CN2591022Y - Sulphuricacid evaporator - Google Patents

Sulphuricacid evaporator Download PDF

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Publication number
CN2591022Y
CN2591022Y CN02294114U CN02294114U CN2591022Y CN 2591022 Y CN2591022 Y CN 2591022Y CN 02294114 U CN02294114 U CN 02294114U CN 02294114 U CN02294114 U CN 02294114U CN 2591022 Y CN2591022 Y CN 2591022Y
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CN
China
Prior art keywords
tube
pipe
evaporator
steam
tantalum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN02294114U
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Chinese (zh)
Inventor
巨建辉
杨永福
叶建林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xibu Metal Material Co., Ltd.
Original Assignee
Western Metal Materials Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Application filed by Western Metal Materials Co ltd filed Critical Western Metal Materials Co ltd
Priority to CN02294114U priority Critical patent/CN2591022Y/en
Application granted granted Critical
Publication of CN2591022Y publication Critical patent/CN2591022Y/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model relates to a sulphuric acid evaporator, which comprises an evaporator casing and a heat exchanger positioned at the inner lower part of the evaporator casing. The sulfuric acid evaporator is characterized in that the heat exchanger comprises a heating tube, a distance sink tube, a first tube plate, a second tube plate, a deflecting plate, a fixed rod, a steam inlet tube, a steam outlet tube and a cover plate. The sulfuric acid evaporator solves that diluted sulfuric acid of 20% to 70 % is concentrated into finished product acid of more than 90 %. The utility model has the characteristics of high evaporation efficiency, low energy consumption and corrosion resistance.

Description

A kind of sulfuric acid evaporator
Technical field
The utility model relates to a kind of sulfuric acid evaporator, and the method that is applicable to vacuum concentration is concentrated into finished acid more than 90% with the dilute sulphuric acid of 20%-70% through heating evaporation.
Background technology
Interchanger generally comprises heater assembly and evaporator room two portions, and the pattern of vaporizer has varied, but all can not solve dilute sulphuric acid etching problem at high temperature.Thereby to use maximum be to adopt iron pan as vaporizer.Heating component is with fire coal or fuel oil direct heating, so iron pan is exactly the direct evaporation chamber.Can produce a large amount of ferric sulfate in this vaporizer operational process, cause iron pan to damage, stop up process system, simultaneously energy consumption height, also contaminate environment.
Summary of the invention
The purpose of this utility model is to have proposed a kind of vaporization efficiency height, low, the corrosion resistant sulfuric acid evaporator of energy consumption at above-mentioned deficiency.
The above-mentioned purpose order is achieved through the following technical solutions.
A kind of sulfuric acid evaporator comprises
Evaporator shell-top has the horizontal enamel still that two interfaces and two ends are respectively equipped with interface, and is supported on the ground with leg;
Interchanger-the be positioned at bottom of evaporator shell;
It is characterized in that interchanger comprises following parts:
Steam inlet pipe-its quantity is two, lays respectively at the top and the bottom of the air chamber of evaporator shell one end;
Steam outlet pipe-the be positioned at bottom that evaporator shell one brings out steam chest;
Cover plate-be 16MnR, be positioned at an end of evaporator shell one end air chamber, and weld mutually with the shell of inlet plenum.
Heating tube-its structure is the tantalum pipe that finger-type is arranged, what be built-in with logical steam at the tantalum pipe leaves the stainless steel tube or the carbon steel pipe in gap with tantalum pipe bottom, steam is come out from the gap of stainless steel tube or carbon steel pipe and tantalum pipe, and forming in the tantalum pipe is heating steam, and the tantalum pipe is outward a dilute sulphuric acid;
Spacing tube-be polyfluortetraethylene pipe, its quantity is two groups, lays respectively at the upper and lower of the heating tube of finger-type arrangement;
First tube sheet-be provided with the hole of inserting heating tube thereon is connected by the interface of bolt with evaporator shell one end;
Second tube sheet-be provided with the hole of the stainless steel tube of inserting logical steam thereon, between inlet plenum and discharge chamber;
Traverse baffle-be polyfluortetraethylene plate, support heating tube and spacing tube, its quantity is 3-4, is provided with the hole of inserting heating tube and spacing tube on its plate, and is provided with flow-guiding mouth;
Fixed link-be polytetrafluoroethylmaterial material, its quantity are 1-2, its underpart respectively with intermediary traverse baffle Joint, its upper end and evaporator shell Joint.
A kind of sulfuric acid evaporator according to claim 1 is characterized in that first tube sheet is tantalum/stainless steel clad plate.
The utility model has solved dilute sulphuric acid with 20%-70% and has been concentrated into finished acid more than 90%, has the vaporization efficiency height, and energy consumption is low, corrosion resistant characteristics; Environmental pollution improves.
Description of drawings
Fig. 1 is a structural representation of the present utility model.
Fig. 2 is the structural representation of interchanger.
Embodiment
Embodiment in conjunction with the accompanying drawings further describes as follows to the utility model:
A kind of sulfuric acid evaporator comprises that evaporator shell 5-top has the horizontal enamel still that two interfaces and two ends are respectively equipped with interface, and is supported on the ground with leg; Interchanger-the be positioned at bottom of evaporator shell; It is characterized in that interchanger is made up of following parts: heating tube 10-its structure is the tantalum pipe that finger-type is arranged, what be built-in with logical steam at the tantalum pipe leaves the stainless steel tube 6 or the carbon steel pipe in gap with tantalum pipe bottom, steam is come out from the gap of stainless steel tube or carbon steel pipe and tantalum pipe, forming in the tantalum pipe is heating steam, and the tantalum pipe is outward a dilute sulphuric acid; By the tantalum tube wall dilute sulphuric acid that heat transferred tantalum pipe is outer; Spacing tube 8-be polyfluortetraethylene pipe, its quantity is two groups, lays respectively at the upper and lower of the heating tube of finger-type arrangement; First tube sheet 9-be provided with the hole of inserting heating tube thereon is connected by the interface of bolt with evaporator shell one end; Second tube sheet 3-be provided with is thereon inserted the hole of the stainless steel tube of logical steam; Traverse baffle 12-be polyfluortetraethylene plate, support heating tube and spacing tube, its quantity is 3-4, is provided with the hole of inserting heating tube and spacing tube on its plate, and is provided with flow-guiding mouth; Fixed link 11-be polytetrafluoroethylmaterial material, its quantity are 1-2, its underpart respectively with intermediary traverse baffle Joint, its upper end and evaporator shell Joint; Steam inlet pipe 1,4-its quantity is two, lays respectively at the top and the bottom of the air chamber of evaporator shell one end; Steam outlet pipe 7-the be positioned at bottom that evaporator shell one brings out steam chest; Cover plate 2-be 16MnR, be positioned at an end of evaporator end air chamber, and weld mutually with the shell of inlet plenum.First tube sheet is tantalum/stainless steel clad plate.

Claims (2)

1. a sulfuric acid evaporator comprises
Evaporator shell-top has the horizontal enamel still that two interfaces and two ends are respectively equipped with interface, and is supported on the ground with leg;
Interchanger-the be positioned at bottom of evaporator shell;
It is characterized in that interchanger comprises following parts:
Steam inlet pipe-its quantity is two, lays respectively at the top and the bottom of the air chamber of evaporator shell one end;
Steam outlet pipe-the be positioned at bottom that evaporator shell one brings out steam chest;
Cover plate-be 16MnR, be positioned at an end of evaporator shell one end air chamber, and weld mutually with the shell of inlet plenum.
Heating tube-its structure is the tantalum pipe that finger-type is arranged, what be built-in with logical steam at the tantalum pipe leaves the stainless steel tube or the carbon steel pipe in gap with tantalum pipe bottom, steam is come out from the gap of stainless steel tube or carbon steel pipe and tantalum pipe, and forming in the tantalum pipe is heating steam, and the tantalum pipe is outward a dilute sulphuric acid;
Spacing tube-be polyfluortetraethylene pipe, its quantity is two groups, lays respectively at the upper and lower of the heating tube of finger-type arrangement;
First tube sheet-be provided with the hole of inserting heating tube thereon is connected by the interface of bolt with evaporator shell one end;
Second tube sheet-be provided with the hole of the stainless steel tube of inserting logical steam thereon, between inlet plenum and discharge chamber;
Traverse baffle-be polyfluortetraethylene plate, support heating tube and spacing tube, its quantity is 3-4, is provided with the hole of inserting heating tube and spacing tube on its plate, and is provided with flow-guiding mouth;
Fixed link-be polytetrafluoroethylmaterial material, its quantity are 1-2, its underpart respectively with intermediary traverse baffle Joint, its upper end and evaporator shell Joint.
2. a kind of sulfuric acid evaporator according to claim 1 is characterized in that first tube sheet is tantalum/stainless steel clad plate.
CN02294114U 2002-12-27 2002-12-27 Sulphuricacid evaporator Expired - Lifetime CN2591022Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN02294114U CN2591022Y (en) 2002-12-27 2002-12-27 Sulphuricacid evaporator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN02294114U CN2591022Y (en) 2002-12-27 2002-12-27 Sulphuricacid evaporator

Publications (1)

Publication Number Publication Date
CN2591022Y true CN2591022Y (en) 2003-12-10

Family

ID=33751725

Family Applications (1)

Application Number Title Priority Date Filing Date
CN02294114U Expired - Lifetime CN2591022Y (en) 2002-12-27 2002-12-27 Sulphuricacid evaporator

Country Status (1)

Country Link
CN (1) CN2591022Y (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101097125B (en) * 2006-06-26 2011-10-12 斯南普罗吉蒂联合股票公司 Anti-corrosion bimetal tube, manufacturing method and the application in tube bundle devices
CN103056637A (en) * 2012-12-27 2013-04-24 西安优耐特容器制造有限公司 Adjustable installation device and method for tantalum heater
CN107963616A (en) * 2017-12-29 2018-04-27 无锡英罗唯森科技有限公司 A kind of evaporator for sulphuric acid concentration
CN109364503A (en) * 2018-11-29 2019-02-22 李晓垚 A kind of sulfuric acid evaporator
CN115253324A (en) * 2022-06-24 2022-11-01 江苏理文化工有限公司 Sulfuric acid concentration heating equipment

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101097125B (en) * 2006-06-26 2011-10-12 斯南普罗吉蒂联合股票公司 Anti-corrosion bimetal tube, manufacturing method and the application in tube bundle devices
CN103056637A (en) * 2012-12-27 2013-04-24 西安优耐特容器制造有限公司 Adjustable installation device and method for tantalum heater
CN103056637B (en) * 2012-12-27 2015-05-20 西安优耐特容器制造有限公司 Adjustable installation device and method for tantalum heater
CN107963616A (en) * 2017-12-29 2018-04-27 无锡英罗唯森科技有限公司 A kind of evaporator for sulphuric acid concentration
CN109364503A (en) * 2018-11-29 2019-02-22 李晓垚 A kind of sulfuric acid evaporator
CN109364503B (en) * 2018-11-29 2021-01-05 广德县桃州镇明莲蔬果种植家庭农场 Sulfuric acid evaporator
CN115253324A (en) * 2022-06-24 2022-11-01 江苏理文化工有限公司 Sulfuric acid concentration heating equipment

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: WEST METAL MATERIAL CO., LTD.

Free format text: FORMER NAME OR ADDRESS: WESTERN METAL MATERIALS CO., LTD.

CP03 Change of name, title or address

Address after: 710056 No. three, No. 56, hi tech Zone, Shaanxi, Xi'an

Patentee after: Xibu Metal Material Co., Ltd.

Address before: Weiyang road 710016 Shaanxi city of Xi'an province No. 96

Patentee before: Xiyan Rare Metal New Material Co., Ltd.

EE01 Entry into force of recordation of patent licensing contract

Assignee: XiAn Unite Container Manufacturing Co., Ltd.

Assignor: Xibu Metal Material Co., Ltd.

Contract record no.: 2011610000039

Denomination of utility model: Method for installing sulfuric acid evaporator tantalum material heating tube nest

Granted publication date: 20031210

License type: Exclusive License

Record date: 20110621

C17 Cessation of patent right
CX01 Expiry of patent term

Expiration termination date: 20121227

Granted publication date: 20031210