CU21712A3 - PROCEDURE FOR THE PREPARATION OF UREA - Google Patents

PROCEDURE FOR THE PREPARATION OF UREA

Info

Publication number
CU21712A3
CU21712A3 CU36231A CU36231A CU21712A3 CU 21712 A3 CU21712 A3 CU 21712A3 CU 36231 A CU36231 A CU 36231A CU 36231 A CU36231 A CU 36231A CU 21712 A3 CU21712 A3 CU 21712A3
Authority
CU
Cuba
Prior art keywords
urea
solution
ammonia
carbon dioxide
concentrated
Prior art date
Application number
CU36231A
Other languages
Spanish (es)
Inventor
Kees Jonckers
Original Assignee
Unie Van Kunstmestfab Bv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unie Van Kunstmestfab Bv filed Critical Unie Van Kunstmestfab Bv
Priority to CU36231A priority Critical patent/CU21712A3/en
Publication of CU21712A3 publication Critical patent/CU21712A3/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Un procedimiento para preparar urea, en el que: en una zona de síntesis, a una presión de 125-350 bares y a la temperatura correspondiente a la zona, se forma una disolución de síntesis de urea que contiene carbamato y amoníaco libre, a partir de dióxido de carbono y un exceso de amoníaco; en una primera operación de descomposición, a presión de síntesis o inferior, una parte del carbamato se descompone por suministro de calor, y la fase gaseosa obtenida en este procedimiento se condensa en una primera zona de condensación; en una segunda operación de descomposición, a una presión de 4-40 bares, otra parte del carbamato aún presente se descompone por suministro de calor y se separa la fase gaseosa formada; en otra operación, el carbamato restante se separa en forma de una mezcla gaseosa que contiene amoníaco y dióxido de carbono, y esta mezcla gaseosa que contiene amoníaco y dióxido de carbono se trata para formar una disolución de amoníaco y dióxido de carbono en agua y la disolución restante que contiene urea se trata para formar una disolución concentrada de urea, caracterizada porque la disolución de urea a concentrar se introduce en los tubos de un cambiador de calor de carcasa y tubos, la mezcla gaseosa se la segunda operación de descomposición se introduce en el lado de la carcasa del cambiador de calor en el extremo opuesto al lugar en que se introduce la disolución de urea a concentrar, la disolución de amoníaco y dióxido de carbono, en un lugar de situado entre la entrada de la mezcla gaseosa y la entrada de la disolución de urea a concentrar, y el producto de concentración se descarga del lado de la carcasa en el extremo en que se introduce en los tubos la disolución de urea a concentrarA process for preparing urea, in which: in a synthesis zone, at a pressure of 125-350 bar and at the temperature corresponding to the zone, a urea synthesis solution containing carbamate and free ammonia is formed from carbon dioxide and excess ammonia; in a first decomposition operation, at synthesis pressure or lower, a part of the carbamate decomposes by supplying heat, and the gas phase obtained in this process is condensed in a first condensation zone; in a second decomposition operation, at a pressure of 4-40 bar, another part of the carbamate still present decomposes by supplying heat and the gas phase formed is separated; In another operation, the remaining carbamate is separated as a gaseous mixture containing ammonia and carbon dioxide, and this gaseous mixture containing ammonia and carbon dioxide is treated to form a solution of ammonia and carbon dioxide in water and the Remaining urea-containing solution is treated to form a concentrated urea solution, characterized in that the urea solution to be concentrated is introduced into the tubes of a shell and tube heat exchanger, the gas mixture in the second decomposition operation is introduced into the side of the heat exchanger housing at the end opposite the place where the urea solution to be concentrated, the ammonia and carbon dioxide solution, is introduced at a location between the gas mixture inlet and the inlet of the urea solution to be concentrated, and the concentration product is discharged from the side of the housing at the end where the d is introduced into the tubes urea solution to concentrate

CU36231A 1984-12-12 1984-12-12 PROCEDURE FOR THE PREPARATION OF UREA CU21712A3 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CU36231A CU21712A3 (en) 1984-12-12 1984-12-12 PROCEDURE FOR THE PREPARATION OF UREA

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CU36231A CU21712A3 (en) 1984-12-12 1984-12-12 PROCEDURE FOR THE PREPARATION OF UREA

Publications (1)

Publication Number Publication Date
CU21712A3 true CU21712A3 (en) 1991-07-15

Family

ID=47352129

Family Applications (1)

Application Number Title Priority Date Filing Date
CU36231A CU21712A3 (en) 1984-12-12 1984-12-12 PROCEDURE FOR THE PREPARATION OF UREA

Country Status (1)

Country Link
CU (1) CU21712A3 (en)

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