CN2251122Y - External heating type furnace for preliminary heat treatment in oxidizing - Google Patents

External heating type furnace for preliminary heat treatment in oxidizing Download PDF

Info

Publication number
CN2251122Y
CN2251122Y CN 95226608 CN95226608U CN2251122Y CN 2251122 Y CN2251122 Y CN 2251122Y CN 95226608 CN95226608 CN 95226608 CN 95226608 U CN95226608 U CN 95226608U CN 2251122 Y CN2251122 Y CN 2251122Y
Authority
CN
China
Prior art keywords
furnace
air
burner hearth
utility
hot
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 95226608
Other languages
Chinese (zh)
Inventor
贺福
贾裕智
赵建国
周国英
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanxi Institute of Coal Chemistry of CAS
Original Assignee
Shanxi Institute of Coal Chemistry of CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanxi Institute of Coal Chemistry of CAS filed Critical Shanxi Institute of Coal Chemistry of CAS
Priority to CN 95226608 priority Critical patent/CN2251122Y/en
Application granted granted Critical
Publication of CN2251122Y publication Critical patent/CN2251122Y/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Inorganic Fibers (AREA)

Abstract

The utility model relates to an external heating type pre-oxidization furnace. The utility model has the vertical and horizontal structure. The interior of the furnace is provided with two to six furnace hearths (8) which are arranged in layer. The upper part and the lower part of the furnace hearth are provided with slide ways (13). A separated frame style heater (7) is provided with an upper heating surface and a lower heating surface is loaded in or dismounted along the slide ways. Each furnace hearth is respectively connected with a hot air furnace. The both sides of the furnace hearth are provided with hot air flow distribution pipes (12) to delivery air. The top of the furnace is provided with an air preheating pipe (6), a waste gas exhaust opening (4) and an air blowing inlet (14). Fiber operates in the wire walking narrow slits (3) of the furnace hearth. The utility model adopts the separated frame style heater, and then the maintenance and the replacement are convenient. The waste gas exhaust opening and the air inlet of the furnace body have obvious energy-saving and consumption-reduction effects through heat exchange.

Description

The external-heat pre-oxidation furnace
The utility model belongs to the pre-oxidation device in the carbon fiber production technology.
One of primary raw material that is used to produce carbon fiber is polyacrylonitrile fibre (PANF), this fiber need carry out pre-oxidation treatment earlier before carbonization, its objective is that the linear molecule chain that makes polyacrylonitrile is converted into heat-resisting trapezium structure,, and keep fibre morphology so that it is molten when high temperature cabonization, do not fire.Because the pre-oxidation stage is a principal element of control carbon fiber quality and output, so preoxidation process requires pre-oxidation furnace to have: furnace body temperature that (1) is wide as far as possible and temperature gradient distribution; (2) wind-warm syndrome, air quantity and the blast of big operating flexibility; (3) satisfy production efficiency and the furnace space of effective time of staying of tow; (4) energy-conservation; (5) be fit to suitability for industrialized production.The vertical heater of present more use is discrete stack, and combustion space is little, and the tow number of feeding is few, and wire travelling speed is slow, yields poorly, and energy consumption is big.Horizontal pre-oxidation furnace is generally internal heat type, and naked light is arranged in the burner hearth, easily causes catching fire of tow.And the heater element electric furnace heating wire of the horizontal pre-oxidation furnace of outer heat that has directly is wrapped in outside the burner hearth, keeps in repair very inconvenient.
The purpose of this utility model is to provide a kind of outer heating pre-oxidation furnace of horizontal type structure, and the effective warm area of this stove and accessory is long, and temperature regulating range is wide, and thermograde is adjustable, the characteristics of temperature multiple spot control.
External-heat pre-oxidation furnace of the present utility model is a horizontal chamber furnace (oven), 2-6 the burner hearth that has layering to be provided with in the stove, on burner hearth, have slideway, have the up and down split frame-type heater of two heating surfaces, can pack into or split out along slideway, each burner hearth all connects a hot-blast stove, blow by the hot-air flow distributor pipe that the burner hearth both sides are provided with, furnace roof is provided with economizer bank, and Waste gas outlet and air are blown into mouth, and fiber is by the operation of the wire slit between burner hearth.
Pre-oxidation furnace of the present utility model adopts the structure of horizontal burner hearth layering, has following advantage:
1. each pre-oxidation furnace comfort zone accumulation length is 66 meters (can supply the effective length of tow layering operation).
2. the equalizing section field width can reach 5-10, and temperature regulating range 150-300 ℃, effectively the time of staying is 40-66 minute.
3. if two pre-oxidation furnace series connection are used, then effective travel is 132 meters, and the time of staying reaches the 80-132 clock.
4. but split frame-type heater convenient for maintaining and replacing.
5. the exhaust gas entrance at body of heater top and fresh air inlet have considerable energy saving consumption reduction effect by heat exchanger.
This stove is handled fiber dimensious 3-320K, maximum operation tow number 100-120 bundle, yearly productive capacity: little tow 30-40 ton, big tow 50-80 ton.
Describe structure of the present utility model and embodiment in detail below by the accompanying drawing that provides.
Figure 1 shows that according to the outer heating pre-oxidation furnace structural representation that the utility model proposes.
Fig. 2 is that Fig. 1 K is to view.
Fig. 3 is the A-A view of Fig. 1.
Fig. 4 is a hot-air flow distributor pipe air-supply distribution schematic diagram in the burner hearth.
1 is polyacrylonitrile fibre among the figure, the 2nd, and godet, the 3rd, wire slit, the 4th, Waste gas outlet, the 5th, heat-barrier material, the 6th, economizer bank, the 7th, heating tube, the 8th, burner hearth, the 9th, surge chamber, the 10th, heat-barrier material, the 11st, furnace tubing, the 12nd, hot-air flow distributor pipe, the 13rd, slideway, the 14th, air intake, the 15th, pore.
As shown in the figure, this oxidation furnace is horizontal body of heater, but layering arranges 2-6 burner hearth 8 in the stove, among Fig. 1 What draw is four burner hearths, has slideway 13 on the burner hearth, and frame-type divides body heater 7 to fill along slideway Enter, be convenient to install or split out maintenance, the up and down position of heater 7 is equipped with heating element heater. Establish the burner hearth both sides Put the hot blast tracheorrhaphy stringing 12 of Heterogeneous Permutation, have pore 15 on the pipe 12. Each burner hearth all connects one Hot-blast stove, hot-blast stove be by surge chamber 9, and furnace tubing 11 forms, two groups of electric furnace heating wires in the furnace tubing with Parallel form is installed, and fire door adopts just open-type flange seal. Hot blast is by hot-air flow distributor pipe 12 15 up and down two in-planes (such as figure four) that are blown into vertical operation tow from the hole, arrow is depicted as hot blast and blows The direction that goes out. The air quantity adjustable range that hot-blast stove provides is 0-300 cubic meter/time, blast 0.003-0.035MPa, body of heater centre wind speed 0.13-0.25 meter per second is continuously adjustable. The body of heater top If Waste gas outlet 4, air intake 14 and heat exchange air economizer bank 6. Air is sent into after metering in advance Oxidation body of heater top makes the hot waste gas that gives off in the stove and the fresh air of sending into carry out heat exchange, after Hold in both hands out waste gas, give fresh air after the heat and import each hot-blast stove and be heated to and send into correspondence after temperature required Each burner hearth. Utilize the external dispersed heat preheating of pre-oxidation furnace body to advance the air of stove, can be with 240 cubes In rice/time,, air was increased to 60-120 ℃ from room temperature, saved electrical power 9-20KW. Polyacrylonitrile fibre 1 by Godet 2 is pulled in back and forth operation in the wire slit 3 between the burner hearth, carries out in 200-270 ℃ of scope Fully pre-oxidation. With the matching used in addition drafter of pre-oxidation furnace, 2-4 dominant draft dress arranged Put, 4-10 secondary drafting system arranged, available frequency converter is arbitrarily regulated the degree of draft of different warm areas. No matter Dominant draft device or secondary drafting system, driven roll all can regulate and drive roll between spacing, with Adapt to the demand degree of draft different with adjusting when wearing thread. Temperature control system available digital formula temperature controller, also The control of available microcomputer network is so that institute's controlling temperature is required ± 3 ℃.
Embodiment 1
Polyacrylonitrile fibre 6K, 60 bundles, 80 meters of the tow speeds of service/time, back and forth moving 11 layers, pre-oxidation furnace is provided with 5 sections of temperature (separate unit body of heater), temperature range 225-265 ℃.The heating air blast, without the heat exchange of pre-oxidation body of heater, hot-blast stove add quantity of hot air be respectively 55,55,60,55 cubic metres/time.Wind-warm syndrome: 220,225,250 ℃, blast 0.01MPa.During dynamic balancing, hot blast protects adduction power 23.38KW.The product test result, intensity 250MPa, elongation 13%, silk footpath 10.1 μ m, density 1.406g/cm 3
Embodiment 2
Polyacrylonitrile fibre 6K, 80 bundles, 85 meters of the tow speeds of service/time, in the stove reciprocal 11 layers.Pre-oxidation furnace is provided with temperature range: 205-270 ℃ of 5 sections of warm area (separate unit body of heater).Air is sent into hot-blast stove heating after the preheating of pre-oxidation furnace body, 195,215,230,250 ℃ of heating-up temperatures, air quantity be respectively 70,70,75,70 cubic metres/time, blast: 0.01MPa.During dynamic balancing, hot-blast stove adduction power 15KW.Product test result: intensity 303MPa, elongation 13.5%, silk footpath 9.87 μ m, density 1.38g/cm 3

Claims (1)

1. external-heat pre-oxidation furnace, be horizontal type structure, it is characterized in that having in the stove 2-6 the burner hearth (8) of layering setting, on burner hearth, have slideway (13), split frame-type heater (7) with two heating surfaces up and down can be packed into or splits out along slideway, each stove subjectively all connects a hot blast and is jealous of, blow by the hot-air flow distributor pipe (12) that the burner hearth both sides are provided with, furnace roof is provided with economizer bank (6), Waste gas outlet (4) and air are blown into mouthful (14), and fiber is by the operation of the wire slit (3) between burner hearth.
CN 95226608 1995-11-27 1995-11-27 External heating type furnace for preliminary heat treatment in oxidizing Expired - Fee Related CN2251122Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 95226608 CN2251122Y (en) 1995-11-27 1995-11-27 External heating type furnace for preliminary heat treatment in oxidizing

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 95226608 CN2251122Y (en) 1995-11-27 1995-11-27 External heating type furnace for preliminary heat treatment in oxidizing

Publications (1)

Publication Number Publication Date
CN2251122Y true CN2251122Y (en) 1997-04-02

Family

ID=33872718

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 95226608 Expired - Fee Related CN2251122Y (en) 1995-11-27 1995-11-27 External heating type furnace for preliminary heat treatment in oxidizing

Country Status (1)

Country Link
CN (1) CN2251122Y (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102660810A (en) * 2012-03-21 2012-09-12 上海联川自动化科技有限公司 Fireproof layers of carbon fiber oxidation furnace
CN107557909A (en) * 2017-08-25 2018-01-09 中国科学院宁波材料技术与工程研究所 A kind of air oxidation stove and its application
CN108716857A (en) * 2018-07-26 2018-10-30 青岛海源实业有限公司 A kind of layering burner hearth Liftable type multilayer resistance-heated furnace
CN114318592A (en) * 2022-01-28 2022-04-12 新创碳谷控股有限公司 Novel carbon fiber pre-oxidation furnace with air distribution structure
CN114775111A (en) * 2022-05-16 2022-07-22 清华大学 Carbon fiber pre-oxidation system and high-temperature tail gas backflow method

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102660810A (en) * 2012-03-21 2012-09-12 上海联川自动化科技有限公司 Fireproof layers of carbon fiber oxidation furnace
CN102660810B (en) * 2012-03-21 2014-04-09 上海联川自动化科技有限公司 Fireproof layers of carbon fiber oxidation furnace
CN107557909A (en) * 2017-08-25 2018-01-09 中国科学院宁波材料技术与工程研究所 A kind of air oxidation stove and its application
CN107557909B (en) * 2017-08-25 2020-07-14 中国科学院宁波材料技术与工程研究所 Air oxidation furnace and application thereof
CN108716857A (en) * 2018-07-26 2018-10-30 青岛海源实业有限公司 A kind of layering burner hearth Liftable type multilayer resistance-heated furnace
CN108716857B (en) * 2018-07-26 2024-04-19 青岛海源碳烯铝合金新材料科技有限公司 Layered hearth lifting type multilayer resistance heating furnace
CN114318592A (en) * 2022-01-28 2022-04-12 新创碳谷控股有限公司 Novel carbon fiber pre-oxidation furnace with air distribution structure
CN114775111A (en) * 2022-05-16 2022-07-22 清华大学 Carbon fiber pre-oxidation system and high-temperature tail gas backflow method

Similar Documents

Publication Publication Date Title
CN210596335U (en) Drafting hot box for producing high-strength high-modulus polyethylene fibers
CN2823937Y (en) Hot air cocoon drier
CN2251122Y (en) External heating type furnace for preliminary heat treatment in oxidizing
CN201459366U (en) Heat shaping device for producing non-woven cotton
CN101135535A (en) High mould high-strength northylen hot blast drying cabinets
CN206143365U (en) A oxidation unit in advance for carbon fiber production
CN201257387Y (en) Sectional type heated air circulation calcination mesh-belt furnace
CN105603164A (en) Roller-hearth quenching furnace
CN209068946U (en) A kind of grain drying tower warm air oil furnace
CN103222574B (en) Drying room for unfrozen sweet potato vermicelli
CN202917263U (en) Vertical type hot air circulation oven for high-speed flat wire enamelling machine
CN109442988A (en) A kind of kiln car formula kiln with waste-heat recovery device
CN201537998U (en) circulating hot-air oven
CN213113626U (en) Continuous pre-oxidation furnace
CN2766577Y (en) Close packing tobacco flue-curing oven
CN2855156Y (en) Improved tunnel type wet/heat boarder
CN2796037Y (en) Novel horizontal catalytic burning heat exchanging and hot air circulation lacquered wire machine baking stove
CN208617366U (en) Automatic horizontal carbonizes converter
CN206398763U (en) Greenhouse heats carburetting gasification furnace with novel biomass
CN201100829Y (en) High mode high intensity polyethene fiber thermal wind drying box
CN201188334Y (en) Novel heated air circulation drying furnace for enamelling machine
CN206736095U (en) A kind of rock wool processes automatic unit weight device
CN101144199A (en) High-module high-strength polyethylene fibre double air channel drafting heat box
CN206207992U (en) A kind of high-efficiency tunnel kiln
CN1062826A (en) A kind of drying room of dry vermicelli

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee