CN2343585Y - Natural gas trace metal sampler - Google Patents

Natural gas trace metal sampler Download PDF

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Publication number
CN2343585Y
CN2343585Y CN 98215714 CN98215714U CN2343585Y CN 2343585 Y CN2343585 Y CN 2343585Y CN 98215714 CN98215714 CN 98215714 CN 98215714 U CN98215714 U CN 98215714U CN 2343585 Y CN2343585 Y CN 2343585Y
Authority
CN
China
Prior art keywords
valve
trace metal
natural gas
filtrator
meter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN 98215714
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Chinese (zh)
Inventor
邵剑梅
罗兴仁
安慕彬
卢福庆
孙立
于燕
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oilfield Construction Design And Research Institute Of Daqing Petroleum Administration
Original Assignee
Oilfield Construction Design And Research Institute Of Daqing Petroleum Administration
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Priority to CN 98215714 priority Critical patent/CN2343585Y/en
Application granted granted Critical
Publication of CN2343585Y publication Critical patent/CN2343585Y/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model relates to a natural gas trace metal sampler for enriching some trace metal elements in the natural gas and ensuring that the concentration the trace metal elements reaches the lower limit of an atomic absorption spectrometer. A natural gas conveying pipeline is connected with a gas inlet valve 4, a pressure gauge 3, a regulating valve 6, a float gauge 12, an emptying valve 7 which is connected in parallel and a master valve 5. A pipeline of the main valve 5 is also connected with a quality flow meter 2 with an electronic meter 23 and a filter 19; a plurality of layers of filtering membranes and partitioned filtering nets is arranged in the filter 9, wherein, the trace metal particles in the natural gas are enriched on the filtering membranes, because of the special treatment of the filtering membranes. Then, the content of the trace metal particles can be tested through the spectrometer.

Description

Rock gas trace meter sampling instrument
The utility model relates to and is used for the on-the-spot enrichment sampling apparatus that petroleum chemical industry is analyzed rock gas minor metallic element content, belongs to rock gas trace meter sampling instrument.
Along with developing rapidly of petrochemical complex industry, rock gas is widely used in the Chemical Manufacture, and it can be used to do fuel, raw material etc.Find to have some trace meter compounds in the rock gas in the production practices process, it mainly exists with gasoloid or particle form.The colloidal solid form is polymolecular aggregate, is difficult for being absorbed liquid and absorbs or be absorbed pipe institute detention.The perishable pipeline of some trace meter compounds in the rock gas, chemical plant, some also can make catalyst poisoning.Because minor metallic element content very little (ppb) level can't adopt analytical instrument directly to detect in the rock gas, does not find the on-the-spot enrichment sampling apparatus of rock gas trace meter content at present as yet.
The purpose of this utility model is to provide a kind of can improve the sampling instrument of concentration effect to some trace metal elements in the rock gas, makes the concentration of the metallic element of being gathered reach the lower limit that detects of Atomic Absorption Spectrometer or other detector.
The purpose of this utility model can reach by the following technical programs: be connected to gas admittance valve, tensimeter, variable valve, float meter and atmospheric valve and main valve in parallel on defeated natural gas line, on the pipeline of main valve, be connected to the mass flowmeter of charged sub-meter and the filtrator of sealing again, which floor filtering membrane is housed in this filtrator, constitutes the sampling instrument of housing.
In the above-mentioned filtrator two-layer filter membrane can be arranged, between two-layer filter membrane,, can adopt through tygon pyridine oxide and glycerine to add the impregnated filtering membrane of water agitating solution every accompanying two-layer filter screen.The sampling instrument of this sealing, gas in the scheduled time, carry out cumulative measurement to gas volume at meter electronics through mass flowmeter: use the filter membrane of special processing can trap less than trace meter in the rock gas in filter membrane aperture, thereby can realize this purpose.
The utlity model has following characteristics: volume is little, and compact conformation is made casing, is convenient to on-site sampling.Be not subjected to gaseous tension, Temperature Influence in scene temperature and the pipeline.Because mass flowmeter is housed, the gas volume of being gathered can be converted, directly metering.Because the filtering membrane of special processing is housed in the filtrator, can reaches 90% to the collecting efficiency of fine particle composition, colloid in the rock gas, and not be subjected to acquisition target to have the influence of form.Repdocutbility is good, and is easy and simple to handle, and the sampling time is realized control automatically, alleviates working strength.Also be applicable to enrichment to metallic compound in other gas.
Accompanying drawing the 1, the 2nd, this sampling instrument outward appearance master looks and left view;
Accompanying drawing 3 is this sampling instrument structural representations;
Accompanying drawing 4 is filtrator 11 sectional views on Fig. 3.
The utility model is described in further detail below in conjunction with inciting somebody to action shown in the accompanying drawing 4:
In conjunction with the accompanying drawings shown in 4, gas enters 1 li of housing through sampling instrument air intake opening 10 in the transport gas pipeline by accompanying drawing 3, is connected to gas admittance valve 4, tensimeter 3, variable valve 6, float meter 12, air release 7 and main valve 5 in parallel on the pipeline in the housing; Connect mass flowmeter 2 that has meter electronics 23 and the filtrator 19 that seals on the pipeline of main valve 5 again, filtrator is equipped with which floor filtering membrane (17,21) for 19 li.
Above-mentioned filtrator can have two-layer filter film (17,21) for 19 li, reaches the air inlet side and accompany two-layer filter screen (18,20) again at interval between two-layer filtering membrane (17,21); Filter membrane and filter screen are the disk shape, between with O type sealed picture (15,16,22) packing, then filtrator 19 is sealed with lid 14 bolt 13 of screwing on.Can adopt through tygon pyridine oxide and glycerine to add the impregnated filtering membrane of water agitating solution (17,21), improve metallic element effect in the enrichment rock gas.On atmospheric valve 7, connect bleeder pipe 9 in addition, be connected to bleeder pipe 8 on the filtrator 19.Carry handle 11 for conveniently guiding and supporting to be equipped with on the sampling instrument.Mass flowmeter 2 and float meter 12 are buying profiled members, and meter electronics 23 is equipped with in mass flowmeter 2 the insides.Earlier main valve 5 cuts out during use, rock gas is entered by import 10, utilize valve 6 to regulate gas discharge, treat flow reach desired value and stable after, open main valve 5 and close atmospheric valve 7, at this moment, rock gas enters mass flowmeter 2, in meter electronics 23 Preset Times, the rock gas volume is carried out cumulative measurement; Rock gas is by filtrator 19, and filtering membrane can fully absorb and dissolve fine particle composition to be measured, makes the concentration of the element of institute's enrichment reach the lower limit that detects of Atomic Absorption Spectrometer or other detector, and filter back gas is emitted fast through gas outlet 8.Each control valve on this sampling instrument (4,5,6,7) and demonstration are observed parts and all are contained in surface of shell, with handled easily and observation.

Claims (3)

1. one kind is used to analyze petroleum gas trace meter sampling instrument, it is characterized in that: the atmospheric valve (7) and the main valve (5) that on the transport gas pipeline, tap into air valve (4), tensimeter (3), variable valve (6), float meter (12), parallel connection, on the pipeline of main valve (5), connect mass flowmeter (2) and the filtrator (19) that has meter electronics (23) again, filtrator (19) lining is equipped with which floor filtering membrane (17,21).
2. sampling instrument according to claim 1 is characterized in that: can there be two-layer filtering membrane (17,21) filtrator (19) lining, between the two-layer filtering membrane (17,21) and the air inlet side be separated with two-layer filter screen (18,20) between again.
3. sampling instrument according to claim 1 and 2 is characterized in that: can adopt through tygon pyridine oxide and glycerine to add the impregnated filtering membrane of water agitating solution (17,21).
CN 98215714 1998-06-16 1998-06-16 Natural gas trace metal sampler Expired - Lifetime CN2343585Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 98215714 CN2343585Y (en) 1998-06-16 1998-06-16 Natural gas trace metal sampler

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 98215714 CN2343585Y (en) 1998-06-16 1998-06-16 Natural gas trace metal sampler

Publications (1)

Publication Number Publication Date
CN2343585Y true CN2343585Y (en) 1999-10-13

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 98215714 Expired - Lifetime CN2343585Y (en) 1998-06-16 1998-06-16 Natural gas trace metal sampler

Country Status (1)

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CN (1) CN2343585Y (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100460858C (en) * 2005-12-13 2009-02-11 上海神开石油化工装备股份有限公司 Method for on-line spectral determining oily gas in drilling liquid
CN100520360C (en) * 2006-07-19 2009-07-29 中国科学院安徽光学精密机械研究所 Opening natural gas leaking multi-channel monitoring method and light path structure
CN103471877A (en) * 2013-09-29 2013-12-25 中国寰球工程公司 System for sampling and component analysis of natural gas generated after absorption tower deacidification
CN108007868A (en) * 2017-12-19 2018-05-08 山东科技大学 Underground natural gas storage gas recovery well moisture content detection device and underground natural gas storage gas recovery well moisture content detecting method
CN113702585A (en) * 2021-08-26 2021-11-26 山东非金属材料研究所 Automatic capturing and digesting device for trace metal elements in high-purity gas

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100460858C (en) * 2005-12-13 2009-02-11 上海神开石油化工装备股份有限公司 Method for on-line spectral determining oily gas in drilling liquid
CN100520360C (en) * 2006-07-19 2009-07-29 中国科学院安徽光学精密机械研究所 Opening natural gas leaking multi-channel monitoring method and light path structure
CN103471877A (en) * 2013-09-29 2013-12-25 中国寰球工程公司 System for sampling and component analysis of natural gas generated after absorption tower deacidification
CN103471877B (en) * 2013-09-29 2016-09-28 中国寰球工程公司 Natural gas sampling after the deacidification of a kind of absorption tower and component analysis system
CN108007868A (en) * 2017-12-19 2018-05-08 山东科技大学 Underground natural gas storage gas recovery well moisture content detection device and underground natural gas storage gas recovery well moisture content detecting method
CN108007868B (en) * 2017-12-19 2024-06-11 山东科技大学 Device and method for detecting water content of natural gas underground gas storage gas production well
CN113702585A (en) * 2021-08-26 2021-11-26 山东非金属材料研究所 Automatic capturing and digesting device for trace metal elements in high-purity gas

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