CN221619408U - Reaction kettle with sampling structure - Google Patents
Reaction kettle with sampling structure Download PDFInfo
- Publication number
- CN221619408U CN221619408U CN202420017134.3U CN202420017134U CN221619408U CN 221619408 U CN221619408 U CN 221619408U CN 202420017134 U CN202420017134 U CN 202420017134U CN 221619408 U CN221619408 U CN 221619408U
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- bolted
- sampling
- kettle body
- sampling structure
- reaction kettle
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- 238000005070 sampling Methods 0.000 title claims abstract description 50
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 30
- 239000011521 glass Substances 0.000 claims abstract description 22
- 238000002955 isolation Methods 0.000 claims description 28
- 238000007789 sealing Methods 0.000 claims description 10
- 229910052751 metal Inorganic materials 0.000 claims description 8
- 239000002184 metal Substances 0.000 claims description 8
- 238000004804 winding Methods 0.000 claims description 7
- 239000003153 chemical reaction reagent Substances 0.000 abstract description 31
- 239000007788 liquid Substances 0.000 abstract description 6
- 238000000926 separation method Methods 0.000 abstract description 6
- 239000000523 sample Substances 0.000 description 20
- 230000000694 effects Effects 0.000 description 7
- 238000005457 optimization Methods 0.000 description 7
- 238000000034 method Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 239000013049 sediment Substances 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000005192 partition Methods 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 229910000617 Mangalloy Inorganic materials 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- QFGIVKNKFPCKAW-UHFFFAOYSA-N [Mn].[C] Chemical compound [Mn].[C] QFGIVKNKFPCKAW-UHFFFAOYSA-N 0.000 description 1
- 230000004308 accommodation Effects 0.000 description 1
- 230000029936 alkylation Effects 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 238000006396 nitration reaction Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Landscapes
- Sampling And Sample Adjustment (AREA)
Abstract
The utility model discloses a reaction kettle with a sampling structure, which belongs to the technical field of reaction kettles and is characterized in that the reaction kettle comprises a kettle body, wherein a top cover is arranged at the top of the kettle body, a communicating pipe is bolted to the outer side of the kettle body, a separation valve is bolted to the bottom of the top communicating pipe and the top of the bottom communicating pipe, a glass pipe is movably connected to one side of the separation valve, which is far away from the communicating pipe, of the glass pipe, a discharge valve is arranged at the outer side of the glass pipe, a sampling assembly is arranged at the top of the top cover, the kettle body is matched with the top cover to serve as a reaction space of a reagent, the arranged communicating pipe is matched with the separation valve and the glass pipe, when the reagent liquid needs to be sampled, the separation valve can be opened, so that the reagent can enter the glass pipe, at the moment, personnel can observe the condition of the internal reagent directly through the glass pipe, and can discharge the reagent through the discharge valve after the separation valve is closed so as to facilitate sampling and collection.
Description
Technical Field
The utility model relates to the technical field of reaction kettles, in particular to a reaction kettle with a sampling structure.
Background
The reaction kettle is widely used in the fields of petroleum, chemical industry, rubber, pesticides, dyes, medicines, foods and the like, and is a pressure container for completing the technological processes of vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like, such as a reactor, a reaction pot, a decomposition pot, a polymerization pot and the like; materials generally include carbon manganese steel, stainless steel, zirconium, nickel-based alloys and other composite materials.
Can use reation kettle when carrying out reagent reaction, current reation kettle need open the top cap when taking a sample to the sample is taken to this process not only is difficult to the volume of control sample, and inside reagent still is by sampling container and environmental pollution easily, uses comparatively inconveniently.
Disclosure of utility model
The utility model provides a reaction kettle with a sampling structure, which aims to solve the problems that the top cover needs to be opened when the existing reaction kettle samples an internal reagent, and a sample is acquired, the sampling amount is difficult to control in the process, the internal reagent is easy to pollute a sampling container and the environment, and the use is inconvenient.
The utility model is realized in such a way, the reaction kettle with the sampling structure comprises a kettle body, wherein a top cover is arranged at the top of the kettle body, a communicating pipe is bolted at the outer side of the kettle body, isolation valves are bolted at the bottom of the top communicating pipe and the top of the bottom communicating pipe, a glass pipe is movably connected at one side of the isolation valve far away from the communicating pipe, a discharge valve is arranged at the outer side of the glass pipe, a sampling assembly is arranged at the top of the top cover, a separation plate is movably connected at the inner side of the bottom of the kettle body, and a containing box is movably connected at the bottom of the kettle body;
The sampling assembly comprises an end cap, a hollow sleeve is bolted to the bottom of the end cap, and a winding rod is bolted to the inner side of the hollow sleeve.
In order to achieve the effect of being convenient for discharging the pressure in the container, the reaction kettle with the sampling structure is preferable, a pressure release valve is arranged at the top of the top cover, an internal thread sleeve is arranged at the top of the top cover, and the inner side of the internal thread sleeve is in threaded connection with the end cap.
In order to achieve the effect of conveniently filtering sampled reagents, the reaction kettle with the sampling structure is preferable in the utility model, a filter screen is movably connected to the inner side of the isolation valve, and the isolation valve is a butterfly valve.
In order to achieve the effect of being convenient for limit the isolation plate, the reaction kettle with the sampling structure is preferable in the utility model, the bottom of the inner wall of the kettle body is provided with the movable groove, the rear side of the inner side of the movable groove is bolted with the spring, and the front side of the spring is bolted with the isolation plate.
In order to achieve the effect of being convenient for reagent to flow, the reaction kettle with the sampling structure is preferable, a round hole is formed in the bottom of the kettle body, and a flow hole is formed in the top of the accommodating box.
In order to achieve the effect of being convenient for supporting the accommodating box, the reaction kettle with the sampling structure is preferable in the utility model, a box frame is bolted to the bottom of the kettle body, and the inner side of the box frame is in sliding connection with the accommodating box.
In order to achieve the effect of being convenient for supporting the accommodating box and the box frame, as the reaction kettle with the sampling structure, a magnetic block is preferably bolted to the rear side of the inner side of the box frame, and a metal block is bolted to the rear side of the accommodating box, and the metal block and the magnetic block are bonded.
In order to achieve the effect of being convenient for improving the tightness between structures, the reaction kettle with the sampling structure is preferable in the utility model, wherein the sealing ring is bolted to the top of the accommodating box, the abutting piece is bolted to the bottom of the isolation plate, the outer side of the abutting piece is matched with the sealing ring for use, and the one-way valve is bolted to the bottom of the accommodating box.
Compared with the prior art, the utility model has the beneficial effects that:
This reation kettle with sampling structure, through setting up the reaction space of the lid of cauldron body cooperation as reagent, communicating pipe cooperation isolation valve and glass pipe of setting, when needs take a sample to reagent liquid, can open the isolation valve, make reagent get into in the glass pipe, personnel can observe the inside reagent condition through the glass pipe this moment, and can discharge it in order to sample collection through the discharge valve after closing the isolation valve, the sample subassembly of setting can be convenient for sample floc etc. that produce in the internal reagent of cauldron, can rotate the end cap and make it become flexible from the lid when using, and sample through hollow cover, floc etc. twine on twining the pole so that sample is collected easily, the division board cooperation that sets up holds the box, reagent sediment to cauldron body bottom is convenient for take a sample, open the pollution that cauldron body top leads to when having avoided the sample, and can carry out the adjustment of sampling method to the content of required sampling, it is comparatively nimble to use.
Drawings
FIG. 1 is an overall structure diagram of a reaction kettle with a sampling structure of the utility model;
FIG. 2 is a schematic diagram of the isolation valve of the present utility model;
FIG. 3 is a schematic view of the bottom structure of the kettle body of the present utility model;
FIG. 4 is a schematic diagram of the connection of the separator of the present utility model;
FIG. 5 is a schematic view of the structure of the accommodating case of the present utility model;
FIG. 6 is a schematic diagram of the internal structure of the sampling assembly according to the present utility model.
In the figure, 1, a kettle body; 2. a top cover; 3. a communicating pipe; 4. an isolation valve; 5. a glass tube; 6. a discharge valve; 7. a sampling assembly; 701. an end cap; 702. a hollow sleeve; 703. winding a rod; 8. a partition plate; 9. a housing case; 10. a pressure release valve; 11. an internal thread sleeve; 12. a filter screen; 13. a movable groove; 14. a spring; 15. a round hole; 16. a flow hole; 17. a box rack; 18. a one-way valve; 19. pressing the sheet; 20. a magnetic block; 21. a metal block; 22. and (3) sealing rings.
Detailed Description
The present utility model will be described in further detail with reference to the drawings and examples, in order to make the objects, technical solutions and advantages of the present utility model more apparent. It should be understood that the specific embodiments described herein are for purposes of illustration only and are not intended to limit the scope of the utility model.
In the description of the present utility model, it should be understood that the terms "length," "width," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like indicate orientations or positional relationships based on the orientation or positional relationships shown in the drawings, merely to facilitate describing the present utility model and simplify the description, and do not indicate or imply that the devices or elements referred to must have a specific orientation, be configured and operated in a specific orientation, and therefore should not be construed as limiting the present utility model. Furthermore, in the description of the present utility model, the meaning of "a plurality" is two or more, unless explicitly defined otherwise.
Referring to fig. 1-6, the present utility model provides the following technical solutions: the utility model provides a reation kettle with sampling structure, including the cauldron body 1, top cap 2 is installed at the top of the cauldron body 1, and the outside bolt of the cauldron body 1 has communicating pipe 3, and the bottom of top communicating pipe 3 and the top of bottom communicating pipe 3 have all been bolted with isolation valve 4, and isolation valve 4 keeps away from one side swing joint of communicating pipe 3 has glass pipe 5, and discharge valve 6 is installed to the outside of glass pipe 5, and the top of top cap 2 is provided with sampling assembly 7, and the inboard swing joint of the bottom of the cauldron body 1 has division board 8, and the bottom swing joint of the cauldron body 1 has accommodation box 9;
the sampling assembly 7 comprises an end cap 701, the bottom of the end cap 701 being bolted with a hollow sleeve 702, the inside of the hollow sleeve 702 being bolted with a winding rod 703.
In this embodiment: through setting up the reaction space of cauldron body 1 cooperation top cap 2 as reagent, communicating pipe 3 cooperation isolation valve 4 and glass pipe 5 that set up, when needs take a sample reagent liquid, can open isolation valve 4, make reagent get into in the glass pipe 5, personnel can directly observe the inside reagent condition through glass pipe 5 this moment, and can discharge it through discharge valve 6 so that sample collection after closing isolation valve 4, sample subassembly 7 that sets up can be convenient for sample the floccule etc. that produce in the reagent in the cauldron body 1, can rotate the end cap 701 and make it become flexible from top cap 2 when using, and sample through hollow cover 702, floccule etc. twine easily on winding pole 703 so that sample collection, the partition plate 8 cooperation that sets up holds box 9, can be convenient for sample the reagent sediment of cauldron body 1 bottom, open the pollution that the cauldron body 1 top leads to when having avoided the sample, and can carry out the adjustment of sampling method to the content of required sample, it is comparatively nimble to use.
As a technical optimization scheme of the utility model, the top of the top cover 2 is provided with the pressure release valve 10, the top of the top cover 2 is provided with the internal thread sleeve 11, and the inner side of the internal thread sleeve 11 is in threaded connection with the end cap 701.
In this embodiment: by arranging the pressure release valve 10, the pressure in the inner space between the top cover 2 and the kettle body 1 can be conveniently removed, and the phenomenon that splash occurs during sampling or the glass tube 5 is broken due to overlarge pressure bearing is avoided.
As a technical optimization scheme of the utility model, the inner side of the isolation valve 4 is movably connected with a filter screen 12, and the isolation valve 4 is a butterfly valve.
In this embodiment: by providing the filter screen 12, it is possible to facilitate the filtration of the liquid passing through the isolation valve 4, avoiding that the precipitate or the like in the reagent is taken out at the time of sampling, or that the structure is blocked.
As a technical optimization scheme of the utility model, the bottom of the inner wall of the kettle body 1 is provided with a movable groove 13, the rear side of the inner side of the movable groove 13 is bolted with a spring 14, and the front side of the spring 14 is bolted with the isolation plate 8.
In this embodiment: through setting up movable slot 13 cooperation spring 14, can be convenient for promote division board 8 and make its shutoff at round hole 15 top, avoid taking place the condition of weeping.
As a technical optimization scheme of the utility model, a round hole 15 is formed in the bottom of the kettle body 1, and a flow hole 16 is formed in the top of the accommodating box 9.
In this embodiment: by providing the circular hole 15 in cooperation with the flow through hole 16, it is possible to facilitate the flow of the reagent into the housing box 9 through the circular hole 15 and the flow through hole 16 when sampling is required.
As a technical optimization scheme of the utility model, the bottom of the kettle body 1 is bolted with a box frame 17, and the inner side of the box frame 17 is in sliding connection with the accommodating box 9.
In this embodiment: through setting up box frame 17, can be convenient for to holding box 9 and cauldron body 1 and connect, avoid taking place the pine of structure when using and take place.
As a technical optimization scheme of the utility model, a magnetic block 20 is bolted to the rear side of the inner side of the box frame 17, a metal block 21 is bolted to the rear side of the accommodating box 9, and the metal block 21 and the magnetic block 20 are bonded.
In this embodiment: by arranging the magnetic block 20 and the metal block 21, the box frame 17 and the accommodating box 9 can be further connected conveniently, and the loosening is avoided when no external force is affected.
As a technical optimization scheme of the utility model, a sealing ring 22 is bolted to the top of the accommodating box 9, a pressing sheet 19 is bolted to the bottom of the isolation plate 8, the outer side of the pressing sheet 19 is matched with the sealing ring 22 for use, and a one-way valve 18 is bolted to the bottom of the accommodating box 9.
In this embodiment: through setting up sealing washer 22 and supporting the preforming 19 cooperation, sealing washer 22 can avoid holding the clearance between box 9 and the cauldron body 1 and take place liquid leakage, and the preforming 19 that supports that sets up can be convenient for make it drive division board 8 and remove so that round hole 15 exposes when sealing washer 22 promotes it to form the sampling space, the check valve 18 that sets up can be convenient for discharge inside reagent after taking down holding box 9.
Working principle: firstly, when sampling liquid, the isolation valve 4 is opened to enable reagent to enter the glass tube 5, at this time, personnel can directly observe the condition of the internal reagent through the glass tube 5, and after closing the isolation valve 4, the reagent can be discharged through the discharge valve 6 so as to be convenient for sampling and collecting, when sampling floccules and the like generated in the reagent in the kettle body 1, the end cap 701 is rotated to loosen the top cap 2, and sampling is carried out through the hollow sleeve 702, because the winding rod 703 connected with the end cap 701 is also rotated when rotating the end cap 701, the floccules and the like are easy to wind on the winding rod 703 so as to be convenient for sampling and collecting, and the arranged isolation plate 8 is matched with the containing box 9 so as to be convenient for sampling the reagent sediment at the bottom of the kettle body 1.
The foregoing description of the preferred embodiments of the utility model is not intended to be limiting, but rather is intended to cover all modifications, equivalents, and alternatives falling within the spirit and principles of the utility model.
Claims (8)
1. Reaction kettle with sampling structure, including the cauldron body (1), its characterized in that: the top cover (2) is installed at the top of the kettle body (1), communicating pipes (3) are bolted to the outer side of the kettle body (1), isolating valves (4) are bolted to the bottom of the top communicating pipes (3) and the top of the bottom communicating pipes (3), a glass pipe (5) is movably connected to one side, far away from the communicating pipes (3), of the isolating valves (4), a discharge valve (6) is installed on the outer side of the glass pipe (5), a sampling assembly (7) is arranged at the top of the top cover (2), an isolating plate (8) is movably connected to the inner side of the bottom of the kettle body (1), and a containing box (9) is movably connected to the bottom of the kettle body (1);
The sampling assembly (7) comprises an end cap (701), the bottom of the end cap (701) is bolted with a hollow sleeve (702), and the inner side of the hollow sleeve (702) is bolted with a winding rod (703).
2. The reaction kettle with a sampling structure according to claim 1, wherein: the top of top cap (2) is installed relief valve (10), internal thread cover (11) are installed at the top of top cap (2), the inboard of internal thread cover (11) and end cap (701) threaded connection.
3. The reaction kettle with a sampling structure according to claim 1, wherein: the inner side of the isolation valve (4) is movably connected with a filter screen (12), and the isolation valve (4) is a butterfly valve.
4. The reaction kettle with a sampling structure according to claim 1, wherein: the bottom of the inner wall of the kettle body (1) is provided with a movable groove (13), a spring (14) is bolted to the rear side of the inner side of the movable groove (13), and the front side of the spring (14) is bolted to the isolation plate (8).
5. The reaction kettle with a sampling structure according to claim 1, wherein: round holes (15) are formed in the bottom of the kettle body (1), and flow holes (16) are formed in the top of the accommodating box (9).
6. The reaction kettle with a sampling structure according to claim 1, wherein: the bottom of the kettle body (1) is bolted with a box frame (17), and the inner side of the box frame (17) is in sliding connection with the accommodating box (9).
7. The reactor with sampling structure according to claim 6, wherein: the rear side of the inner side of the box frame (17) is bolted with a magnetic block (20), the rear side of the accommodating box (9) is bolted with a metal block (21), and the metal block (21) is adhered with the magnetic block (20).
8. The reactor with sampling structure according to claim 7, wherein: the top bolt that holds box (9) has sealing washer (22), the bottom bolt of division board (8) has support preforming (19), the outside of support preforming (19) is used with sealing washer (22) cooperation, the bottom bolt that holds box (9) has check valve (18).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202420017134.3U CN221619408U (en) | 2024-01-03 | 2024-01-03 | Reaction kettle with sampling structure |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202420017134.3U CN221619408U (en) | 2024-01-03 | 2024-01-03 | Reaction kettle with sampling structure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN221619408U true CN221619408U (en) | 2024-08-30 |
Family
ID=92487252
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202420017134.3U Active CN221619408U (en) | 2024-01-03 | 2024-01-03 | Reaction kettle with sampling structure |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN221619408U (en) |
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2024
- 2024-01-03 CN CN202420017134.3U patent/CN221619408U/en active Active
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