DD255053A3 - DEVICE FOR ELECTROLYTIC TREATMENT OF METAL SAMPLES FOR ELECTRONIC MICROSCOPES - Google Patents

DEVICE FOR ELECTROLYTIC TREATMENT OF METAL SAMPLES FOR ELECTRONIC MICROSCOPES Download PDF

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Publication number
DD255053A3
DD255053A3 DD26778084A DD26778084A DD255053A3 DD 255053 A3 DD255053 A3 DD 255053A3 DD 26778084 A DD26778084 A DD 26778084A DD 26778084 A DD26778084 A DD 26778084A DD 255053 A3 DD255053 A3 DD 255053A3
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DD
German Democratic Republic
Prior art keywords
toka
otbepcthh
electrolytic treatment
metal samples
mhkpockonob
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DD26778084A
Other languages
German (de)
Inventor
Ivan I Cemeris
Vasilij Ja Ryzkov
Nikolaj I Korotkorucko
Vilen N Kaplicnyj
Valerij V Skorobogatko
Michail E Tyscuk
Original Assignee
Z Elektronnych Mikroskopov Im
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Priority claimed from SU833577963A external-priority patent/SU1131255A1/en
Application filed by Z Elektronnych Mikroskopov Im filed Critical Z Elektronnych Mikroskopov Im
Priority to DD26778084A priority Critical patent/DD255053A3/en
Publication of DD255053A3 publication Critical patent/DD255053A3/en

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Abstract

Die Erfindung bezieht sich auf die elektrochemische Bearbeitung von Metallen, auf die elektrochemische Verduennung von Proben, die im Durchstrahlungselektronenmikroskop untersucht werden. Die Vorrichtung enthaelt ein Gehaeuse 1 mit einer Aussparung fuer den Objekttraeger 4 und einer Duese 2, die mit der Pumpe 3 zum Pumpen des Elektrolyten verbunden ist, den Objekttraeger 4 mit der Probe 5, die positive Elektrode 6 in Form eines Bechers, der mit einer nichtstromleitenden Fluessigkeit gefuellt ist, dessen Boden die Probe 5 ist, die Elektrode 7, den Verstaerker 8, die Speisequelle 9 und die Schaltelemente 10 und 12. FigurThe invention relates to the electrochemical machining of metals, to the electrochemical dismutation of samples which are examined by transmission electron microscopy. The device contains a housing 1 with a recess for the slide 4 and a Duese 2, which is connected to the pump 3 for pumping the electrolyte, the slide 4 with the sample 5, the positive electrode 6 in the form of a cup, with a is filled with non-conductive liquid, the bottom of which is the sample 5, the electrode 7, the amplifier 8, the supply source 9 and the switching elements 10 and 12. FIG

Description

7-7-

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-A-oöpaeeq 5 η 3aMHKaeT 3JieKTpH*iecKyio ii;enb -A- oöpaeeq 5 η 3aMHKaeT 3JieKTpH * iecKyio ii; enb

IIHTaHHfl 9. Πο,ΕΙ £6HCTBHβΜ SJieKTpOXHMHUeCKOH nOJIHpOBKH θ6-IIHTaHHfl 9. Πο, ΕΙ £ 6HCTBHβΜ SJieKTpOXHMHUeKKOH nOJIHpOBKH θ6-

B ΜΟΜΘΗΤ 06pa30BaHHfl OTBepCTHHB ΜΟΜΘΗΤ 06pa30BaHHfl OTBepCTHH

nonagaioT β ΗβτοκοπροΒΟ,ΐΐΗΠίνίο jKH#KOCTb 3JieKTpo,na 6, npoBOiiHMocTb ijenn yilT 8 £0 cpaöaTHsaHHH KJiio^eBHX TOB IO n 12, OTKJiioyaiomHX sJieKTpo^BHraTejib II η 9. ΠρΗ 3Τ0Μ no^atia sjieKTpojiHTa β conjio a yepe3 oßpaeoBaBineecH oTBepcTHenonagaioT β ΗβτοκοπροΒΟ, ΐΐΗΠίνίο JKH # KOCTb 3JieKTpo, na 6, npoBOiiHMocTb ijenn yilT 8 £ 0 cpaöaTHsaHHH KJiio ^ eBHX TOB IO n 12, OTKJiioyaiomHX sJieKTpo ^ BHraTejib II η 9. ΠρΗ 3Τ0Μ no ^ atia sjieKTpojiHTa β conjio a yepe3 oßpaeoBaBineecH oTBepcTHe

npocatiHBaeTCH Ha oöpaTHy© CTopony oßpaeiia η pa3-ÖaBJifler OCTaBEiHHCH Ha ero noBepxHocTH aJieKTpojiHT, neu eTCH ero XHMHtiecKoe fle^cTBHe.npocatiHBaeTCH Ha oöpaTHy © CTopony oßpaeiia η pa3-ÖaBJifler OCTaBEiHHCH Ha ero noBepxHocTH aJieKTpojHT, a new eCHe Ero XHMHtiecKoe fle ^ cTBHe.

Hcn0JIb30BaHHe flaHHOrO yCTpOHCTBa n03B0JlHeT nOBHCHTb 06pa3Ii0B H CHH3HTb Tp^^OeMKOCTb HX HSrOTOBJieHHH SJieKTpOHHOMHKpOCKOIlHtieCKHX HCCJIe1IIOBaHHHX MeTaJIJIOB HHcn0JIb30BaHHe flaHHOrO yCTpOHCTBa n03B0JlHeT nOBHCHTb 06pa3Ii0B H CHH3HTb Tp ^^ OeMKOCTb HX HSrOTOBJieHHH SJieKTpOHHOMHKpOCKOIlHtieCKHX HCCJIe 1 IIOBaHHHX MeTaJIJIOB H

Ο,ΣΙΗΟδ H3 ΠρΗΜΗΗ, 3aTpy,EHHKaiiHX HCnOJIbSOBaHHe ΠρΟΟΒβ-SJieKTpOHHtIX MHKpOCKOnOB B ΜβΤθΛΠΟΒβ,ΙΙβΗΗΗ, HBJIH-eTCH Tp^flHOCTb npnrOTOBJieHHH H3 MaCCHBHbDC MaTepHSJIOB TOH-KHX o6pa3qOB, npo3patiHHx sJieKTpoHHOMy ji^tjy. QynjecTB^iomHe η onncaHHHe β JiHTepaT^pe ^CTponcTBa He odecnetiHBaioT CBoe-BpeMeHHoM OCTaHOBKH npoijecca sjieKTponojiHpoBKH, a BaTeJIbHO, H aBT0MaTH3Hp0BaHH0e nOJiyiieHHe Mcnojib3OBaHHe ,aaHHoro H3o6pereHHH πρκ paepa-Ο, ΣΙΗΟδ H3 ΠρΗΜΗΗ, 3aTpy, EHHKaiiHX HCnOJIbSOBaHHe ΠρΟΟΒβ-SJieKTpOHHtIX MHKpOCKOnOB B ΜβΤθΛΠΟΒβ, ΙΙβΗΗΗ, HBJIH etch Tp ^ flHOCTb npnrOTOBJieHHH H3 MaCCHBHbDC MaTepHSJIOB TOH KHX o6pa3qOB, npo3patiHHx sJieKTpoHHOMy ji ^ TJY. QynjecTB ^ iomHe η onncaHHHe β JiHTepaT ^ pe ^ CTponcTBa He odecnetiHBaioT CBOE BpeMeHHoM OCTaHOBKH npoijecca sjieKTponojiHpoBKH, a BaTeJIbHO, H aBT0MaTH3Hp0BaHH0e nOJiyiieHHe Mcnojib3OBaHHe, aaHHoro H3o6pereHHH πρκ paepa-

^ΤΟΗΧίβΗΗΗ MeTaJIJIHtieCKHX 0Öpa3U;0B n03B0JIHT BBfflOJIHHTb βΓΟ ÖOJiee npOCTHM H TeXHOJIOrHtiHfclM B H3r0T0BJie-HHH H ^1EOOHbIM B SKCÜJiyaTatiHH.^ ΤΟΗΧίβΗΗΗ MeTaJIJIHtieCKHX 0p0a3U; 0B n03B0JIHT BBfflOJIHHTb βΓΟ ÖOjiee npOCTHM H TeXHOJIOrHtiHfclM B H3r0T0BJie-HHH H ^ 1 EOOHbIM B SKCÜJiyaTatiHH.

3K0H0MHtieCKHii 3φφβΚΤ OT BHeflpeHHH COCTaBHT 140000 T.3K0H0MHtieCKHii 3φφβΚΤ OT BHeflpeHHH COCTaBHT 140000 T.

Ha 100 πρκοΌροΒ β γο,ε.Ha 100 πρκοΌροΒ β γο, ε.

ι -!ι -!

Claims (2)

ΦΟΡΜΑ ,HJIH 3JieKTp0JIHTHtieCK0ß O6pa6OTKH o6pa3i^oB ,aJifl ΘΛβκτροΗΗΗΧ MHKpocKonoB, co.liepstamee C ΓΗβ3,30Μ ,IiJlH ΟΟΈβΚΤΟ,ΙΙβρΑαΤβΛΗ, CHCTeMy qMpKyJIfl- ajieKTpojiHTa, hcto^hhk TOKa πολμροβκμ, ^cHJiHTejib TOKa Hatiajia o<5pa3OBaHHH oTBepcTHH, μ CMCTeMy ΘΛβκτρο^οΒ, OTJiHtiaiomeecH QTO, C IjeJIbiO nOBiimeHHfl KaxieCTBa OÖpaÖOTKH Π^ΤβΜ KpaeBbix βφφβκτοε, oho CHaömeHo KaMepoö c KpyiKocTbio, β κοτοροΜ iOTaHOBJieH sjieKTpo^, 3aKpenjieHHbiS β 0O1BeKTO1HepacaTene, η coüjiom ,jjjih no,natiH sjieKTpojinTa, pacnojioaceHHbiM c ^pyroü CTopoHH ο6τ>βκτο^βρκατβΛΗ, conjio coe^HHeHO c hctotjhhkom TOKa. HcTOiiHHKH ΜΗφορΜαΙίΜΗ, ΠρΗΗΗΤΗβ BO ΒΗΗΜβΉΗβ 3KcnepTH3e:ΦΟΡΜΑ, HJIH 3JieKTp0JIHTHtieCK0ß O6pa6OTKH o6pa3i ^ NE, aJifl ΘΛβκτροΗΗΗΧ MHKpocKonoB, co.liepstamee C ΓΗβ3,30Μ, IiJlH ΟΟΈβΚΤΟ, ΙΙβρΑαΤβΛΗ, CHCTeMy qMpKyJIfl- ajieKTpojiHTa, hcto ^ hhk Toka πολμροβκμ, ^ cHJiHTejib Toka Hatiajia o <5pa3OBaHHH oTBepcTHH, μ CMCTeMy ΘΛβκτρο ^ οΒ, OTJiHtiaiomeecH QTO, C IjeJIbiO nOBiimeHHfl KaxieCTBa OÖpaÖOTKH Π ^ ΤβΜ KpaeBbix βφφβκτοε, oho CHaömeHo KaMepoö c KpyiKocTbio, β κοτοροΜ iOTaHOBJieH sjieKTpo ^, 3aKpenjieHHbiS β 0O1BeKTO1HepacaTene, η coüjiom, jjjih no, natiH sjieKTpojinTa, pacnojioaceHHbiM c ^ pyroü CTopoHH ο6τ> βκτο ^ βρκατβΛΗ, conjio coe ^ HHeHO c hctotjhhkom TOKa. HcTOiiHHKH ΜΗφορΜαΙίΜΗ, ΠρΗΗΗΤΗβ BO ΒΗΗΜβΉΗβ 3KcnepTH3e: 1. SU ,A, 630306..1. SU, A, 630306 .. 2. J.M. Larson, R. Taggart, D.H. Polonis, - Rev Sei Instrument, 40, p.3_338, 1969.2. J.M. Larson, R. Taggart, D.H. Polonis, - Rev Sei Instrument, 40, p.3_338, 1969. U 3.U 3.
DD26778084A 1983-01-10 1984-09-26 DEVICE FOR ELECTROLYTIC TREATMENT OF METAL SAMPLES FOR ELECTRONIC MICROSCOPES DD255053A3 (en)

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SU833577963A SU1131255A1 (en) 1983-01-10 1983-01-10 Apparatus for electrolytic treatment of metal specimens for electron microscopes
DD26778084A DD255053A3 (en) 1983-01-10 1984-09-26 DEVICE FOR ELECTROLYTIC TREATMENT OF METAL SAMPLES FOR ELECTRONIC MICROSCOPES

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19529222C1 (en) * 1995-08-09 1997-04-03 Univ Dresden Tech Electrolytic prodn. of TEM specimen

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19529222C1 (en) * 1995-08-09 1997-04-03 Univ Dresden Tech Electrolytic prodn. of TEM specimen

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