CN221208031U - Pilot-scale experimental equipment for separating precipitation reaction from solid-liquid reactant - Google Patents
Pilot-scale experimental equipment for separating precipitation reaction from solid-liquid reactant Download PDFInfo
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- CN221208031U CN221208031U CN202322575832.3U CN202322575832U CN221208031U CN 221208031 U CN221208031 U CN 221208031U CN 202322575832 U CN202322575832 U CN 202322575832U CN 221208031 U CN221208031 U CN 221208031U
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- 239000007788 liquid Substances 0.000 title claims abstract description 73
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 55
- 238000001556 precipitation Methods 0.000 title claims abstract description 40
- 239000000376 reactant Substances 0.000 title claims abstract description 28
- 238000011020 pilot scale process Methods 0.000 title claims abstract description 21
- 239000000243 solution Substances 0.000 claims abstract description 57
- 238000000926 separation method Methods 0.000 claims abstract description 32
- 238000003756 stirring Methods 0.000 claims abstract description 24
- 230000005540 biological transmission Effects 0.000 claims abstract description 19
- 238000002347 injection Methods 0.000 claims abstract description 18
- 239000007924 injection Substances 0.000 claims abstract description 18
- 239000007787 solid Substances 0.000 claims abstract description 14
- 238000012360 testing method Methods 0.000 claims abstract description 9
- 238000002474 experimental method Methods 0.000 claims description 41
- 230000000149 penetrating effect Effects 0.000 claims description 6
- 238000007789 sealing Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000007790 scraping Methods 0.000 claims description 2
- 239000013049 sediment Substances 0.000 claims 3
- 238000000034 method Methods 0.000 abstract description 8
- 230000008569 process Effects 0.000 abstract description 6
- 230000009471 action Effects 0.000 description 3
- 238000004062 sedimentation Methods 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000001612 separation test Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model discloses pilot-scale experimental equipment for separating precipitation reaction from solid-liquid reactants, which comprises a fixed bottom plate, a fixed vertical frame, a precipitation solid-liquid pilot-scale experimental assembly and a precipitation solid-liquid separation assembly, wherein the precipitation solid-liquid pilot-scale experimental assembly comprises a rotating motor, a transmission rotating shaft, a pilot-scale experimental barrel body, a driven rotating shaft, a closed barrel cover, a liquid injection pipe, a solid injection funnel, a motor support, a stirring motor, a stirring transmission shaft and a stirring mixing rod, and the precipitation solid-liquid separation assembly comprises a solution discharge port, a solid-liquid separation filter screen, an outlet closed cover, a fixed seat chute, a fixed seat slide block, a solution barrel fixed seat, a reaction solution storage barrel, a reaction solution injection hopper and a reaction solution output pipe. The solid-liquid intermediate test component can realize the purpose of facilitating the uniform mixing reaction of the solid and the liquid in the test process, and the solid-liquid precipitation separation and transportation of the reactant after the test can be realized through the precipitation solid-liquid separation component.
Description
Technical Field
The utility model belongs to the technical field of pilot-scale experimental equipment, and particularly relates to pilot-scale experimental equipment for separating a precipitation reaction from a solid-liquid reactant.
Background
In the field of experimental research and production, precipitation reactions and separation of solid-liquid reactants are considered as relatively independent processes or technologies, and therefore, precipitation reactions and separation of solid-liquid substances are performed in different reactors and separation devices, respectively. However, such a separation test apparatus is inconvenient in carrying out a uniform mixing reaction of solid and liquid during an experiment and in carrying out a solid-liquid precipitation separation and transportation of the reactant after the experiment is completed, and thus, a pilot test apparatus for separating a precipitation reaction from a solid-liquid reactant is urgently required to solve the above-mentioned problems.
Disclosure of utility model
Aiming at the situation, in order to overcome the defects of the prior art, the utility model provides pilot-scale experimental equipment for separating a precipitation reaction from a solid-liquid reactant.
In order to realize the functions, the technical scheme adopted by the utility model is as follows: the utility model provides a pilot scale experimental facilities of precipitation reaction and solid-liquid reactant separation, includes PMKD, be connected with fixed grudging post on the PMKD, be connected with the pilot scale experimental subassembly of precipitation solid-liquid on the fixed grudging post, the rotating electrical machines of fixedly connected with on the fixed grudging post is included to the pilot scale experimental subassembly of precipitation solid-liquid, the output of rotating electrical machines is connected with the transmission pivot, be connected with pilot scale experiment staving in the transmission pivot, be connected with the driven pivot of rotating with fixed grudging post side wall on the pilot scale experiment staving lateral wall, the buckle is connected with the sealed bung on the pilot scale experiment staving, the fixedly connected with liquid injection pipe runs through on the sealed bung, the fixedly connected with puts in the funnel on the sealed bung, fixedly connected with stirring motor on the solid put in the funnel, stirring motor output is connected with stirring transmission shaft, fixedly connected with stirring mixing rod on the stirring transmission shaft, be connected with precipitation solid-liquid separation subassembly on the PMKD.
For smoothly realizing the purpose that conveniently carries out solid-liquid precipitation separation and transport to the reactant that the experiment was accomplished, precipitate solid-liquid separation subassembly includes the solution discharge port that pilot scale experiment staving lateral wall bottom through-connection had, the buckle is connected with the solid-liquid separation filter screen on the solution discharge port, the buckle is connected with the export closing cap on the solid-liquid separation filter screen, the fixing base spout that is equipped with on the PMKD, sliding connection has the fixing base slider on the fixing base spout, fixedly connected with solution bucket fixing base on the fixing base slider, fixedly connected with reaction solution deposits the bucket on the solution bucket fixing base, through-connection has the reaction solution injection bucket on the reaction solution deposits the bucket roof, through-connection has the reaction solution output tube on the reaction solution deposits the bucket lateral wall.
In order to achieve the purpose of conveniently checking reactant solution in real time, the side wall of the pilot experiment barrel body is connected with a transparent checking board, and the side wall of the reaction solution storage barrel is symmetrically connected with a transparent checking board.
Further, a sealing water leakage preventing strip is bonded and connected between the pilot-scale experiment barrel body and the closed barrel cover.
Further, the liquid injection pipe and the reaction solution output pipe are both rotatably connected with a bolt plug switch.
Wherein, be connected with the stave brush of striking off on the stirring transmission shaft.
Preferably, the fixing stand is arranged in an H shape, and the motor support is arranged in an L shape.
The beneficial effects obtained by the utility model by adopting the structure are as follows: according to the pilot scale experimental equipment for separating the precipitation reaction from the solid-liquid reactant, the purpose of carrying out uniform mixing reaction on the solid and the liquid in the experimental process can be achieved through the precipitation solid-liquid pilot scale experimental assembly, and the purpose of carrying out solid-liquid precipitation separation and transportation on the reactant subjected to the experiment can be achieved through the precipitation solid-liquid separation assembly.
Drawings
FIG. 1 is a schematic structural diagram of a pilot plant experimental facility for separating solid-liquid reactants from precipitation reactions according to the present solution;
FIG. 2 is a schematic view of another angle structure of a pilot plant for separating solid-liquid reactants from precipitation reaction according to the present embodiment;
Fig. 3 is a cross-sectional view of a pilot plant for separating solid-liquid reactants from precipitation reactions according to the present embodiment.
Wherein, 1, a fixed bottom plate, 2, a fixed vertical frame, 3, a sedimentation solid-liquid pilot experiment component, 4, a sedimentation solid-liquid separation component, 5, a rotating motor, 6, a transmission rotating shaft, 7, a pilot experiment barrel body, 8, a driven rotating shaft, 9, a closed barrel cover, 10, a liquid injection pipe, 11, a solid delivery funnel, 12 and a motor support, 13, stirring motors, 14, stirring transmission shafts, 15, stirring mixing rods, 16, a solution discharge port, 17, a solid-liquid separation filter screen, 18, an outlet closing cover, 19, a fixed seat chute, 20, a fixed seat slide block, 21, a solution barrel fixed seat, 22, a reaction solution storage barrel, 23, a reaction solution injection hopper, 24 and a reaction solution output pipe.
The accompanying drawings are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate the utility model and together with the embodiments of the utility model, serve to explain the utility model.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and fully with reference to the accompanying drawings, in which it is evident that the embodiments described are only some, but not all embodiments of the utility model; all other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
As shown in fig. 1-2, in order to realize the above functions, the technical scheme adopted by the utility model is as follows: the utility model provides a pilot plant experiment equipment of precipitation reaction and solid-liquid reactant separation, including fixed bottom plate 1, be connected with fixed grudging post 2 on the fixed bottom plate 1, fixed grudging post 2 is H shape setting, be connected with precipitation solid-liquid pilot plant experiment subassembly 3 on the fixed grudging post 2, precipitation solid-liquid pilot plant experiment subassembly 3 includes fixed rotating electrical machines 5 of fixed connection on the grudging post 2, the output of rotating electrical machines 5 is connected with transmission pivot 6, be connected with pilot plant experiment staving 7 on the transmission pivot 6, be connected with transparent viewing board on pilot plant experiment staving 7 lateral wall, be connected with on the pilot plant experiment staving 7 lateral wall with fixed grudging post 2 lateral wall rotation be connected with driven pivot 8, the buckle is connected with sealed bung 9 on the pilot plant experiment staving 7, be connected with sealed leak protection water strip between pilot plant experiment staving 7 and the sealed bung 9, run-through fixedly connected with liquid injection pipe 10 on the sealed bung 9, run-through is connected with solid input funnel 11 on the sealed bung 9, symmetrically connect with motor support 12 on the sealed bung 9, motor support 12 is L shape setting, be fixedly connected with motor 13 on the solid input stirring shaft 13, be connected with 14 on the fixed stirring shaft 14, be connected with the solid-liquid solid input drive shaft 14 on the stirring shaft is connected with the stirring rod 14.
As shown in fig. 1-2, the precipitation solid-liquid separation assembly 4 comprises a solution discharge port 16 penetrating through and connected with the bottom of the side wall of the pilot experiment barrel body 7, a solid-liquid separation filter screen 17 is connected to the solution discharge port 16 in a buckling manner, an outlet closing cover 18 is connected to the solid-liquid separation filter screen 17 in a buckling manner, a fixed seat sliding chute 19 is arranged on the fixed base plate 1, a fixed seat sliding block 20 is connected to the fixed seat sliding chute 19 in a sliding manner, a solution barrel fixed seat 21 is fixedly connected to the solution barrel fixed seat 21, a reaction solution storage barrel 22 is fixedly connected to the solution barrel fixed seat 21, transparent observation plates are symmetrically connected to the side wall of the reaction solution storage barrel 22, a reaction solution injection hopper 23 is connected to the top wall of the reaction solution storage barrel 22 in a penetrating manner, a reaction solution output pipe 24 is connected to the side wall of the reaction solution storage barrel 22 in a penetrating manner, and a bolt plug switch is connected to the liquid injection pipe 10 and the reaction solution output pipe 24 in a rotating manner.
When the device is specifically used, a user starts the rotating motor 5, the transmission rotating shaft 6 rotates along with the rotating shaft to drive the pilot experiment barrel 7 and the driven rotating shaft 8 to rotate, the rotating motor 5 is stopped when the pilot experiment barrel 7 rotates to an upward angle of the solution discharge port 16, then a bolt plug switch on the liquid injection pipe 10 is opened, pilot experiment solution is injected into the pilot experiment barrel 7 from the liquid injection pipe 10, solid reaction raw materials are put into the pilot experiment barrel 7 from the solid injection funnel 11, after the stirring motor 13 is started, the stirring transmission shaft 14 rotates along with the stirring transmission shaft to drive the stirring and mixing rod 15 to rotate, so that reactants in the pilot experiment barrel 7 can be uniformly mixed and stirred, meanwhile, a barrel wall scraping brush can scrape off reactants adhered on the inner wall of the pilot experiment barrel 7, after the pilot experiment is completed, the rotating motor 5 is started to adjust the angle of the pilot experiment barrel body 7 to a vertical angle, the fixed seat sliding block 20 and the solution barrel fixed seat 21 are moved along the fixed seat sliding groove 19, the reaction solution storage barrel 22 is moved to a position convenient for receiving solution to stop pushing, then the outlet sealing cover 18 is taken down from the solid-liquid separation filter screen 17, then the liquid in the pilot experiment barrel body 7 can be injected into the reaction solution storage barrel 22 through the reaction solution injection hopper 23 after being filtered by the solid-liquid separation filter screen 17, the solid is left in the pilot experiment barrel body 7, the bolt plug switch on the reaction solution output pipe 24 is opened to output the solution in the reaction solution storage barrel 22, and the above is all the using processes of the pilot experiment equipment for separating the whole precipitation reaction from the solid-liquid reactant.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.
The utility model and its embodiments have been described above with no limitation, and the actual construction is not limited to the embodiments of the utility model as shown in the drawings. In summary, if one of ordinary skill in the art is informed by this disclosure, a structural manner and an embodiment similar to the technical solution should not be creatively devised without departing from the gist of the present utility model.
Claims (7)
1. The utility model provides a pilot scale experimental facilities of precipitation reaction and solid-liquid reactant separation, includes fixed bottom plate, be connected with fixed grudging post on the fixed bottom plate, its characterized in that: the utility model discloses a solid-liquid separation device, including fixed riser, fixed riser is last to be connected with sediment solid-liquid pilot test experiment subassembly, sediment solid-liquid pilot test experiment subassembly includes fixed riser on fixedly connected rotating electrical machines, the output of rotating electrical machines is connected with the transmission pivot, be connected with pilot test experiment staving in the transmission pivot, be connected with the driven pivot of rotating with fixed riser one side wall on the pilot test experiment staving lateral wall, the buckle is connected with the sealed bung on the pilot test experiment staving, the fixedly connected with liquid injection pipe runs through on the sealed bung, the fixedly connected with solid puts in the funnel on the sealed bung, the symmetrically connected with motor support on the sealed bung, fixedly connected with agitator motor on the solid puts in the funnel, the agitator motor output is connected with stirring transmission shaft, fixedly connected with stirring and mixing rod on the stirring transmission shaft, be connected with sediment solid-liquid separation subassembly on the PMKD.
2. The pilot plant for separating solid-liquid reactants from precipitation reaction according to claim 1, wherein: the precipitation solid-liquid separation assembly comprises a solution discharge port which is connected with the bottom of the side wall of a pilot experiment barrel body in a penetrating manner, a solid-liquid separation filter screen is connected to the solution discharge port in a buckling manner, an outlet sealing cover is connected to the solid-liquid separation filter screen in a buckling manner, a fixing seat sliding groove is formed in a fixing base plate, a fixing seat sliding block is connected to the fixing seat sliding groove in a sliding manner, a solution barrel fixing seat is fixedly connected to the fixing seat sliding block, a reaction solution storage barrel is fixedly connected to the solution barrel fixing seat, a reaction solution injection bucket is connected to the top wall of the reaction solution storage barrel in a penetrating manner, and a reaction solution output pipe is connected to the side wall of the reaction solution storage barrel in a penetrating manner.
3. The pilot plant for separating solid-liquid reactants from precipitation reaction according to claim 2, wherein: transparent viewing plates are connected to the side wall of the pilot-plant experiment barrel body, and transparent viewing plates are symmetrically connected to the side wall of the reaction solution storage barrel.
4. A pilot plant for the separation of solid-liquid reactants from precipitation reactions according to claim 3, wherein: and a sealing water leakage preventing strip is bonded and connected between the pilot-scale experiment barrel body and the closed barrel cover.
5. The pilot plant for separating solid-liquid reactants from precipitation according to claim 4, wherein: the liquid injection pipe and the reaction solution output pipe are both rotationally connected with a bolt plug switch.
6. The pilot plant for separating solid-liquid reactants from precipitation according to claim 5, wherein: the stirring transmission shaft is connected with a barrel wall scraping brush.
7. The pilot plant for separating solid-liquid reactants from precipitation according to claim 6, wherein: the fixed vertical frame is H-shaped, and the motor support is L-shaped.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322575832.3U CN221208031U (en) | 2023-09-22 | 2023-09-22 | Pilot-scale experimental equipment for separating precipitation reaction from solid-liquid reactant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322575832.3U CN221208031U (en) | 2023-09-22 | 2023-09-22 | Pilot-scale experimental equipment for separating precipitation reaction from solid-liquid reactant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN221208031U true CN221208031U (en) | 2024-06-25 |
Family
ID=91577602
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202322575832.3U Active CN221208031U (en) | 2023-09-22 | 2023-09-22 | Pilot-scale experimental equipment for separating precipitation reaction from solid-liquid reactant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN221208031U (en) |
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2023
- 2023-09-22 CN CN202322575832.3U patent/CN221208031U/en active Active
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