DE1061783B - Process for the preparation of 3-mercuri-2-methoxy-1-succinimido-propane derivatives - Google Patents
Process for the preparation of 3-mercuri-2-methoxy-1-succinimido-propane derivativesInfo
- Publication number
- DE1061783B DE1061783B DEA27904A DEA0027904A DE1061783B DE 1061783 B DE1061783 B DE 1061783B DE A27904 A DEA27904 A DE A27904A DE A0027904 A DEA0027904 A DE A0027904A DE 1061783 B DE1061783 B DE 1061783B
- Authority
- DE
- Germany
- Prior art keywords
- methoxy
- mercuri
- succinimido
- preparation
- propane derivatives
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims 2
- KDCGOANMDULRCW-UHFFFAOYSA-N 7H-purine Chemical compound N1=CNC2=NC=NC2=C1 KDCGOANMDULRCW-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- BRMYZIKAHFEUFJ-UHFFFAOYSA-L mercury diacetate Chemical compound CC(=O)O[Hg]OC(C)=O BRMYZIKAHFEUFJ-UHFFFAOYSA-L 0.000 description 2
- AXEUBXNTRJZUKG-UHFFFAOYSA-N 1-prop-2-enylpyrrolidine-2,5-dione Chemical compound C=CCN1C(=O)CCC1=O AXEUBXNTRJZUKG-UHFFFAOYSA-N 0.000 description 1
- QYZBCWXZSYTIOY-UHFFFAOYSA-N Mercuric oxide Chemical compound [O-2].[Hg+2] QYZBCWXZSYTIOY-UHFFFAOYSA-N 0.000 description 1
- 229960000583 acetic acid Drugs 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 229940101209 mercuric oxide Drugs 0.000 description 1
- UKWHYYKOEPRTIC-UHFFFAOYSA-N mercury(II) oxide Inorganic materials [Hg]=O UKWHYYKOEPRTIC-UHFFFAOYSA-N 0.000 description 1
- 150000003212 purines Chemical class 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D473/00—Heterocyclic compounds containing purine ring systems
- C07D473/02—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6
- C07D473/04—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms
- C07D473/06—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms with radicals containing only hydrogen and carbon atoms, attached in position 1 or 3
- C07D473/08—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms with radicals containing only hydrogen and carbon atoms, attached in position 1 or 3 with methyl radicals in positions 1 and 3, e.g. theophylline
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/10—Mercury compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Saccharide Compounds (AREA)
Description
in der X einen Säurerest darstellt oder die Gruppe -OH-HY, in der HY für ein Purin steht, durch Umsetzung von N-Allylsuccinimid mit Mercuriacetat in methanolischer Lösung und gegebenenfalls Behandlung des erhaltenen 3-Acetoxymercuri-2-methoxy-1-succinimidopropans mit Salzen oder Säuren oder Umsetzung mit Purinen gemäß Patentanmeldung A24939IVb/12p, (deutsche Auslegeschrift 1057117), dadurch gekennzeichnet, daß man das Mercuriacetat in der Reaktionsmischung aus Mercurioxyd und Eisessig herstellt.in which X represents an acid residue or the group -OH-HY in which HY stands for a purine through Reaction of N-allylsuccinimide with mercuric acetate in methanolic solution and, if necessary, treatment of the obtained 3-acetoxymercuri-2-methoxy-1-succinimidopropane with salts or acids or reaction with purines according to patent application A24939IVb / 12p, (German Auslegeschrift 1057117), characterized in that the mercuric acetate in the reaction mixture of mercuric oxide and Produces glacial acetic acid.
Claims (1)
^-CH2-CH-CH2- HgXOCH 3
^ -CH 2 -CH-CH 2 - HgX
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DK782050X | 1955-08-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1061783B true DE1061783B (en) | 1959-07-23 |
Family
ID=8152765
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEA24939A Pending DE1057117B (en) | 1955-08-22 | 1956-05-19 | Process for the preparation of 3-mercuri-2-methoxy-1-succinimido-propane derivatives |
| DEA27904A Pending DE1061783B (en) | 1955-08-22 | 1957-09-13 | Process for the preparation of 3-mercuri-2-methoxy-1-succinimido-propane derivatives |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEA24939A Pending DE1057117B (en) | 1955-08-22 | 1956-05-19 | Process for the preparation of 3-mercuri-2-methoxy-1-succinimido-propane derivatives |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US2860136A (en) |
| DE (2) | DE1057117B (en) |
| FR (1) | FR1175419A (en) |
| GB (1) | GB782050A (en) |
| NL (2) | NL95180C (en) |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2635982A (en) * | 1951-01-18 | 1953-04-21 | Lakeside Lab Inc | Mercurated allylurea derivatives and diuretics containing the same |
-
0
- NL NL209589D patent/NL209589A/xx unknown
- NL NL95180D patent/NL95180C/xx active
-
1956
- 1956-04-27 US US580985A patent/US2860136A/en not_active Expired - Lifetime
- 1956-05-15 GB GB15134/56A patent/GB782050A/en not_active Expired
- 1956-05-19 DE DEA24939A patent/DE1057117B/en active Pending
- 1956-08-22 FR FR1175419D patent/FR1175419A/en not_active Expired
-
1957
- 1957-09-13 DE DEA27904A patent/DE1061783B/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| NL95180C (en) | 1900-01-01 |
| FR1175419A (en) | 1959-03-26 |
| NL209589A (en) | 1900-01-01 |
| DE1057117B (en) | 1959-05-14 |
| US2860136A (en) | 1958-11-11 |
| GB782050A (en) | 1957-08-28 |
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