDAUSGABE DER
AUSLEGESCHRIFT: 4. OKTOB E R 1962
NOTICE
THE REGISTRATION
AND ISSUE OF
EDITORIAL: OCTOBER 4, 1962

Es ist bereits ein Verfahren zur Herstellung von Verbundsicherheitsglas durch Trockenzusammenfügen in einem Autoklaven bekannt, bei welchem der am Rand durch Klemmen od. dgl. zusammengehaltene Verbund aus mindestens zwei Glasplatten und mindestens einer Zwischenfolie aus thermoplastischem Kunststoff zuerst einem Unterdruck oder Vakuum und danach einem Überdruck bei gleichzeitiger Erwärmung ausgesetzt wird.It is already a process for the production of laminated safety glass by dry joining Known in an autoclave in which the one held together at the edge by clamping or the like Composite of at least two glass plates and at least one intermediate film made of thermoplastic Plastic first a negative pressure or vacuum and then an overpressure at the same time Is exposed to heating.

Dieses Verfahren ist ausgezeichnet, wenn man für die Verbundsicherheitsgläser Glasplatten von üblicher Dicke, d. h. von 2 bis 2,5 mm verwendet. Nimmt man jedoch dünnere Glasplatten, von 1,5 mm oder weniger, so stellt man fest, daß die zwischen den Glasplatten und der dazwischenliegenden thermoplastischen Kunststoffolie eingeschlossene Luft bei der Erwärmungsstufe im Vakuum häufig den Bruch der Glasplatten bewirkt.This process is excellent if one is the usual glass plates for the laminated safety glass Thickness, d. H. from 2 to 2.5 mm used. However, if you use thinner glass plates, of 1.5 mm or less, it is found that the thermoplastic between the glass plates and the intervening Plastic film trapped air during the heating stage in the vacuum often causes the breakage of the glass plates causes.

Es wurde nun gefunden, daß man den Bruch der Glasplatten bei dem vorgenannten Verfahren dadurch verhindern kann, daß man erfindungsgemäß bei Verwendung von dünnen Glasplatten von einer Stärke von etwa 1,5 mm und weniger den Verbund durch die Klemmen zwischen zwei starren Platten, gegebenenfalls unter Zwischenlegen von Folien aus einem EIastomeren, hält. Unter diesen Bedingungen entweicht die Luft wie im Falle normal dicker Glasplatten durch die Ränder des Verbundes, ohne einen Bruch hervorzurufen. It has now been found that the breakage of the glass plates in the aforementioned method thereby can prevent you according to the invention when using thin glass plates of a thickness of about 1.5 mm and less the bond through the clamps between two rigid plates, if necessary with the interposition of foils made of an elastomer. Under these conditions escapes the air through the edges of the composite, as in the case of normal thick glass plates, without causing a break.

Weiterhin wurde gefunden, daß nach diesem Verfahren außerdem der Bruch der in den Verbunden verwendeten dünnen Glasplatten noch weiter vermieden wird, wenn man in weiterer Ausbildung der Erfindung den Verbund der Erhitzung im Autoklaven anfänglich unter atmosphärischem Druck und danach unter Überdruck unterwirft, ohne daß man irgendwann Vakuum in dem Behälter anwendet.Furthermore, it has been found that after this process, the breakage in the compounds used thin glass plates is avoided even further if one is in further training of the Invention of the combination of heating in the autoclave initially under atmospheric pressure and then subjected to positive pressure without ever applying vacuum to the container.

Als Platten verwendet man vorzugsweise Platten von glatter Oberfläche. Polierte Glasplatten von 2 mm oder mehr eignen sich sehr gut, doch kann man auch Metallplatten verwenden. Wenn die Platten nicht vollkommen glatt sind, schiebt man die Folien aus Kautschuk oder anderen Elastomeren ein, die jedoch bei den im Autoklaven angewendeten Temperaturen, d. h. in der Nähe von 140° C noch ausreichend stabil sein müssen.The plates used are preferably plates with a smooth surface. Polished glass plates of 2 mm or more are very suitable, but metal plates can also be used. If the panels aren't perfect are smooth, you push in the rubber or other elastomer sheets, which, however, are the temperatures used in the autoclave, d. H. still sufficiently stable in the vicinity of 140 ° C must be.

Die erfindungsgemäß erhaltenen dünnen Verbundsicherheitsgläser können auch für die Herstellung optischer Gläser verwendet werden.The thin laminated safety glasses obtained according to the invention can also be used for production optical glasses can be used.

Verfahren zur Herstellung
von Verbundsicherheitsglas
Method of manufacture
of laminated safety glass

Anmelder:Applicant:

Societe des Usines Chimiques Rhöne-Poulenc, ParisSociete des Usines Chimiques Rhone-Poulenc, Paris

Vertreter: Dr. F. Zumstein,Representative: Dr. F. Zumstein,

Dipl.-Chem. Dr. rer. nat. E. AssmannDipl.-Chem. Dr. rer. nat. E. Assmann

und Dipl.-Chem. Dr. R. Koenigsberger,and Dipl.-Chem. Dr. R. Koenigsberger,

Patentanwälte, München 2, Bräuhausstr. 4Patent Attorneys, Munich 2, Bräuhausstr. 4th

Beanspruchte Priorität:Claimed priority:

Frankreich vom 22. September 1959 und 19. Juli 1960
(Nr. 805 727 und Nr. 833 334)
France from September 22, 1959 and July 19, 1960
(No. 805 727 and No. 833 334)

Henri Rhety, Lyon, Rhone (Frankreich),
ist als Erfinder genannt worden
Henri Rhety, Lyon, Rhone (France),
has been named as the inventor

Claims (2)

PATENTANSPRÜCHE:PATENT CLAIMS: 1. Verfahren zur Herstellung von Verbundsicherheitsglas durch Trockenzusammenfügen von mindestens zwei Glasplatten und mindestens einer Zwischenfolie aus thermoplastischem Kunststoff, bei welchem der am Rand durch Klemmen od. dgl. zusammengehaltene Verbund in einem Autoklav zuerst einem niederen Druck, gegebenenfalls einem Unterdruck, und danach einem Überdruck bei gleichzeitiger Erwärmung ausgesetzt wird, dadurch gekennzeichnet, daß man bei Verwendung von dünnen Glasplatten von einer Stärke von etwa 1,5 mm und weniger den Verbund durch die Klemmen od. dgl. zwischen zwei starren Platten, gegebenenfalls unter Zwischenlegen von Folien aus einem Elastomeren, hält.1. A process for the production of laminated safety glass by dry joining at least two glass plates and at least one intermediate film made of thermoplastic material, in which the composite held together at the edge by clamping or the like is first subjected to a low pressure, possibly a negative pressure, and then an overpressure in an autoclave is exposed with simultaneous heating, characterized in that when using thin glass plates of a thickness of about 1.5 mm and less, the bond by the clamps or the like between two rigid plates, optionally with the interposition of foils made of an elastomer, holds. 2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, daß man den Verbund der Erhitzung im Autoklav anfänglich unter atmosphärischem Druck unterwirft.2. The method according to claim 1, characterized in that the composite of the heating initially subjected to atmospheric pressure in the autoclave. In Betracht gezogene Druckschriften:
Deutsche Auslegeschrift Nr. 1010 266.
Considered publications:
German interpretative document No. 1010 266.
DES69631A 1959-09-22 1960-07-27 Process for the production of laminated safety glass Pending DE1137548B (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR805727A FR1244958A (en) 1959-09-22 1959-09-22 Safety glass manufacturing process
FR833334A FR78116E (en) 1959-09-22 1960-07-19 Safety glass manufacturing process

Publications (1)

Publication Number Publication Date
DE1137548B true DE1137548B (en) 1962-10-04

Family

ID=26184419

Family Applications (1)

Application Number Title Priority Date Filing Date
DES69631A Pending DE1137548B (en) 1959-09-22 1960-07-27 Process for the production of laminated safety glass

Country Status (5)

Country Link
CH (1) CH363479A (en)
DE (1) DE1137548B (en)
FR (2) FR1244958A (en)
GB (1) GB908338A (en)
NL (2) NL122057C (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1755395B1 (en) * 1968-01-29 1975-02-27 Saint Gobain Windshield for automobiles
DE2640206A1 (en) * 1975-09-09 1977-03-24 Asahi Glass Co Ltd LAMINATED GLASS WINDSHIELD AND METHOD OF MANUFACTURING THE SAME

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0600022D0 (en) * 2006-01-03 2006-02-08 Pilkington Plc Glazings
EP2861542A1 (en) 2012-06-14 2015-04-22 Corning Incorporated Process for laminating thin glass laminates
CN109937139B (en) * 2017-10-18 2023-04-28 法国圣戈班玻璃厂 Improved alignment and joining method for preparing thin composite glass
CN113386445B (en) * 2021-06-16 2022-08-30 海南海玻工程玻璃有限公司 Device and method for processing laminated glass

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1010266B (en) * 1953-12-07 1957-06-13 Rhone Poulenc Sa Process for the production of multilayer glass

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1010266B (en) * 1953-12-07 1957-06-13 Rhone Poulenc Sa Process for the production of multilayer glass

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1755395B1 (en) * 1968-01-29 1975-02-27 Saint Gobain Windshield for automobiles
DE2640206A1 (en) * 1975-09-09 1977-03-24 Asahi Glass Co Ltd LAMINATED GLASS WINDSHIELD AND METHOD OF MANUFACTURING THE SAME

Also Published As

Publication number Publication date
GB908338A (en) 1962-10-17
FR78116E (en) 1962-06-08
NL255626A (en)
NL122057C (en)
CH363479A (en) 1962-07-31
FR1244958A (en) 1960-11-04

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