CN220990808U - Dibromohexane preparation facilities - Google Patents
Dibromohexane preparation facilities Download PDFInfo
- Publication number
- CN220990808U CN220990808U CN202322599884.4U CN202322599884U CN220990808U CN 220990808 U CN220990808 U CN 220990808U CN 202322599884 U CN202322599884 U CN 202322599884U CN 220990808 U CN220990808 U CN 220990808U
- Authority
- CN
- China
- Prior art keywords
- fixedly connected
- dibromohexane
- block
- alcohol lamp
- clamping
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- SAWCWRKKWROPRB-UHFFFAOYSA-N 1,1-dibromohexane Chemical compound CCCCCC(Br)Br SAWCWRKKWROPRB-UHFFFAOYSA-N 0.000 title claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 33
- 238000003756 stirring Methods 0.000 claims abstract description 31
- 238000004140 cleaning Methods 0.000 claims description 7
- 239000000126 substance Substances 0.000 abstract description 3
- 239000000463 material Substances 0.000 description 15
- 239000007788 liquid Substances 0.000 description 4
- 230000006978 adaptation Effects 0.000 description 3
- 239000012295 chemical reaction liquid Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000011435 rock Substances 0.000 description 2
- 239000002051 C09CA08 - Olmesartan medoxomil Substances 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229960001199 olmesartan medoxomil Drugs 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- -1 triphenyl olmesartan medoxomil compound Chemical class 0.000 description 1
Landscapes
- Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)
Abstract
The utility model discloses a dibromohexane preparation device, which relates to the technical field of chemical preparation and comprises a base, a shell arranged at the top of the base, a door body arranged on the surface of the shell, and an alcohol lamp arranged in the shell, wherein a clamping mechanism is arranged at the bottom of the alcohol lamp and on the surface of the shell, the clamping mechanism comprises an air pump, the output end of the air pump is fixedly connected with a pushing block, the other end of the positioning block is fixedly connected with a clamping block, and the clamping block is connected with a movable plate through the positioning block. According to the dibromohexane preparation device provided by the utility model, the door body is opened to place the alcohol lamp on the surfaces of the inner sides of the two groups of clamping blocks, then the air pump is started to enable the output end of the air pump to push the pushing block to drive the movable plate to slide on the surface of the sliding block until the alcohol lamp is completely clamped, so that the purpose of clamping the alcohol lamp is achieved, and the problem that the alcohol lamp is deviated due to shaking caused by larger amplitude when the stirring mechanism is operated is further solved.
Description
Technical Field
The utility model relates to the technical field of chemical preparation, in particular to a dibromohexane preparation device.
Background
There are many organic compounds in the chemical field, dibromohexane is one of them, which can also be called ethylene dibromo, and the appearance is colorless transparent liquid, mainly used as a solvent.
The Chinese patent with the publication number of CN216024822U discloses equipment for preparing the triphenyl olmesartan medoxomil compound, a stirring motor drives a stirring fan blade to rotate, so that raw liquid is mixed more uniformly, the phenomenon that reaction liquid is layered up and down due to standing is prevented, the quality of products is effectively improved, the practicability of the equipment is enhanced, the reaction liquid in the equipment can be prevented from being extruded from a liquid inlet when a module is hydraulically pressed through a sealing mechanism, the preparation yield of the compound is increased, after the reaction liquid is injected into the module, a fixed block at the upper end can be buckled, a cover plate is driven to move together, the liquid inlet is sealed, the preparation cost of the compound is effectively reduced, the equipment is convenient for people to use, and a better application prospect is brought.
When preparing dibromohexane, generally, firstly place the material that needs to use in the inside of container, use alcohol lamp to heat the bottom of container afterwards, the intensive mixing that the rethread rabbling mechanism carried out the material, but because the container is generally directly placed on the tray at alcohol lamp top, stirring mechanism if the range is too big probably can lead to the alcohol lamp to rock and cause its angular displacement, lead to the material in the container to be heated unevenly and influence preparation effect.
Disclosure of utility model
The present utility model has been made in view of the above-mentioned problems occurring in the prior art.
Therefore, the utility model aims to provide a dibromohexane preparation device, which solves the problem that when a stirring mechanism works, the stirring mechanism can cause the shaking of an alcohol lamp to cause uneven heating of materials in a container due to overlarge amplitude.
In order to achieve the above object, the present utility model provides the following technical solutions:
The utility model provides a dibromohexane preparation facilities, includes the base, is located the cover shell at the base top, installs at the door body on cover shell surface, is located the inside alcohol burner of cover shell, the bottom of alcohol burner and the surface mounting who is located the cover shell have fixture, fixture includes the air pump, the output fixedly connected with impeller, the one end of impeller is connected with pivot and fly leaf, the fly leaf is located the surface of impeller, the fly leaf is connected through the pivot with impeller, the other end of fly leaf is connected with the locating piece, the other end fixedly connected with grip block of locating piece, the grip block is connected through the locating piece with the fly leaf, the spout with slider looks adaptation is seted up to the bottom of grip block and is located the surface fixedly connected with slider of cover shell, and the spout with slider looks adaptation is all connected with fly leaf, impeller, pivot and air pump and mutual symmetry, and can hold in the alcohol burner's bottom adaptation and can carry out the grip block through the grip block to avoid because the stirring mechanism range is too big and lead to its problem that produces to rock.
Preferably, the top of the casing is connected with a fixing ring, a container is arranged at the top of the fixing ring, a stirring mechanism is arranged in the container, and clamping grooves which are mutually matched with the container and the casing are formed in the top and the bottom of the fixing ring.
Preferably, the stirring mechanism comprises a motor positioned at the top of the container, the output end of the motor penetrates through the container and is fixedly connected with a rotating rod, the surface of the rotating rod is fixedly connected with a stirring rod with an annular array, a cleaning brush is arranged at the bottom of the stirring rod, the stirring mechanism can uniformly stir materials in the container to enable the materials to be better fused, and the cleaning brush can prevent the bottom of the container from precipitating.
Preferably, the top of container is equipped with rubber buffer and outlet duct, the surface of base still is connected with the fixed column, the surface of fixed column is equipped with the swiveling ring, one side fixedly connected with connecting rod A of swiveling ring, connecting rod A's the other end is connected with the outlet duct, and the bottom of swiveling ring just is located the fixed column the fixed surface of fixed column fixedly connected with spacing collar, and swiveling ring can drive connecting rod A and make the outlet duct rotate at the surface of spacing collar.
Further, the inboard of fixed column is equipped with the telescopic link, the top fixedly connected with connecting rod B of telescopic link, the telescopic link can make the retainer plate go up and down.
Preferably, the other end of the connecting rod B is fixedly connected with the fixed ring, the fixed ring is connected with the fixed column through the connecting rod B, guide rails which are mutually matched are arranged on two sides of the connecting rod B and on the inner side of the fixed column, and the connecting rod B can be stably lifted.
In the technical scheme, the utility model has the technical effects and advantages that:
1. According to the utility model, the clamping mechanism is arranged, when the alcohol lamp is used, the door body is opened to place the alcohol lamp on the inner side surfaces of the two groups of clamping blocks, then the air pump is started to enable the output end of the alcohol lamp to push the pushing block to drive the movable plate to slide on the surface of the sliding block until the alcohol lamp is clamped completely, so that the purpose of clamping the alcohol lamp is achieved, and the problem that the alcohol lamp is deviated due to shaking of the alcohol lamp caused by large amplitude when the stirring mechanism is used is further solved.
2. In addition, the cleaning brush is arranged at the bottom of a group of stirring rods at the bottom of the rotating rod, so that the phenomenon that the materials are precipitated in the stirring process can be effectively prevented, and the aim of fully fusing the materials is further achieved.
Drawings
In order to more clearly illustrate the embodiments of the present utility model or the technical solutions in the prior art, the drawings required for the embodiments will be briefly described below, and it is apparent that the drawings in the following description are only some embodiments described in the present utility model, and other drawings may be obtained according to these drawings for a person having ordinary skill in the art.
FIG. 1 is a schematic perspective view of the present utility model;
FIG. 2 is a structural representation of the present utility model;
FIG. 3 is a cross-sectional perspective view of the present utility model;
FIG. 4 is a schematic view of a clamping assembly according to the present utility model;
fig. 5 is a schematic structural view of the stirring mechanism of the present utility model.
Reference numerals illustrate:
1. A base; 2. a casing; 3. a door body; 4. an alcohol lamp; 5. an air pump; 6. a pushing block; 7. a movable plate; 8. a rotating shaft; 9. a clamping block; 10. a positioning block; 11. a fixing ring; 12. a container; 13. a stirring rod; 14. a cleaning brush; 15. a rotating rod; 16. a motor; 17. a rubber stopper; 18. an air outlet pipe; 19. fixing the column; 20. a rotating ring; 21. a connecting rod A; 22. a telescopic rod; 23. a connecting rod B; 24. a sliding block.
Detailed Description
In order to make the technical scheme of the present utility model better understood by those skilled in the art, the present utility model will be further described in detail with reference to the accompanying drawings.
The embodiment of the utility model discloses a dibromohexane preparation device.
The utility model provides a dibromohexane preparation device as shown in figures 1-5, which comprises a base 1, a shell 2 positioned at the top of the base 1, a door body 3 arranged on the surface of the shell 2, an alcohol lamp 4 positioned in the shell 2, wherein a clamping mechanism is arranged at the bottom of the alcohol lamp 4 and positioned on the surface of the shell 2, the clamping mechanism comprises an air pump 5, the output end of the air pump 5 is fixedly connected with a pushing block 6, one end of the pushing block 6 is connected with a rotating shaft 8 and a movable plate 7, the movable plate 7 is positioned on the surface of the pushing block 6, the movable plate 7 is connected with the pushing block 6 through the rotating shaft 8, the other end of the movable plate 7 is connected with a positioning block 10, the other end of the positioning block 10 is fixedly connected with a clamping block 9, the bottom of the clamping block 9 is fixedly connected with a sliding block 24 positioned on the surface of the shell 2, the clamping block 9 is connected with the movable plate 7 through the positioning block 10, the top of the shell 2 is connected with a fixed ring 11, the top of the fixed ring 11 is provided with a container 12, and the inside of the container 12 is provided with a stirring mechanism.
When the alcohol lamp 4 is clamped, the door body 3 is firstly opened to place the alcohol lamp 4 on the inner side surfaces of the two groups of clamping blocks 9, then the air pump 5 is started to enable the output end of the alcohol lamp 4 to push the pushing block 6 to drive the movable plate 7 to slide on the surface of the sliding block 24, and the pushing block 6 is movably connected with the movable plate 7 through the rotating shaft 8, so that when the air pump 5 is started, the output end of the air pump 5 can enable the pushing block 6 to be extruded forwards, and meanwhile, the two groups of movable plates 7 are driven to move towards the center of the air pump 5 and the two groups of clamping blocks 9 are driven to move along the surface of the sliding block 24 until the alcohol lamp 4 is completely clamped, so that the purpose of clamping the alcohol lamp 4 is achieved, and the problem that the alcohol lamp 4 is deviated due to shaking of the large amplitude of the stirring mechanism in operation is further solved.
For material fusion, as shown in fig. 2, 3 and 5, the stirring mechanism comprises a motor 16 positioned at the top of the container 12, the output end of the motor 16 penetrates through the container 12 to be fixedly connected with a rotary rod 15, the surface of the rotary rod 15 is fixedly connected with a stirring rod 13 in an annular array, and a cleaning brush 14 is arranged at the bottom of the stirring rod 13.
When stirring the material, start motor 16 makes rotary rod 15 drive puddler 13 and rotates to alright reach the purpose that makes the material carry out intensive mixing, in addition, because the bottom of rotary rod 15 bottommost a set of puddler 13 is equipped with cleaning brush 14, can effectually prevent the phenomenon that the material can deposit in the in-process of stirring, further reached the purpose that makes the material carry out intensive mixing.
Finally, for the smoothness of operation, as shown in fig. 1-2, a rubber plug 17 and an air outlet pipe 18 are arranged at the top of the container 12, a fixing column 19 is further connected to the surface of the base 1, a rotating ring 20 is arranged on the surface of the fixing column 19, a connecting rod A21 is fixedly connected to one side of the rotating ring 20, the other end of the connecting rod A21 is connected with the air outlet pipe 18, a telescopic rod 22 is arranged on the inner side of the fixing column 19, a connecting rod B23 is fixedly connected to the top of the telescopic rod 22, the other end of the connecting rod B23 is fixedly connected with the fixing ring 11, and the fixing ring 11 is connected with the fixing column 19 through the connecting rod B23.
When dibromohexane is prepared, firstly, the rubber plug 17 is opened to pour the material into the container 12, after pouring, the rubber plug 17 is installed back, then the connecting rod A21 drives the air outlet pipe 18 to rotate by rotating the rotating ring 20, the air outlet pipe 18 is connected with the container 12 after rotating, then the alcohol lamp 4 is fixed by the clamping mechanism, and then the stirring mechanism stirs the material in the container 12.
The connecting rod B23 can be driven by the telescopic rod 22, so that the fixing ring 11 drives the container 12 to adjust the distance between the container 12 and the alcohol lamp 4, and the temperature can be controlled.
While certain exemplary embodiments of the present utility model have been described above by way of illustration only, it will be apparent to those of ordinary skill in the art that modifications may be made to the described embodiments in various different ways without departing from the spirit and scope of the utility model. Accordingly, the drawings and description are to be regarded as illustrative in nature and not as restrictive of the scope of the utility model, which is defined by the appended claims.
Claims (6)
1. The dibromohexane preparation device comprises a base (1), a casing (2) positioned at the top of the base (1), a door body (3) arranged on the surface of the casing (2) and an alcohol lamp (4) positioned in the casing (2), and is characterized in that a clamping mechanism is arranged at the bottom of the alcohol lamp (4) and positioned on the surface of the casing (2);
The clamping mechanism comprises an air pump (5), the output end of the air pump (5) is fixedly connected with a pushing block (6), one end of the pushing block (6) is connected with a rotating shaft (8) and a movable plate (7), the movable plate (7) is located on the surface of the pushing block (6), the movable plate (7) is connected with the pushing block (6) through the rotating shaft (8), the other end of the movable plate (7) is connected with a positioning block (10), the other end of the positioning block (10) is fixedly connected with a clamping block (9), the clamping block (9) is connected with the movable plate (7) through the positioning block (10), and the bottom of the clamping block (9) is fixedly connected with a sliding block (24) located on the surface of the casing (2).
2. The dibromohexane preparation device according to claim 1, wherein a fixing ring (11) is connected to the top of the jacket (2), a container (12) is provided at the top of the fixing ring (11), and a stirring mechanism is provided inside the container (12).
3. The dibromohexane preparation device according to claim 2, wherein the stirring mechanism comprises a motor (16) positioned at the top of the container (12), an output end of the motor (16) penetrates through the container (12) to be fixedly connected with a rotating rod (15), a stirring rod (13) in an annular array is fixedly connected to the surface of the rotating rod (15), and a cleaning brush (14) is arranged at the bottom of the stirring rod (13).
4. The dibromohexane preparation device according to claim 3, wherein a rubber plug (17) and an air outlet pipe (18) are arranged at the top of the container (12), a fixing column (19) is further connected to the surface of the base (1), a rotating ring (20) is arranged on the surface of the fixing column (19), a connecting rod A (21) is fixedly connected to one side of the rotating ring (20), and the other end of the connecting rod A (21) is connected with the air outlet pipe (18).
5. The dibromohexane preparation device according to claim 4, wherein a telescopic rod (22) is arranged on the inner side of the fixed column (19), and a connecting rod B (23) is fixedly connected to the top of the telescopic rod (22).
6. The dibromohexane preparation device according to claim 5, wherein the other end of the connecting rod B (23) is fixedly connected with a fixing ring (11), and the fixing ring (11) is connected with a fixing column (19) through the connecting rod B (23).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202322599884.4U CN220990808U (en) | 2023-09-25 | 2023-09-25 | Dibromohexane preparation facilities |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202322599884.4U CN220990808U (en) | 2023-09-25 | 2023-09-25 | Dibromohexane preparation facilities |
Publications (1)
Publication Number | Publication Date |
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CN220990808U true CN220990808U (en) | 2024-05-24 |
Family
ID=91090257
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202322599884.4U Active CN220990808U (en) | 2023-09-25 | 2023-09-25 | Dibromohexane preparation facilities |
Country Status (1)
Country | Link |
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CN (1) | CN220990808U (en) |
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2023
- 2023-09-25 CN CN202322599884.4U patent/CN220990808U/en active Active
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