CN85108512A - Produce cocoa butter equivalent with centrifuging from oleum sapii (seed) - Google Patents
Produce cocoa butter equivalent with centrifuging from oleum sapii (seed) Download PDFInfo
- Publication number
- CN85108512A CN85108512A CN 85108512 CN85108512A CN85108512A CN 85108512 A CN85108512 A CN 85108512A CN 85108512 CN85108512 CN 85108512 CN 85108512 A CN85108512 A CN 85108512A CN 85108512 A CN85108512 A CN 85108512A
- Authority
- CN
- China
- Prior art keywords
- sherwood oil
- cocoa butter
- butter equivalent
- centrifugation
- raw material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Abstract
The invention belongs to the method for producing cocoa butter equivalent in the oil chemical technology field.Its main points are, are raw material with rough oleum sapii or Chinese tallow tree seed or refining oleum sapii, through heating and filtering, are dissolved in sherwood oil, and centrifugation is sloughed sherwood oil and obtained cocoa butter equivalent.The present invention compares with prior art, and it is wide to have raw material sources, and technology is simpler, and product yield higher (73-89%) thereby low cost and other advantages more help the peculiar and abundant vegetable oil resource of this China of development and utilization Chinese tallow tree seed.
Description
The invention belongs to the oil chemical technology field, the cocoa butter equivalent of producing is widely used in foodstuffs industry.
Along with growth in the living standard, people are increasing to the demand of theobroma oil.But the place of production scope of natural cocoa butter is little, yield poorly, the price height, can not satisfy the needs in market far away, therefore, produces the various methodologies of cocoa butter equivalent and just arises at the historic moment.
At present, the raw material of producing cocoa butter equivalent abroad has: plam oil, butter nut fat, two sieve fruit fat, mother-in-law sieve's fat, Semen Mangiferae indicae fat etc. mostly are the grease of tropical plants.What adopt on technology is that multistep crystallization and solvent branch are put forward the method for (for example United States Patent (USP) 3,944,585 " multistep crystallizations from Beeftallow, with various various combinations to obtain the grease of required specific physicochemical property ").In China, then utilize China's special product, resourceful oleum sapii (seed) produces cocoa butter equivalent for raw material.So far known method has fractional crystallization (Chinese patent authorization bulletin CN 85100005B " is the method that raw material is produced cocoa butter equivalent with oleum sapii (or seed) ") and solvent branch to carry (Chinese patent authorization bulletin CN 85100006B " is the method that raw material is produced cocoa butter equivalent with the oleum sapii ").Because producing cocoa butter equivalent from oleum sapii (or seed) still belongs to a kind of technology newly developed in China, so present fractional crystallization and solvent divide extracting method like also having weak point.At first, the raw material that this method is used is the purified oleum sapii, and the factory of the refining oleum sapii of China's production at present seldom; A large amount of is, and the workshop, rural area produces is rough oleum sapii (being used for doing cured candle in the past).Cost height so not only, complex process has also limited the extensive utilization to abundant Chinese tallow tree seed resource.Secondly, the product yield of these two kinds of methods is not high, only at 30-70%.
It is simple that the present invention is intended to seek a kind of technology, easy to operate, and product yield height can utilize oleum sapii (seed) resource to produce the method for cocoa butter equivalent widely.
Main points of the present invention are: (get cured layer through taking off with rough oleum sapii (raw product in workshop, rural area) or Chinese tallow tree seed, use petroleum ether extraction, extraction liquid) or refining oleum sapii be raw material, add sherwood oil, through centrifugation, take off sherwood oil (sherwood oil is recyclable to be used repeatedly) and produce cocoa butter equivalent.Technological process is looked the difference of raw material and different, and concrete grammar is as follows:
1. be raw material with rough oleum sapii.Raw material is heated to 100-150 ℃, cooling; Filter impurity elimination during to 60-90 ℃, filtrate is cooled off again; During to 35-45 ℃, add sherwood oil (the sherwood oil boiling point is 30-60 ℃), both proportionings are 1: 2-5; Carry out centrifugation when the mixed solution of filtrate and sherwood oil is cooled to 15-25 ℃, the controlled temperature when centrifugal is-4～5 ℃, and centrifugal force is 2300-4700g, and centrifugation time is 40-60 minute; After centrifugal, get supernatant liquor, promptly get cocoa butter equivalent through sloughing sherwood oil.
2. be raw material with the Chinese tallow tree seed.Raw material taken off get cured layer; Be 30-60 ℃ petroleum ether extraction then with boiling point, cured layer is 1 with the proportioning of sherwood oil: 7-10; Carry out centrifugation when extraction liquid is cooled to 15-25 ℃, the controlled temperature when centrifugal is-4～5 ℃, and centrifugal force is 2300-4700g, and centrifugation time is 40-60 minute; After centrifugal, get supernatant liquor, promptly get cocoa butter equivalent through sloughing sherwood oil.
3. be raw material with the purified oleum sapii.Raw material is heated to 35-45 ℃, add sherwood oil (the sherwood oil boiling point is 30-60 ℃), both proportionings are 1: 2-5, when being cooled to 15-25 ℃, the mixed solution of refining oleum sapii and sherwood oil carries out centrifugation, controlled temperature when centrifugal is-4～5 ℃, centrifugal force is 2300-4700g, and centrifugation time is 40-60 minute; After centrifugal, get supernatant liquor, promptly get cocoa butter equivalent through sloughing sherwood oil.
Compared with the prior art the present invention has the advantage that can utilize widely rich in natural resources: raw material need not made with extra care, and does not need alkali refining (the Chinese tallow tree seed raw material to some Special Circumstances will carry out alkali refining) substantially, need not decolour.In addition, technology of the present invention is simple, and is easy to operate, product yield height (73-89%).
The cocoa butter equivalent that the present invention produces is compared with other products, and its physicochemical constant relatively approaches natural cocoa butter.More helping HUMAN HEALTH (palmitic acid content is higher, and stearic acid content is lower) aspect the composition of lipid acid even than natural cocoa butter.Prove through toxicity test: harmless.Concrete comparative data is as follows:
1. physicochemical constant is relatively:
2. the lipid acid ratio of components is:
Claims (10)
1, a kind of preparation method of cocoa butter equivalent the invention is characterized in that with rough oleum sapii be raw material, is heated to 100-150 ℃, cooling; Filter impurity elimination during to 60-90 ℃; When being cooled to 35-45 ℃, filtrate adds sherwood oil (the sherwood oil boiling point is 30-60 ℃); When filtrate and sherwood oil mixed solution are cooled to 15-25 ℃, carry out centrifugation, get supernatant liquor, slough sherwood oil and promptly get cocoa butter equivalent.
2, preparation method according to claim 1, the proportioning that it is characterized in that filtrate and sherwood oil is 1: 2-5.
3, according to claim 1,2 described preparation methods, the controlled temperature when it is characterized in that centrifugation is-4～5 ℃, and centrifugal force is 2300-4700g, and centrifugation time is 40-60 minute.
4, a kind of preparation method of cocoa butter equivalent the invention is characterized in that with the Chinese tallow tree seed be raw material, sloughs cured layer, be 30-60 ℃ petroleum ether extraction then with boiling point, when extraction liquid is cooled to 15-25 ℃, carry out centrifugation, get supernatant liquor, slough sherwood oil and promptly get cocoa butter equivalent.
5, preparation method according to claim 4 is characterized in that the cured layer and the proportioning of sherwood oil are 1: 7-10.
6, according to claim 4,5 described preparation methods, the controlled temperature when it is characterized in that centrifugation is-4～5 ℃, and centrifugal force is 2300-4700g, and centrifugation time is 40-60 minute.
7, a kind of preparation method of cocoa butter equivalent, the invention is characterized in that with refining oleum sapii be raw material, be heated to 35-45 ℃, add sherwood oil (the sherwood oil boiling point is 30-60 ℃), when being cooled to 15-25 ℃, the mixed solution of refining oleum sapii and sherwood oil carries out centrifugation, get supernatant liquor, promptly get cocoa butter equivalent through sloughing sherwood oil.
8, preparation method according to claim 7 is characterized in that the proportioning of refining oleum sapii and sherwood oil is 1: 2-5.
9, according to claim 7,8 described preparation methods, the controlled temperature when it is characterized in that centrifugation is-4～5 ℃, and centrifugal force is 2300-4700g, and centrifugation time is 40-60 minute.
10, a kind of preparation method of cocoa butter equivalent the invention is characterized in that with oleum sapii (or seed) be raw material, through heating and melting, filters impurity elimination, is dissolved in chemical solvents, and centrifugation is sloughed chemical solvents and produced cocoa butter equivalent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN85108512A CN85108512B (en) | 1985-10-21 | 1985-10-21 | Preparation of cacao butter from stillingia sebifera seeds by centrifugation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN85108512A CN85108512B (en) | 1985-10-21 | 1985-10-21 | Preparation of cacao butter from stillingia sebifera seeds by centrifugation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN85108512A true CN85108512A (en) | 1987-04-29 |
| CN85108512B CN85108512B (en) | 1987-11-04 |
Family
ID=4796042
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN85108512A Expired CN85108512B (en) | 1985-10-21 | 1985-10-21 | Preparation of cacao butter from stillingia sebifera seeds by centrifugation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN85108512B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101433575B (en) * | 2007-11-13 | 2011-06-08 | 蒋爱芳 | Chinese sapium bark seed extract and preparation method thereof |
| CN102215696A (en) * | 2008-11-07 | 2011-10-12 | Cj第一制糖株式会社 | Cocoa butter equivalents produced by the enzymatic interesterification process and method for preparing the same |
-
1985
- 1985-10-21 CN CN85108512A patent/CN85108512B/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101433575B (en) * | 2007-11-13 | 2011-06-08 | 蒋爱芳 | Chinese sapium bark seed extract and preparation method thereof |
| CN102215696A (en) * | 2008-11-07 | 2011-10-12 | Cj第一制糖株式会社 | Cocoa butter equivalents produced by the enzymatic interesterification process and method for preparing the same |
Also Published As
| Publication number | Publication date |
|---|---|
| CN85108512B (en) | 1987-11-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA1060465A (en) | Production of edible liquid oils from palm oil and similar oils | |
| CN106117297B (en) | The preparation method of one plant sterols and sterol ester | |
| EP0081881B1 (en) | A process for the solvent fractionation of palm oil stearines and products obtained with said process | |
| US2293676A (en) | Method of separating fatty acids | |
| CN1898369B (en) | Method of dry fractionation of fat or oil | |
| CN1272872A (en) | Method for reducing saturated fatty acids from fatty acid compositions | |
| CN85108512A (en) | Produce cocoa butter equivalent with centrifuging from oleum sapii (seed) | |
| US2697113A (en) | Method of removing protein from fatty tissue | |
| CN102250488B (en) | Method for improving quality of capsanthin product | |
| CN105831370A (en) | Preparation method of cocoa butter equivalent | |
| CN104711112A (en) | Method for realization of combined production of high quality rice bran oil and ferulic acid from rice bran | |
| US2421157A (en) | Method of separating fatty acids | |
| CN1067688C (en) | Process and apparatus for producing pectine by pre-acidolysis and continuous high-acidity extraction | |
| JPH0687787B2 (en) | How to make salad oil | |
| US4920096A (en) | Method for extracting cedar wood oil | |
| CN1159929A (en) | Process for producing health Buthus martensi liquor | |
| CN1246317C (en) | Proanthocyan extraction process from rapeseed husk | |
| CN85100006A (en) | With oleum sapii (or seed) is the method that raw material is produced cocoa butter equivalent | |
| CN113943605B (en) | Winterization and fractionation method for microbial oil | |
| CN110627802A (en) | Method for extracting sesame lignan from by-product generated in sesame oil production | |
| ATE116989T1 (en) | METHOD FOR PURIFYING HEMIN, NEW HEMIN DERIVATIVE AND METHOD FOR PRODUCTION. | |
| CN85102662A (en) | From citrus peel, obtain through refining the method for pectin coproduction simultaneously wine, oil, sauce, pigment and orange peel glucoside | |
| CN1059847A (en) | A kind of method of extracting Chinese medicinal ingredients | |
| CN86104396A (en) | The preparation method of Chinese tallow tree fat and Chinese catalpa oil and purposes | |
| CN1021651C (en) | Processing of anise camphor with high freezing point |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| PB01 | Publication | ||
| C06 | Publication | ||
| C13 | Decision | ||
| GR02 | Examined patent application | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |