CN220736229U - Horizontal rotary evaporation separation device - Google Patents
Horizontal rotary evaporation separation device Download PDFInfo
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- CN220736229U CN220736229U CN202322117864.9U CN202322117864U CN220736229U CN 220736229 U CN220736229 U CN 220736229U CN 202322117864 U CN202322117864 U CN 202322117864U CN 220736229 U CN220736229 U CN 220736229U
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- inner cylinder
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- cylinder
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- 238000002390 rotary evaporation Methods 0.000 title claims abstract description 19
- 238000000926 separation method Methods 0.000 title claims abstract description 14
- 230000007246 mechanism Effects 0.000 claims abstract description 19
- 238000007599 discharging Methods 0.000 claims description 42
- 238000010438 heat treatment Methods 0.000 claims description 19
- 238000002347 injection Methods 0.000 claims description 9
- 239000007924 injection Substances 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 3
- 239000002994 raw material Substances 0.000 abstract description 34
- 238000001704 evaporation Methods 0.000 description 10
- 230000008020 evaporation Effects 0.000 description 10
- 238000000034 method Methods 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a horizontal rotary evaporation separation device which comprises a support frame and an outer cylinder, wherein the support frame is fixed on the outer side of the outer cylinder, an inner cylinder is movably embedded in the outer cylinder, a first pipeline is movably sleeved on one side of the inner cylinder, a rotating mechanism which is convenient for driving the inner cylinder to rotate is arranged on one side of the first pipeline, a first supporting block is fixedly arranged on one side of the outer cylinder, the first supporting block is fixed on the outer side of the first pipeline, a second pipeline is movably sleeved on the other side of the inner cylinder, and a second supporting block is fixedly arranged on one side of the outer cylinder. When the utility model is used, raw materials are injected into the inner cylinder through the first pipeline, hot air is injected into the outer cylinder through the air pump, so that the hot air surrounds the outer side of the inner cylinder to uniformly heat the inner cylinder, the raw materials in the inner cylinder are ensured to be uniformly heated, the non-target raw materials are prevented from being evaporated, the required raw materials are discharged through the second pipeline after being evaporated, and the raw materials which are not evaporated are left in the inner cylinder.
Description
Technical Field
The utility model relates to the field of horizontal rotary evaporation separators, in particular to a horizontal rotary evaporation separation device.
Background
Currently, horizontal rotary evaporation separators are devices for separating a liquid mixture, which are usually composed of a horizontal cylindrical vessel with rotation and heating functions, by separating the liquid into different components using the evaporation principle.
The horizontal rotary evaporation separator is heated by the heating device when in use, the temperature rise near the heating position is fast, and when the container rotates, the temperature of the rotating area near the heating position is higher than that of the rotating area far away from the heating position, so that the heating is not uniform enough, the unnecessary raw materials are partially evaporated after the evaporation of the necessary raw materials easily caused by the overhigh temperature, and the purity of the raw materials discharged from the steam is affected, so that a device is needed to solve the problems.
Disclosure of Invention
The utility model aims to provide a horizontal rotary evaporation separation device, which is used for solving the problem that raw materials in the background technology are heated unevenly.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model provides a horizontal rotary evaporation separator, includes support frame and urceolus, the support frame is fixed in the urceolus outside, the inside activity of urceolus is inlayed and is provided with the inner tube, inner tube one side activity cup joints and sets up first pipeline, first pipeline one side is provided with conveniently drives inner tube pivoted slewing mechanism, urceolus one side is fixed and is provided with first supporting shoe, first supporting shoe is fixed in first pipeline outside, the activity of inner tube opposite side cup joints and is provided with the second pipeline, urceolus one side is fixed and is provided with the second supporting shoe, the second supporting shoe is fixed in the second pipeline outside, the fixed blast pipe that is provided with in urceolus one side, urceolus one side is provided with the inside heating mechanism of convenient heating urceolus, inner tube and urceolus bottom are provided with the discharge mechanism of convenient discharge surplus material, heating mechanism includes hollow disc, injection tube and air pump, the injection tube inlays and fixes in urceolus one side, hollow disc fixes in hollow disc one side, the air pump is fixed in the hollow disc one side, and is inside the inner tube is inlayed with the inner tube through first inner tube to the raw materials when using, will pour into the inner tube through the urceolus into inside, so make and encircle evenly in the outside and need not evaporate the inside the evaporation by the evaporation, the inside the evaporation demand of raw materials after guaranteeing the inside is heated by the evaporation.
Preferably, the rotating mechanism comprises a motor and a cross rod, the cross rod is fixed inside the inner cylinder, the motor is fixed on one side of the first pipeline, the motor is a stepping motor, the output end of the motor is fixed on the cross rod, the motor is started when in use, the motor drives the cross rod to rotate, so that the inner cylinder rotates, raw materials inside the inner cylinder are clung to the inner side wall of the inner cylinder, and heating uniformity is further improved.
Preferably, the discharging mechanism comprises a first discharging pipe, a second discharging pipe and an electromagnetic valve, the first discharging pipe is embedded and fixed on the inner cylinder, the second discharging pipe is embedded and fixed on the outer cylinder, the electromagnetic valve is provided with two discharging pipes which are respectively fixed at the bottom ends of the first discharging pipe and the second discharging pipe, the opening and closing of the first discharging pipe and the second discharging pipe are conveniently controlled, the device is closed after evaporation is completed, the first discharging pipe is located at the bottom end position after the device stops rotating, the electromagnetic valve is opened at the moment, the first discharging pipe and the second discharging pipe are opened, and residual raw materials in the inner part are discharged.
Preferably, the first pipeline is movably and hermetically connected with the inner cylinder, and the second pipeline is movably and hermetically connected with the inner cylinder.
Preferably, both sides of the inner cylinder extend to the outer side of the outer cylinder through fixed pipelines.
Preferably, the air pump output end extends to the inside of the outer cylinder through a pipeline.
Compared with the prior art, the utility model has the beneficial effects that:
when the utility model is used, raw materials are injected into the inner cylinder through the first pipeline, hot air is injected into the outer cylinder through the air pump, so that the hot air surrounds the outer side of the inner cylinder to uniformly heat the inner cylinder, the raw materials in the inner cylinder are ensured to be uniformly heated, the non-target raw materials are prevented from being evaporated, the required raw materials are discharged through the second pipeline after being evaporated, and the raw materials which are not evaporated are left in the inner cylinder;
when the device is used, the motor is started, the motor drives the cross rod to rotate, so that the inner cylinder rotates, raw materials in the inner cylinder are clung to the inner side wall of the inner cylinder, heating uniformity is further improved, the device is closed after evaporation is finished, the first discharging pipe is positioned at the bottom end position after the device stops rotating, the electromagnetic valve is started at the moment, the first discharging pipe and the second discharging pipe are started, and residual raw materials in the inner cylinder are discharged.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a horizontal rotary evaporation separation device according to the present utility model;
FIG. 2 is a cross-sectional view of a horizontal rotary evaporation separation device according to the present utility model;
fig. 3 is an enlarged schematic diagram of a horizontal rotary evaporation separation device according to the present utility model.
In the figure: 1. a support frame; 2. an outer cylinder; 3. an injection tube; 4. a first pipe; 5. a first support block; 6. a hollow disc; 7. an air pump; 8. an inner cylinder; 9. an exhaust pipe; 10. a motor; 11. a cross bar; 12. a second pipe; 13. a second support block; 14. a first discharge pipe; 15. an electromagnetic valve; 16. and a second discharge pipe.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1-3, the present utility model provides a technical solution: a horizontal rotary evaporation separation device comprises a support frame 1 and an outer cylinder 2, wherein the support frame 1 is fixed on the outer side of the outer cylinder 2 through bolts, an inner cylinder 8 is movably embedded in the outer cylinder 2, two sides of the inner cylinder 8 extend to the outer side of the outer cylinder 2 through fixed pipelines, a first pipeline 4 is movably sleeved on one side of the inner cylinder 8, a rotating mechanism which is convenient for driving the inner cylinder 8 to rotate is arranged on one side of the first pipeline 4, a first supporting block 5 is fixedly welded on one side of the outer cylinder 2, the first supporting block 5 is fixedly welded on the outer side of the first pipeline 4, the first pipeline 4 is movably and hermetically connected with the inner cylinder 8, a second pipeline 12 is movably sleeved on the other side of the inner cylinder 8, a second supporting block 13 is fixedly welded on one side of the outer cylinder 2, a second supporting block 13 is fixedly welded on the outer side of the second pipeline 12, an exhaust pipe 9 is fixedly embedded on one side of the outer cylinder 2, the heating mechanism for conveniently heating the inside of the outer cylinder 2 is arranged on one side of the outer cylinder 2, the discharge mechanism for conveniently discharging residual materials is arranged at the bottom ends of the inner cylinder 8 and the outer cylinder 2, the heating mechanism comprises a hollow disc 6, an injection pipe 3 and an air pump 7, the injection pipe 3 is embedded and fixed on one side of the outer cylinder 2, the hollow disc 6 is welded and fixed on one side of the injection pipe 3, the air pump 7 is fixed on one side of the hollow disc 6 through a mounting frame, the output end of the air pump 7 extends to the inside of the outer cylinder 2 through a pipeline, raw materials are injected into the inside of the inner cylinder 8 through a first pipeline 4 when in use, hot air is injected into the inside of the outer cylinder 2 through the air pump 7, so that the hot air surrounds the inner cylinder 8 to uniformly heat the inner cylinder 8, raw materials inside the inner cylinder 8 are guaranteed to be heated uniformly, non-target raw materials are prevented from being evaporated, required raw materials are discharged through a second pipeline 12 after being evaporated, and raw materials which are not evaporated are left inside the inner cylinder 8.
In one instance of this embodiment, the slewing mechanism includes motor 10 and horizontal pole 11, and horizontal pole 11 welded fastening is inside inner tube 8, and motor 10 passes through the mounting bracket to be fixed in first pipeline 4 one side, and motor 10 is step motor, and motor 10 output passes through the shaft coupling to be fixed on horizontal pole 11, starts motor 10 when using, and motor 10 drives horizontal pole 11 and rotates, so makes inner tube 8 rotate for inner tube 8 inside raw materials hugs closely on inner tube 8 inside wall, further improves the heating homogeneity.
In one case of this embodiment, the discharging mechanism includes a first discharging tube 14, a second discharging tube 16 and an electromagnetic valve 15, where the first discharging tube 14 is embedded and fixed on the inner tube 8, the second discharging tube 16 is embedded and fixed on the outer tube 2, two electromagnetic valves 15 are respectively fixed at the bottom ends of the first discharging tube 14 and the second discharging tube 16, so as to conveniently control the opening and closing of the first discharging tube 14 and the second discharging tube 16, and after evaporation is completed, the device is closed, after stopping, the first discharging tube 14 is located at the bottom end position, at this time, the electromagnetic valve 15 is opened, so that the first discharging tube 14 and the second discharging tube 16 are opened, and the internal residual raw materials are discharged.
Working principle: when the utility model is used, raw materials are injected into the inner cylinder 8 through the first pipeline 4, hot air is injected into the outer cylinder 2 through the air pump 7, so that the hot air surrounds the outer side of the inner cylinder 8 to uniformly heat the inner cylinder 8, the raw materials in the inner cylinder 8 are ensured to be uniformly heated, non-target raw materials are prevented from being evaporated, required raw materials are discharged through the second pipeline 12 after being evaporated, and raw materials which are not evaporated are left in the inner cylinder 8; when the novel evaporator is used, the motor 10 is started, the motor 10 drives the cross rod 11 to rotate, so that the inner barrel 8 rotates, raw materials inside the inner barrel 8 are clung to the inner side wall of the inner barrel 8, heating uniformity is further improved, the device is closed after evaporation is finished, the first discharging pipe 14 is positioned at the bottom end position after the device stops rotating, the electromagnetic valve 15 is started at the moment, the first discharging pipe 14 and the second discharging pipe 16 are started, and residual raw materials inside the novel evaporator are discharged.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides a horizontal rotary evaporation separator, includes support frame (1) and urceolus (2), its characterized in that: the support frame (1) is fixed on the outer side of the outer cylinder (2), an inner cylinder (8) is movably embedded in the outer cylinder (2), a first pipeline (4) is movably sleeved on one side of the inner cylinder (8), a rotating mechanism which is convenient for driving the inner cylinder (8) to rotate is arranged on one side of the first pipeline (4), a first supporting block (5) is fixedly arranged on one side of the outer cylinder (2), the first supporting block (5) is fixed on the outer side of the first pipeline (4), a second pipeline (12) is movably sleeved on the other side of the inner cylinder (8), a second supporting block (13) is fixedly arranged on one side of the outer cylinder (2), an exhaust pipe (9) is fixedly embedded on one side of the outer cylinder (2), a heating mechanism which is convenient for heating the inner part of the outer cylinder (2) is arranged on one side of the outer cylinder, a discharging mechanism which is convenient for discharging residual materials is arranged on the bottom end of the inner cylinder (8) and the outer cylinder (2), the heating mechanism comprises a hollow disc (6) and an injection pipe (3), the injection pump (7) is fixedly arranged on one side of the outer cylinder (3), the injection pipe (3) is fixedly embedded on one side of the hollow disc (6), the air pump (7) is fixed at one side of the hollow disc (6).
2. A horizontal rotary evaporation separation device according to claim 1, wherein: the rotating mechanism comprises a motor (10) and a cross rod (11), the cross rod (11) is fixed inside the inner cylinder (8), the motor (10) is fixed on one side of the first pipeline (4), the motor (10) is a stepping motor, and the output end of the motor (10) is fixed on the cross rod (11).
3. A horizontal rotary evaporation separation apparatus according to claim 2, wherein: the discharging mechanism comprises a first discharging pipe (14), a second discharging pipe (16) and an electromagnetic valve (15), wherein the first discharging pipe (14) is embedded and fixed on the inner cylinder (8), the second discharging pipe (16) is embedded and fixed on the outer cylinder (2), and the electromagnetic valve (15) is provided with two discharging pipes which are respectively fixed at the bottoms of the first discharging pipe (14) and the second discharging pipe (16).
4. A horizontal rotary evaporation separation device according to claim 3, wherein: the first pipeline (4) is movably and hermetically connected with the inner cylinder (8), and the second pipeline (12) is movably and hermetically connected with the inner cylinder (8).
5. The horizontal rotary evaporation separation device according to claim 4, wherein: the two sides of the inner cylinder (8) extend to the outer side of the outer cylinder (2) through fixed pipelines.
6. A horizontal rotary evaporation separation device according to claim 5, wherein: the output end of the air pump (7) extends to the inside of the outer cylinder (2) through a pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322117864.9U CN220736229U (en) | 2023-08-08 | 2023-08-08 | Horizontal rotary evaporation separation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322117864.9U CN220736229U (en) | 2023-08-08 | 2023-08-08 | Horizontal rotary evaporation separation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220736229U true CN220736229U (en) | 2024-04-09 |
Family
ID=90549777
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202322117864.9U Active CN220736229U (en) | 2023-08-08 | 2023-08-08 | Horizontal rotary evaporation separation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220736229U (en) |
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2023
- 2023-08-08 CN CN202322117864.9U patent/CN220736229U/en active Active
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