CN2649227Y - Metal uniform particle generator - Google Patents
Metal uniform particle generator Download PDFInfo
- Publication number
- CN2649227Y CN2649227Y CN 03258305 CN03258305U CN2649227Y CN 2649227 Y CN2649227 Y CN 2649227Y CN 03258305 CN03258305 CN 03258305 CN 03258305 U CN03258305 U CN 03258305U CN 2649227 Y CN2649227 Y CN 2649227Y
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- Prior art keywords
- crucible
- generator
- nozzle
- battery lead
- lead plate
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Abstract
A metal uniform particle generator consists of a quartz container, a crucible, a piezoelectric excitative generator, a thermocouple, a heating device, a gas-protected supplying pipe, a vibration generator, an electrode plate and a vessel with coolant. The piezoelectric excitative generator is arranged on top of the crucible; the vibration generator is arranged inside the lower part of the crucible; the thermocouple and the gas-protected supplying pipe are inserted respectively in the crucible; a nozzle is provided at the bottom of the crucible; the electrode plate is provided outside the lower part of the nozzle, wherein an opening is arranged, opposite to the electrode plate; potential difference is produced between the crucible and the electrode plate; the vessel with coolant is arranged right under the opening of the electrode plate; the devices above-mentioned are arranged in the vacuum quartz container. The advantages are that the utility model can produce uniform spherical particles of metal or alloy of a single size; the physical and chemical properties between particles are highly consistent and can be applied to the welding of integrated circuit and also improves the consistency of the electronic system therefore has a wide prospect of application.
Description
(1) field under:
The utility model belongs to a kind of device of producing the metal or alloy powder, particularly a kind of metal single-size generator.
(2) background technology:
At present, the method of the production metal or alloy powder (particle) of comparative maturity and extensive use on China's powder metallurgy industry is aerosolization, water atomization method, but metal or alloy powder (particle) size distribution that this method is prepared is inhomogeneous, each intergranular microstructure and physical and chemical performance have certain difference, use morely in traditional field such as surperficial anticorrosion with painting, but can not satisfy the application of high-tech sector.
(3) summary of the invention:
The purpose of this utility model is to design a kind of metal single-size generator, and it makes the problems referred to above be solved, and produces the metal or alloy powder of even particle size distribution, satisfies the needs that high-tech sector is used.
The technical solution of the utility model: a kind of metal single-size generator is characterized in that this device is made up of the container of quartz container, crucible, piezoelectric excitation generator, thermocouple, heater, protective gas feeding pipe, clapp oscillator, battery lead plate and interior dress cooling fluid; Said piezoelectric excitation generating apparatus is in crucible top oral area, the clapp oscillator that is connected with the piezoelectric excitation generator places bottom in the crucible, thermocouple and protective gas feeding pipe insert from top, crucible both sides respectively, heater places the crucible wall periphery, there is a micropore crucible bottom, nozzle is equipped with at the micropore place, battery lead plate places the outside below of crucible bottom nozzle, there is opening at battery lead plate and nozzle place relative crucible bottom parallel with crucible bottom, between crucible and battery lead plate potential difference is arranged, the container that cooling liquid is housed place the battery lead plate opening under; Said said apparatus places in the quartz container that vacuumizes.
The diameter of above-mentioned said crucible bottom nozzle is between 20-100 μ m.
Clapp oscillator can be that disk and rocking beam constitute in the above-mentioned said crucible, also can be other shapes that are beneficial to the liquid metals vibration.
The protective gas that the above-mentioned said protective gas feeding pipe that is inserted in the crucible provides can be nitrogen or other inert gas.
A certain amount of anti-oxidation high pure nitrogen or other inert gas also should be arranged in the above-mentioned said quartz container, and with crucible in gas have pressure difference.
The course of work of the present utility model and operation principle are: quartz container is vacuumized, charge into then to avoid high pure nitrogen or other inert gas of metal (alloy) oxidation, to be heated to the uniform temperature fusion in metal or the platform gold crucible and keep several minutes, input surpasses an atmospheric nitrogen or other inert gas in crucible then.The pressure difference of crucible and quartz container makes molten metal or alloy liquid spray from nozzle, forms cylindrical metal liquid stream, applies the higher-order of oscillation in this metal liquid, makes metal liquid be fractured into fine drop when ejection.The metal or alloy drop is when nozzle sprays, and charging electrode fills on drop and adds electric charge, because the skin effect of drop electric charge, makes between each drop mutually exclusively, avoids the polymerization in dropping process.When tiny molten drop falls, remove to collect the metal or alloy drop of these whereabouts with the container that cooling liquid is housed, then can obtain the metal or alloy single-size of single size.
Superiority of the present utility model is: the metal or alloy particle that 1, adopts metal single-size generator to produce, visible granular is the even spherical particle of single size under the light microscope, physics between the particle is consistent with the chemical property height, and is in full accord as each particle resistance value; 2, with this device fabrication welding material particle, can be applied in the welding of integrated circuit, because each soldered ball of gained all has identical physical and chemical performance, can guarantee the welding quality of thousands of solder joints on the integrated circuit mainboard, greatly improve the uniformity of electronic system, reduce the defective occurrence probability of entire product greatly; 3, with this device fabrication metal dust, also can be applied on the static pressure powder mould-forming process, greatly improve the performance and the life-span of mould; 4, with this equipment depositing metal films (or coating) on substrate, can obtain the bonding jumper (or band) of property, have broad application prospects.
(4) description of drawings:
Accompanying drawing is the overall structure schematic diagram of the related a kind of metal single-size generator of the utility model.
Wherein: 1 is the piezoelectric excitation generator, and 2 is thermocouple, and 3 is that protective gas is given pipeline altogether, and 4 is crucible; 5 is clapp oscillator, and 6 is heater, and 7 is melt metal or alloy liquid, and 8 is nozzle; 9 is the positively charged battery lead plate, and 10 is even molten drop, and 11 have the container of cooling liquid in being.
(5) specific embodiment:
Embodiment: a kind of metal single-size generator (seeing accompanying drawing) is characterized in that this device is made up of the container 11 of quartz container, crucible 4, piezoelectric excitation generator 1, thermocouple 2, heater 6, protective gas feeding pipe 3, clapp oscillator 5, battery lead plate 9 and interior dress cooling fluid; Said piezoelectric excitation generator 1 is installed on crucible 4 top oral areas, the clapp oscillator 5 that is connected with piezoelectric excitation generator 1 places bottom in the crucible 4, thermocouple 2 and protective gas feeding pipe 3 insert from top, crucible 4 both sides respectively, heater 6 places crucible 4 side wall perimeter, there is a micropore crucible 4 bottoms, nozzle 8 is equipped with at the micropore place, battery lead plate 9 places the outside below of crucible 4 bottom nozzles 8, there is opening at battery lead plate 9 and nozzle place relative crucible bottom parallel with crucible 4 bottoms, 9 of crucible 4 and battery lead plates have potential difference, the container 11 that cooling liquid is housed place battery lead plate 9 openings under; Said said apparatus places in the quartz container that vacuumizes.
The diameter of above-mentioned said crucible 4 bottom nozzles 8 is got 60 μ m.
The protective gas that the above-mentioned said protective gas feeding pipe 3 that is inserted in the crucible 4 provides is a nitrogen.
The atmospheric pressure that the above-mentioned said protective gas feeding pipe 3 that is inserted in the crucible 4 provides should surpass an atmospheric pressure.
Claims (3)
1, a kind of metal single-size generator is characterized in that this device is made up of the container of quartz container, crucible, piezoelectric excitation generator, thermocouple, heater, protective gas feeding pipe, clapp oscillator, battery lead plate and interior dress cooling fluid; Said piezoelectric excitation generating apparatus is in crucible top oral area, the clapp oscillator that is connected with the piezoelectric excitation generator places bottom in the crucible, thermocouple and protective gas feeding pipe insert from top, crucible both sides respectively, heater places the crucible wall periphery, there is a micropore crucible bottom, nozzle is equipped with at the micropore place, battery lead plate places the outside below of crucible bottom nozzle, there is opening at battery lead plate and nozzle place relative crucible bottom parallel with crucible bottom, between crucible and battery lead plate potential difference is arranged, the container that cooling liquid is housed place the battery lead plate opening under; Said said apparatus places in the quartz container that vacuumizes.
2, according to the said a kind of metal single-size generator of claim 1, the diameter that it is characterized in that said crucible bottom nozzle is between 20-100 μ m.
3, according to the said a kind of metal single-size generator of claim 1, it is characterized in that clapp oscillator can be that disk and rocking beam constitute in the said crucible, also can be other shapes that are beneficial to the liquid metals vibration.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 03258305 CN2649227Y (en) | 2003-08-21 | 2003-08-21 | Metal uniform particle generator |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 03258305 CN2649227Y (en) | 2003-08-21 | 2003-08-21 | Metal uniform particle generator |
Publications (1)
Publication Number | Publication Date |
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CN2649227Y true CN2649227Y (en) | 2004-10-20 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN 03258305 Expired - Fee Related CN2649227Y (en) | 2003-08-21 | 2003-08-21 | Metal uniform particle generator |
Country Status (1)
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CN (1) | CN2649227Y (en) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100402201C (en) * | 2006-05-08 | 2008-07-16 | 西安交通大学 | Short technological process of preparing metal grains |
CN100431746C (en) * | 2005-07-21 | 2008-11-12 | 北京有色金属研究总院 | Method and device for preparing precision welding ball |
CN101279373B (en) * | 2007-12-28 | 2010-05-19 | 天津大学 | Device for preparing nano granule by twice coulomb fissions |
CN101244460B (en) * | 2008-03-13 | 2010-06-02 | 大连理工大学 | Method for producing minuteness conductive fiber |
CN106714955A (en) * | 2014-09-29 | 2017-05-24 | 卡萨尔公司 | Apparatus and method for prilling a liquid, preferably urea melt |
US20170312849A1 (en) * | 2016-05-02 | 2017-11-02 | Electronics And Telecommunications Research Institute | Extruder for metal material and 3d printer using the same |
WO2020063625A1 (en) * | 2018-09-25 | 2020-04-02 | 大连理工大学 | Device and method for preparing ultrafine spherical metal powder using drop-by-drop centrifugal atomization method |
CN114850484A (en) * | 2022-04-29 | 2022-08-05 | 中国科学院赣江创新研究院 | Preparation device and preparation method of rare earth metal microspheres |
-
2003
- 2003-08-21 CN CN 03258305 patent/CN2649227Y/en not_active Expired - Fee Related
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100431746C (en) * | 2005-07-21 | 2008-11-12 | 北京有色金属研究总院 | Method and device for preparing precision welding ball |
CN100402201C (en) * | 2006-05-08 | 2008-07-16 | 西安交通大学 | Short technological process of preparing metal grains |
CN101279373B (en) * | 2007-12-28 | 2010-05-19 | 天津大学 | Device for preparing nano granule by twice coulomb fissions |
CN101244460B (en) * | 2008-03-13 | 2010-06-02 | 大连理工大学 | Method for producing minuteness conductive fiber |
CN106714955A (en) * | 2014-09-29 | 2017-05-24 | 卡萨尔公司 | Apparatus and method for prilling a liquid, preferably urea melt |
CN106714955B (en) * | 2014-09-29 | 2019-12-31 | 卡萨尔公司 | Device and method for granulating a liquid, preferably a urea melt |
US20170312849A1 (en) * | 2016-05-02 | 2017-11-02 | Electronics And Telecommunications Research Institute | Extruder for metal material and 3d printer using the same |
US11110540B2 (en) * | 2016-05-02 | 2021-09-07 | Electronics And Telecommunications Research Institute | Extruder for metal material and 3D printer using the same |
WO2020063625A1 (en) * | 2018-09-25 | 2020-04-02 | 大连理工大学 | Device and method for preparing ultrafine spherical metal powder using drop-by-drop centrifugal atomization method |
CN114850484A (en) * | 2022-04-29 | 2022-08-05 | 中国科学院赣江创新研究院 | Preparation device and preparation method of rare earth metal microspheres |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C19 | Lapse of patent right due to non-payment of the annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |