CN2654194Y - Mass transfer reinforced rotary bed over gravity machine - Google Patents

Mass transfer reinforced rotary bed over gravity machine Download PDF

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Publication number
CN2654194Y
CN2654194Y CN 03243973 CN03243973U CN2654194Y CN 2654194 Y CN2654194 Y CN 2654194Y CN 03243973 CN03243973 CN 03243973 CN 03243973 U CN03243973 U CN 03243973U CN 2654194 Y CN2654194 Y CN 2654194Y
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China
Prior art keywords
filler
mass transfer
packing layer
mass
ring
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Expired - Fee Related
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CN 03243973
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Chinese (zh)
Inventor
薛碧
王大权
薛海燕
薛雯潞
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Individual
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Abstract

The utility model relates to a high gravity rotating packed bed with intensified mass transfer, mainly comprising multi layers of concentric ring fillers on the rotating bed, and the filling layer and the middle of the filling layer have ring interspace. The utility model improves the efficiency of the mass transfer largely.

Description

Strengthen the rotating bed super gravity machine of mass transfer
The utility model is a kind of reaction and the hypergravity device that separates.
In recent years, the rotating bed super gravity technology has solved much insoluble problem under normal gravitational field, and mass-transfer efficiency has had large increase, still, present high-gravity technology, also some is unable to do what one wishes to some difficult problem.For example: use high gravity desulfurization, though than conventional method efficient large increase has been arranged, the unit desulfuration efficiency does not also reach national environmental standard, is there what way on existing high-gravity technology, further to improve mass-transfer efficiency greatly?
The purpose of this utility model will provide a kind of exactly, further strengthens the rotating bed super gravity machine of mass-transfer efficiency.
Of the present utility model being achieved through the following technical solutions:
In the hypergravity machine of sealing, be provided with rotatable packed bed, packed bed is provided with the ring-like filler of fixing multilayer concentric, be provided with ring-like space in the middle of packing layer and the packing layer, be provided with liquid distribution trough in the packing layer center cavity, liquid distribution trough links to each other with casing feed tube outward, the drop of liquid distribution trough spray, when striking the packing layer inner edge, under the shearing force effect of the filler that rotates at a high speed, be ground into minimum droplet, pull into film, thin silk, the huge phase contact area of this high speed conversion has greatly improved mass-transfer efficiency, and Here it is " entrance point effect ".In order to improve mass-transfer efficiency.We make one deck packing layer into two layers, three layers or more multi-layered.After drop is thrown away from nexine packing layer outer rim, when clashing into outer filler inner edge again, form new " entrance point effect " again, thereby further improve mass-transfer efficiency through interstice coverage.Liquid through the multi-layer efficient mass transfer under the action of the centrifugal at last, is thrown out of outer filler outer rim, falls from liquid outlet and discharges.Gas enters hypergravity machine from the air inlet on the housing, under pressure, enters filler by outer filler outer rim, through multilayer filler mass transfer, enters the packing layer center cavity at last, is discharged by exhaust outlet.
The utility model effect, this multilayer filler hypergravity machine because of having increased " end effect district ", therefore, has improved mass-transfer efficiency greatly, two layers, three layers filler, than stack pile simple layer filler, mass-transfer efficiency can improve more than the 50%-100%.
Below in conjunction with the accompanying drawing illustrated embodiment, the utility model is described further.
Fig. 1 is the utility model " the rotation hypergravity machine of reinforcement mass transfer " structure chart.
Fig. 2 is Fig. 1 D-D profile
Embodiment: as shown in Figure 1, this machine has and is provided with rotatable packed bed (5) in the seal casinghousing (2), filler divides A, B, three layers of C, be provided with fixing (6) in packed bed (5) center cavity, distributor (6) links to each other with feed tube (1), liquid sprays on filler (A) the layer inner edge through liquid distribution trough (6), under the super gravity field effect, through filler A, B, the C mass transfer throws away from filler (C) layer outer rim at last and falls, discharge by liquid outlet (9), gas enters filler (C) layer outer rim through air flue (3), through packing layer C under pressure then by air inlet (4), B, the A mass transfer, enter center cavity, discharge by gas outlet (10).(7) are line shafts among the figure, and (8) are sealed bearings.
See that Fig. 2 works as drop when spraying to filler (A) layer inner edge by liquid distribution trough (6), jet power and filler (A) be the tangential force of rotation generation at a high speed, make drop bump to such an extent that pulverize at the E of filler (A) point, the droplet of granular, the huge phase contact area of high speed conversion is provided, improved mass-transfer efficiency greatly, after tiny droplet enters filler (A) inner edge, because stopping of the irregular internal diameter of packing layer, under the cross shear effect of rotation at a high speed, small drop is drawn as film as thin as a wafer, silk, drip, this has further strengthened mass-transfer efficiency, but along with liquid enters going deep into of packing layer, liquid progressively is tending towards and filler (A) rotation synchronously, displacement slows down relatively, and alternate renewal interface reduces, and mass-transfer efficiency also reduces greatly, though Here it is filler " import petiolarea " why is very narrow reason place of really having concentrated whole packing layer mass-transfer efficiency 70%-80%! In order to improve mass-transfer efficiency, we can reach by increasing " end effect district ", and for this reason, we have the multilayer in space just passable in the middle of being divided under the situation that does not change the original thickness of filler.When drop after fill in material (A) outer rim E1 and throw away, during along tangent line bump filler (B) inner edge E2 point, because the tangential force that filler (B) rotates at a high speed and the direction of E1E2 power have a very mitre V, high-speed impact like this, can form a new point at E2 again and throw away a little, when clashing into filler (C) layer inner edge again through interstice coverage, again can be at the E4 point, create new " an end effect district ", thereby further strengthen mass-transfer efficiency.

Claims (1)

1, a kind of rotating bed super gravity machine of strengthening mass transfer, in the hypergravity machine of sealing, be provided with rotatable packed bed, packed bed is provided with the ring-like filler of fixing multilayer concentric, and the packing layer center cavity is provided with liquid distribution trough, and liquid distribution trough links to each other with feed tube, casing is provided with air inlet, gas outlet and liquid outlet is characterized in that: the rotary packed bed ring-like filler of fixing multilayer concentric that is provided with is provided with ring-like space in the middle of packing layer and the packing layer.
CN 03243973 2003-04-08 2003-04-08 Mass transfer reinforced rotary bed over gravity machine Expired - Fee Related CN2654194Y (en)

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Application Number Priority Date Filing Date Title
CN 03243973 CN2654194Y (en) 2003-04-08 2003-04-08 Mass transfer reinforced rotary bed over gravity machine

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Application Number Priority Date Filing Date Title
CN 03243973 CN2654194Y (en) 2003-04-08 2003-04-08 Mass transfer reinforced rotary bed over gravity machine

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CN2654194Y true CN2654194Y (en) 2004-11-10

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101254356B (en) * 2007-11-23 2010-12-22 浙江工业大学 Concentric ring adverse current type hypergravity swinging bed device
CN101940860A (en) * 2010-09-08 2011-01-12 国家海洋局天津海水淡化与综合利用研究所 Gas-liquid segregating unit
CN101254357B (en) * 2007-11-23 2011-05-25 浙江工业大学 Concentric ring adverse current type hypergravity swinging bed device
CN102258880A (en) * 2011-06-09 2011-11-30 北京化工大学 Supergravity rotating bed device adopting sectional type liquid feeding mode to strengthen rotor end effect
CN101549274B (en) * 2008-04-01 2011-12-21 北京化工大学 Supergravity revolving bed device and application in carbon dioxide collecting and purification process
WO2013143243A1 (en) * 2012-03-26 2013-10-03 北京化工大学 Hypergravity rotating packed bed catalytic reactor and application thereof for modulating distribution of fischer-tropsch process synthetic product
CN104368301A (en) * 2013-08-14 2015-02-25 中国石油化工股份有限公司 Hyper-gravity reactor and reaction method
CN104511235A (en) * 2013-09-29 2015-04-15 北京化工大学 Self-pressurized rotation filling bed apparatus with whole structured filler, and applications thereof
CN105148685A (en) * 2015-09-23 2015-12-16 中北大学 Constant-channel type rotating-packed-bed mass transferring and reacting device
CN108771959A (en) * 2018-07-06 2018-11-09 北京化工大学 It is a kind of based on the hypergravity atomising device of silk screen rotor and application
CN109661284A (en) * 2016-09-06 2019-04-19 西门子股份公司 Method and apparatus for carrying out the process for removing filler from the cavity being present in component
CN112337139A (en) * 2019-08-09 2021-02-09 北京化工大学 In-situ heat-supplementing supergravity devolatilization device and application
CN112337140A (en) * 2019-08-09 2021-02-09 北京化工大学 Method for removing volatile components in polymer by virtue of supergravity by supplementing heat energy in situ
CN113213620A (en) * 2021-03-01 2021-08-06 北京大学 Process for treating sewage by using supergravity reinforced activated sludge
CN113769684A (en) * 2021-08-24 2021-12-10 北京化工大学 Supergravity device for efficient coupling and strengthening in liquid-liquid heterogeneous reaction and product two-phase separation process
CN116407935A (en) * 2023-06-12 2023-07-11 中国科学院大学 Selective desulfurization method based on supergravity reactor

Cited By (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101254357B (en) * 2007-11-23 2011-05-25 浙江工业大学 Concentric ring adverse current type hypergravity swinging bed device
CN101254356B (en) * 2007-11-23 2010-12-22 浙江工业大学 Concentric ring adverse current type hypergravity swinging bed device
CN101549274B (en) * 2008-04-01 2011-12-21 北京化工大学 Supergravity revolving bed device and application in carbon dioxide collecting and purification process
CN101940860A (en) * 2010-09-08 2011-01-12 国家海洋局天津海水淡化与综合利用研究所 Gas-liquid segregating unit
CN101940860B (en) * 2010-09-08 2012-07-04 国家海洋局天津海水淡化与综合利用研究所 Gas-liquid segregating unit
CN102258880A (en) * 2011-06-09 2011-11-30 北京化工大学 Supergravity rotating bed device adopting sectional type liquid feeding mode to strengthen rotor end effect
CN102258880B (en) * 2011-06-09 2013-05-29 北京化工大学 Supergravity rotating bed device adopting sectional type liquid feeding mode to strengthen rotor end effect
WO2013143243A1 (en) * 2012-03-26 2013-10-03 北京化工大学 Hypergravity rotating packed bed catalytic reactor and application thereof for modulating distribution of fischer-tropsch process synthetic product
CN104368301B (en) * 2013-08-14 2016-08-17 中国石油化工股份有限公司 A kind of supergravity reactor and reaction method
CN104368301A (en) * 2013-08-14 2015-02-25 中国石油化工股份有限公司 Hyper-gravity reactor and reaction method
CN104511235A (en) * 2013-09-29 2015-04-15 北京化工大学 Self-pressurized rotation filling bed apparatus with whole structured filler, and applications thereof
CN105148685B (en) * 2015-09-23 2017-12-08 中北大学 The rotary packed bed mass transfer of constant channel formula and consersion unit
CN105148685A (en) * 2015-09-23 2015-12-16 中北大学 Constant-channel type rotating-packed-bed mass transferring and reacting device
CN109661284A (en) * 2016-09-06 2019-04-19 西门子股份公司 Method and apparatus for carrying out the process for removing filler from the cavity being present in component
CN109661284B (en) * 2016-09-06 2021-06-25 西门子股份公司 Method for removing a filling material from a cavity present in a component and device for carrying out the method
CN108771959A (en) * 2018-07-06 2018-11-09 北京化工大学 It is a kind of based on the hypergravity atomising device of silk screen rotor and application
CN112337139A (en) * 2019-08-09 2021-02-09 北京化工大学 In-situ heat-supplementing supergravity devolatilization device and application
CN112337140A (en) * 2019-08-09 2021-02-09 北京化工大学 Method for removing volatile components in polymer by virtue of supergravity by supplementing heat energy in situ
CN112337139B (en) * 2019-08-09 2022-04-19 北京化工大学 In-situ heat-supplementing supergravity devolatilization device and application
CN113213620A (en) * 2021-03-01 2021-08-06 北京大学 Process for treating sewage by using supergravity reinforced activated sludge
CN113769684A (en) * 2021-08-24 2021-12-10 北京化工大学 Supergravity device for efficient coupling and strengthening in liquid-liquid heterogeneous reaction and product two-phase separation process
CN116407935A (en) * 2023-06-12 2023-07-11 中国科学院大学 Selective desulfurization method based on supergravity reactor
CN116407935B (en) * 2023-06-12 2023-08-15 中国科学院大学 Selective desulfurization method based on supergravity reactor
US11952547B1 (en) 2023-06-12 2024-04-09 University Of Chinese Academy Of Sciences Selective desulfurization method implemented based on high gravity reactor

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