CN221084692U - Production device for synthesizing gamma-undecalactone synthesized spice through rectification - Google Patents
Production device for synthesizing gamma-undecalactone synthesized spice through rectification Download PDFInfo
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- CN221084692U CN221084692U CN202323092302.XU CN202323092302U CN221084692U CN 221084692 U CN221084692 U CN 221084692U CN 202323092302 U CN202323092302 U CN 202323092302U CN 221084692 U CN221084692 U CN 221084692U
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- tower
- undecalactone
- rotating shaft
- pipe
- synthetic
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- PHXATPHONSXBIL-UHFFFAOYSA-N xi-gamma-Undecalactone Chemical compound CCCCCCCC1CCC(=O)O1 PHXATPHONSXBIL-UHFFFAOYSA-N 0.000 title claims abstract description 83
- PHXATPHONSXBIL-JTQLQIEISA-N gamma-Undecalactone Natural products CCCCCCC[C@H]1CCC(=O)O1 PHXATPHONSXBIL-JTQLQIEISA-N 0.000 title claims abstract description 40
- 229940020436 gamma-undecalactone Drugs 0.000 title claims abstract description 40
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 26
- 230000002194 synthesizing effect Effects 0.000 title claims abstract description 19
- 235000013599 spices Nutrition 0.000 title claims description 7
- 239000002304 perfume Substances 0.000 claims abstract description 34
- 238000001816 cooling Methods 0.000 claims description 21
- 239000002994 raw material Substances 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 15
- 230000005540 biological transmission Effects 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 8
- 238000009833 condensation Methods 0.000 claims description 7
- 230000005494 condensation Effects 0.000 claims description 7
- 238000012856 packing Methods 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- 239000012535 impurity Substances 0.000 description 5
- 241000220317 Rosa Species 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000011550 stock solution Substances 0.000 description 3
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000000484 citronellol Nutrition 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000010648 geranium oil Substances 0.000 description 1
- 235000019717 geranium oil Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
Abstract
The utility model discloses a production device for synthesizing gamma-undecalactone synthetic perfume through rectification, which comprises a rectifying tower and a condensing box, wherein the structure is reasonable.
Description
Technical Field
The utility model relates to the technical field of production and manufacture of peach aldehyde (gamma-undecalactone) synthetic perfume, in particular to a production device for rectifying and synthesizing peach aldehyde (gamma-undecalactone) synthetic perfume.
Background
The device for producing the synthesized gamma-undecalactone perfume by rectification is a rectifying tower, the rectification is a separation process for separating each component by utilizing different volatilities of each component in the mixture, common equipment comprises a plate rectifying tower and a packing rectifying tower, the principle and the equipment flow of the precise rectification are the same as those of the common rectification, and the relative volatilities among the components in a system to be separated are smaller (1.05-1.10), so that the separation and purification of the components to be separated are realized by adopting high-efficiency precise packing. In the case where there is often a coexistence of isomers in a natural essential oil, which is a raw material for producing an isolated perfume, for example, citronellol and rosmarinol which are coexistent in a natural essential oil such as geranium oil, rose grass oil and the like are optical isomers. The difference in boiling points of these isomers is relatively small, and it is difficult to achieve effective separation of such isolated fragrances using conventional rectification processes, so that precision rectification has wide application in the production of isolated fragrances. The high-efficiency packing used in the precision rectifying tower comprises a bulk packing such as Q-net ring packing, saddle packing and the like and a regular packing represented by silk-screen corrugated packing.
The existing production device for synthesizing gamma-undecalactone synthetic perfume by rectification has the following defects: when gamma-undecalactone synthetic perfume production manufacturing process, need to use the rectifying column to process, traditional rectifying column carries out steam treatment to liquid, generally adopt static mode to evaporate, and then lead to liquid to be heated unevenly, cause the slower condition of evaporation to take place, influence gamma-undecalactone synthetic perfume whole rectification reaction efficiency, simultaneously gamma-undecalactone synthetic perfume can exist partial granule impurity in the evaporation process, filter the processing in the relevant steam of evaporation gas is not adopted to the further quality after can greatly influencing gamma-undecalactone synthetic perfume production manufacturing, on the one hand reduced the result of use of rectifying the apparatus for producing gamma-undecalactone synthetic perfume, also direct influence the quality and the efficiency after the production of rectifying synthetic gamma-undecalactone synthetic perfume.
It is therefore necessary to develop a device for producing a synthetic perfume of gamma-undecalactone by rectification.
Disclosure of utility model
The utility model aims to provide a production device for synthesizing gamma-undecalactone synthetic perfume through rectification, which is provided with stirring paddles, a cooling pipe and filter paper, wherein the stirring paddles are correspondingly arranged on the outer walls of a rotating shaft A and a rotating shaft B, and are matched with a motor, so that raw materials for synthesizing the gamma-undecalactone synthetic perfume entering a rectifying tower are mixed and stirred by the motor-driven stirring paddles, tower kettle steam is matched during the process, the raw material steam efficiency for synthesizing the gamma-undecalactone synthetic perfume is improved, the cooling pipe is arranged on the outer wall of a condensing circulation pipe on a condensing box, the steam is subjected to condensed gas in the condensing circulation pipe, the temperature of the steam is accelerated, the cooled steam stock solution is filtered by a plurality of layers of filter papers in the filter box, the influence on the whole quality caused by a small amount of impurities in the steam stock solution is avoided as much as possible, the production device for synthesizing the gamma-undecalactone synthetic perfume through rectification is effectively improved in use effect, the quality and the production efficiency of the gamma-undecalactone synthetic perfume through rectification are also directly improved, and the problem that the production device for synthesizing the gamma-undecalactone synthetic perfume through rectification is poor in quality is solved in the background technology.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the production device for synthesizing the gamma-undecalactone synthesized perfume by rectification comprises a rectification tower and a condensing box, wherein a top steam pipe is arranged at the center of the top of the rectification tower, a tower seat is arranged at the bottom of the rectification tower, and a connecting pipeline is arranged at the top of the condensing box;
The filter tank is installed at the bottom of the condensing box.
Preferably, a raw material pipe is arranged above the outer wall of one side of the rectifying tower, a tower kettle steam pipe is arranged below the outer wall of one side of the rectifying tower, and a tower bottom discharge pipe is arranged at the front end and the rear end of the bottom of the rectifying tower.
Preferably, a motor is installed on one side of the bottom of the tower base, and an output shaft on the motor is fixedly connected with the bottom end of the rotating shaft A through a coupler.
Preferably, a belt pulley A is arranged below the outer wall of the rotating shaft A, a rotating shaft B is rotatably connected to one side of the inside of the tower seat, and a belt pulley B is arranged below the outer wall of the rotating shaft B.
Preferably, the belt pulley B is in transmission connection with the belt pulley A through a transmission belt, and stirring paddles are arranged above the outer walls of the rotating shaft B and the rotating shaft A.
Preferably, one end of the connecting pipeline is fixedly connected with the top end of the tower top steam pipe, a condensation circulating pipe is arranged on one side of the interior of the condensing box, and a cooling pipe is arranged on the outer wall of the condensation circulating pipe.
Preferably, the filter plate is installed to inside below of rose box, the top of filter is provided with filter paper, filter paper is established into two sets of, the liquid outlet has been seted up to the bottom central point of rose box.
Compared with the prior art, the utility model has the beneficial effects that:
Through being equipped with stirring rake, cooling tube and filter paper, set up the stirring rake on the outer wall of pivot A and pivot B with the cooperation motor, make the raw materials that get into the gamma-undecalactone synthetic spice in the rectifying column used, mix the stirring by motor drive stirring rake to the raw materials, cooperate tower cauldron steam during this, improve the used raw materials steam efficiency of gamma-undecalactone synthetic spice, through setting up the cooling tube on the condensation circulation pipe outer wall on the condenser tank, make steam receive the condensation gas in the condensation circulation pipe, can accelerate to steam cooling, the steam stoste after waiting to cool down is filtered by multilayer filter paper in the filter tank, avoid a small amount of impurity to influence whole quality in the steam stoste as far as possible, the effectual apparatus for producing the synthetic spice of rectifying gamma-undecalactone has improved the result of use, also directly improved the quality and the production efficiency of the synthetic spice of rectifying gamma-undecalactone.
Drawings
FIG. 1 is a front cross-sectional view of the present utility model;
FIG. 2 is a front view of the present utility model;
FIG. 3 is an enlarged view of the structure shown in FIG. 1;
FIG. 4 is an enlarged view of the structure at B in FIG. 1 provided by the present utility model;
Fig. 5 is a perspective view of a part of the structure provided by the utility model.
In the figure: 1. a rectifying tower; 101. a raw material pipe; 102. a tower kettle steam pipe; 103. a bottom discharge pipe; 104. a top steam pipe; 2. a tower base; 201. a motor; 202. a rotating shaft A; 203. a belt pulley A; 204. a rotating shaft B; 205. a belt pulley B; 206. stirring paddles; 3. a condensing box; 301. a connecting pipe; 302. a condensing circulation pipe; 303. a cooling tube; 4. a filter box; 401. a filter plate; 402. a filter paper; 403. and a liquid outlet.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
The utility model provides the following technical scheme: the production device for synthesizing the peach aldehyde (gamma-undecalactone) synthesized perfume through rectification can effectively improve the use effect and efficiency of the production device for synthesizing the gamma-undecalactone synthesized perfume through rectification in the use process, a stirring paddle 206, a cooling pipe 303 and a filter paper 402 are added, referring to figures 1-5, the production device comprises a rectification tower 1 and a condensing box 3, a raw material pipe 101 is arranged above one side outer wall of the rectification tower 1, a tower kettle steam pipe 102 is arranged below one side outer wall of the rectification tower 1, a tower bottom discharge pipe 103 is arranged at the front end and the rear end of the bottom of the rectification tower 1, a tower top steam pipe 104 is arranged at the center of the top of the rectification tower 1, a tower seat 2 is arranged at the bottom of the rectification tower 1, a motor 201 is arranged at one side of the bottom of the tower seat 2, an output shaft on the motor 201 is fixedly connected with the bottom end of a rotating shaft A202 through a coupling, the motor 201 can drive and control the rotating shaft A202 to rotate positively or reversely, the belt pulley A203 is arranged below the outer wall of the rotating shaft A202, the rotating shaft B204 is rotationally connected to one side of the inside of the tower seat 2, the belt pulley B205 is arranged below the outer wall of the rotating shaft B204, the belt pulley B205 is connected with the belt pulley A203 through transmission belt transmission, the rotating shaft A202 can synchronously drive the rotating shaft B204 to rotate positively or reversely, the stirring paddles 206 are arranged above the outer walls of the rotating shaft B204 and the rotating shaft A202, a plurality of groups of stirring paddles 206 are correspondingly arranged on the outer walls of the rotating shaft B204 and the rotating shaft A202, the rotating paddles 206 can be synchronously driven to rotate, raw materials used for synthesizing perfume by gamma-undecalactone entering the rectifying tower 1 are mixed and stirred by the motor 201, and high-temperature steam entering the steam pipe 102 of the tower kettle is matched during the mixing process, the raw material steam efficiency of gamma-undecalactone synthetic perfume can be improved, two groups of tower bottom discharge pipes 103 are arranged at the same time and correspondingly arranged at the front end and the rear end of the bottom of the rectifying tower 1, so that the belt transmission connection between a belt pulley A203 and a belt pulley B205 is not affected, a connecting pipe 301 is arranged at the top of a condensing box 3, one end of the connecting pipe 301 is fixedly connected with the top end of a tower top steam pipe 104, a condensing circulating pipe 302 is arranged at one side of the interior of the condensing box 3, a cooling pipe 303 is arranged on the outer wall of the condensing circulating pipe 302, the connecting pipe 301 on the condensing box 3 is communicated with the tower top steam pipe 104 on the rectifying tower 1, the top end of the cooling pipe 303 on the condensing circulating pipe 302 is communicated with the connecting pipe 301, steam in the rectifying tower 1 enters the cooling pipe 303 through the connecting pipe 301, and then is matched with condensed gas in the condensing circulating pipe 302, the steam generated by raw material in the rectifying tower 1 can be cooled, the cooling treatment can be effectively slowed down by adopting a spiral state to the cooling pipe, the flow of the effective steam gas can be contacted with the condensed gas 302 uniformly, and the cooling efficiency of the raw material can be improved;
The filter tank 4 is installed to the bottom of the condensing tank 3, the filter plate 401 is installed to the inside below of filter tank 4, filter paper 402 is provided with at the top of filter plate 401, filter paper 402 is established to two sets of, liquid outlet 403 has been seted up to the bottom central point of filter tank 4, lay two sets or multiunit filter paper 402 with the filter plate 401 surface on the filter tank 4, make the steam after the cooling, drip on filter paper 402 surface in the form of liquid, adopt fine filtration by filter paper 402 again, avoid containing a little impurity in the steam stoste and influencing whole quality as far as possible.
Working principle: when the utility model is used, the motor 201 is arranged on the tower seat 2 on the bottom of the rectifying tower 1, the output shaft on the motor 201 is provided with the rotating shaft A202 by the coupler, the motor 201 can drive and control the rotating shaft A202 to rotate positively or reversely, the rotating shaft B204 is arranged on one side of the interior of the tower seat 2 in a rotating connection mode, the belt pulley B205 on the rotating shaft B204 is connected with the belt pulley A203 on the rotating shaft A202 by a transmission belt in a transmission way, the rotating shaft A202 rotates positively or reversely, the rotating shaft B204 can be synchronously driven to rotate positively or reversely, the rotating shaft B204 and the rotating shaft A202 are correspondingly provided with a plurality of groups of stirring paddles 206, the rotating shaft B204 and the rotating shaft A202 can be synchronously driven to rotate, raw materials used for synthesizing perfume by gamma-undecalactone entering the rectifying tower 1 are driven by the motor 201 to mix and stir the raw materials, and high-temperature steam entering the tower kettle steam pipe 102 is matched during the mixing process, the efficiency of raw material steam used by gamma-undecalactone synthetic perfume can be improved, two groups of tower bottom discharge pipes 103 are arranged at the front end and the rear end of the bottom of the rectifying tower 1, the belt transmission connection between the belt pulley A203 and the belt pulley B205 is not affected, the connecting pipeline 301 on the condensing box 3 is connected with the tower top steam pipe 104 on the rectifying tower 1, the top end of the cooling pipe 303 on the condensing circulating pipe 302 is connected with the connecting pipeline 301, the steam in the rectifying tower 1 enters the cooling pipe 303 through the connecting pipeline 301, the condensing gas in the condensing circulating pipe 302 is matched, the cooling treatment of the steam generated by raw materials in the rectifying tower 1 can be achieved, the flowing speed of the steam gas can be effectively slowed down by adopting a spiral state to the cooling pipe 303, the steam gas can be effectively ensured to be uniformly contacted with the condensed gas emitted by the condensing pipe 302, the raw material steam cooling efficiency is improved, the filter box 4 is arranged at the bottom of the condensing box 3, two or more groups of filter papers 402 are paved on the surface of the filter plate 401 on the filter box 4, so that cooled steam is dripped on the surface of the filter papers 402 in a liquid state, fine filtration is performed by the filter papers 402, the influence on the whole quality caused by the fact that a small amount of impurities are contained in a steam stock solution is avoided as much as possible, the using effect of the production device for synthesizing gamma-undecalactone synthetic perfume through rectification is improved, and the quality and the production efficiency of synthesizing gamma-undecalactone synthetic perfume through rectification are also directly improved.
Although the utility model has been described hereinabove with reference to embodiments, various modifications thereof may be made and equivalents may be substituted for elements thereof without departing from the scope of the utility model. In particular, the features of the disclosed embodiments may be combined with each other in any manner so long as there is no structural conflict, and the exhaustive description of these combinations is not given in this specification merely for the sake of brevity and resource saving. Therefore, it is intended that the utility model not be limited to the particular embodiment disclosed, but that the utility model will include all embodiments falling within the scope of the appended claims.
Claims (7)
1. The utility model provides a production device of synthetic spices of rectifying and synthesizing gamma-undecalactone, includes rectifying column (1) and condensing chamber (3), top central point of rectifying column (1) puts and is provided with top of the tower steam pipe (104), its characterized in that: a tower seat (2) is arranged at the bottom of the rectifying tower (1), and a connecting pipeline (301) is arranged at the top of the condensing box (3);
the bottom of the condensing box (3) is provided with a filter box (4).
2. The apparatus for producing a synthetic γ -undecalactone perfume by rectification according to claim 1, wherein: a raw material pipe (101) is arranged above one side outer wall of the rectifying tower (1), a tower kettle steam pipe (102) is arranged below one side outer wall of the rectifying tower (1), and a tower bottom discharge pipe (103) is arranged at the front end and the rear end of the bottom of the rectifying tower (1).
3. The apparatus for producing a synthetic γ -undecalactone perfume by rectification according to claim 1, wherein: a motor (201) is arranged at one side of the bottom of the tower base (2), and an output shaft on the motor (201) is fixedly connected with the bottom end of the rotating shaft A (202) through a coupler.
4. A production apparatus for synthesizing gamma-undecalactone synthetic perfume by rectification as claimed in claim 3, wherein: the belt pulley A (203) is arranged below the outer wall of the rotating shaft A (202), the rotating shaft B (204) is rotatably connected to one side of the inside of the tower base (2), and the belt pulley B (205) is arranged below the outer wall of the rotating shaft B (204).
5. The apparatus for producing a synthetic γ -undecalactone perfume by rectification according to claim 4, wherein: the belt pulley B (205) is in transmission connection with the belt pulley A (203) through a transmission belt, and stirring paddles (206) are arranged above the outer walls of the rotating shaft B (204) and the rotating shaft A (202).
6. The apparatus for producing a synthetic γ -undecalactone perfume by rectification according to claim 1, wherein: one end of the connecting pipeline (301) is fixedly connected with the top end of the tower top steam pipe (104), a condensation circulating pipe (302) is arranged on one side of the interior of the condensing box (3), and a cooling pipe (303) is arranged on the outer wall of the condensation circulating pipe (302).
7. The apparatus for producing a synthetic γ -undecalactone perfume by rectification according to claim 1, wherein: the filter is characterized in that a filter plate (401) is arranged below the inside of the filter box (4), filter paper (402) is arranged at the top of the filter plate (401), the filter paper (402) is arranged into two groups, and a liquid outlet (403) is formed in the center of the bottom of the filter box (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202323092302.XU CN221084692U (en) | 2023-11-15 | 2023-11-15 | Production device for synthesizing gamma-undecalactone synthesized spice through rectification |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202323092302.XU CN221084692U (en) | 2023-11-15 | 2023-11-15 | Production device for synthesizing gamma-undecalactone synthesized spice through rectification |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN221084692U true CN221084692U (en) | 2024-06-07 |
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ID=91318484
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202323092302.XU Active CN221084692U (en) | 2023-11-15 | 2023-11-15 | Production device for synthesizing gamma-undecalactone synthesized spice through rectification |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN221084692U (en) |
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2023
- 2023-11-15 CN CN202323092302.XU patent/CN221084692U/en active Active
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