CN220736223U - Distillation plant is used in production of hydroxy benzene propionic acid - Google Patents
Distillation plant is used in production of hydroxy benzene propionic acid Download PDFInfo
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- CN220736223U CN220736223U CN202322347389.4U CN202322347389U CN220736223U CN 220736223 U CN220736223 U CN 220736223U CN 202322347389 U CN202322347389 U CN 202322347389U CN 220736223 U CN220736223 U CN 220736223U
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- distillation
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- liquid discharge
- plate
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- 238000004821 distillation Methods 0.000 title claims abstract description 84
- 238000004519 manufacturing process Methods 0.000 title abstract description 7
- RWFHJEVTRVSDNX-UHFFFAOYSA-N phenol;propanoic acid Chemical compound CCC(O)=O.OC1=CC=CC=C1 RWFHJEVTRVSDNX-UHFFFAOYSA-N 0.000 title description 5
- 238000010438 heat treatment Methods 0.000 claims abstract description 39
- NWCHELUCVWSRRS-UHFFFAOYSA-N atrolactic acid Chemical compound OC(=O)C(O)(C)C1=CC=CC=C1 NWCHELUCVWSRRS-UHFFFAOYSA-N 0.000 claims abstract description 35
- 238000001816 cooling Methods 0.000 claims abstract description 30
- 230000007246 mechanism Effects 0.000 claims abstract description 24
- 239000007788 liquid Substances 0.000 claims description 45
- 239000002184 metal Substances 0.000 claims description 14
- 239000000110 cooling liquid Substances 0.000 claims description 9
- 238000000926 separation method Methods 0.000 claims description 8
- 230000000694 effects Effects 0.000 abstract description 8
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 description 6
- 230000003110 anti-inflammatory effect Effects 0.000 description 4
- 239000003963 antioxidant agent Substances 0.000 description 4
- 230000003078 antioxidant effect Effects 0.000 description 4
- 238000007599 discharging Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000002537 cosmetic Substances 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 206010061218 Inflammation Diseases 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 230000004054 inflammatory process Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 150000002894 organic compounds Chemical class 0.000 description 2
- 230000004792 oxidative damage Effects 0.000 description 2
- 150000003254 radicals Chemical class 0.000 description 2
- WFOFRQGMZWSZOD-UHFFFAOYSA-N 2-hydroxy-2-phenylpropanoic acid Chemical compound OC(=O)C(O)(C)C1=CC=CC=C1.OC(=O)C(O)(C)C1=CC=CC=C1 WFOFRQGMZWSZOD-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Chemical group 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical group OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Abstract
The utility model relates to a distillation device for producing hydroxy phenylpropionic acid, relates to the technical field of hydroxy phenylpropionic acid production, and solves the problems of poor distillation effect, high energy consumption and complex operation in the prior art. The technical characteristics include a base, a distillation mechanism arranged on the base and a collection mechanism; the distillation mechanism comprises a heating chamber, a heating plate, a distillation chamber, a plate structure, a temperature sensor and a timer; the heating chamber is arranged on the base, the distillation chamber is arranged on the base and is connected with the heating chamber through a conduit, the heating plate is arranged on the inner lower surface of the distillation chamber, the plate-type structure is arranged in the distillation chamber and is connected with the heating plate, the temperature sensor is arranged in the distillation chamber, and the timer is arranged in the distillation chamber; the collecting mechanism is used for cooling and collecting the evaporated hydroxy phenylpropionic acid.
Description
Technical Field
The utility model relates to the technical field of production of hydroxy phenylpropionic acid, in particular to a distillation device for producing hydroxy phenylpropionic acid.
Background
The hydroxy phenylpropionic acid (Hydroxyphenylpropionic acid) is an organic compound with a chemical formula of C9H10O3. It is an aromatic acid containing hydroxyl and acid groups, often numbered in the position of its adjacent hydroxyl group.
The hydroxyphenylpropionic acid may be present in natural products, such as phenolic compounds in certain plants, or may be obtained by chemical synthesis. It has certain antioxidant and anti-inflammatory properties, and can be widely used in the fields of medicine, cosmetics, etc.
Hydroxy phenylpropionic acid has been studied in medicine as an antioxidant to help reduce free radical production in cells and thereby protect cells from oxidative damage. In addition, the hydroxyphenylpropionic acid is also considered to have a certain anti-inflammatory effect, and can help to alleviate inflammatory reactions.
In the cosmetic field, hydroxy-phenylpropionic acid is often added to skin care and anti-aging products to provide antioxidant and anti-inflammatory effects. It can help reduce free radical damage during skin aging and promote skin repair and regeneration.
In short, the hydroxy phenylpropionic acid is an organic compound with antioxidant and anti-inflammatory properties, and is widely applied to the fields of medicines, cosmetics and the like. Its function is mainly to protect cells from oxidative damage and to alleviate inflammatory reactions.
At present, the existing distillation device for producing the hydroxy-benzene propionic acid has poor distillation effect, high energy consumption and complex operation, so that the design of the distillation device for producing the hydroxy-benzene propionic acid is necessary.
Disclosure of Invention
The utility model aims to solve the technical problems of poor distillation effect, high energy consumption and complex operation in the prior art and provides a distillation device for producing hydroxy phenylpropionic acid.
In order to solve the technical problems, the technical scheme of the utility model is as follows:
a distillation device for producing hydroxy phenylpropionic acid comprises a base, a distillation mechanism and a collection mechanism, wherein the distillation mechanism is arranged on the base;
the distillation mechanism comprises a heating chamber, a heating plate, a distillation chamber, a plate structure, a temperature sensor and a timer;
the heating chamber is arranged on the base, the distillation chamber is arranged on the base and is connected with the heating chamber through a conduit, the heating plate is arranged on the inner lower surface of the distillation chamber, the plate-type structure is arranged in the distillation chamber and is connected with the heating plate, the temperature sensor is arranged in the distillation chamber, and the timer is arranged in the distillation chamber;
the collecting mechanism is used for cooling and collecting the evaporated hydroxy phenylpropionic acid.
Preferably, the plate structure is a plurality of vertically arranged parallel plates, and a series of slits and holes are formed between the plurality of parallel plates so as to increase the gas-liquid contact area and promote the separation effect.
Preferably, the collecting mechanism comprises a cooling cavity, cooling liquid, radiating fins, a plurality of metal pipes, a fan and a collecting part;
the cooling cavity is arranged on the inner upper surface of the distillation chamber, the cooling liquid is arranged in the cooling cavity, at least partial openings at the two ends of the metal guide pipes are inserted into the cooling cavity, the cooling ends of the metal guide pipes are arranged on the upper surface of the distillation chamber, the radiating fins are arranged on the cooling ends of the metal guide pipes, the fan is arranged on the radiating fins, and at least part of the collecting part is arranged in the distillation chamber and used for collecting cooled liquid.
Preferably, the collecting part comprises a collecting plate, a plurality of liquid discharging tanks, a plurality of through holes, an electromagnetic valve, a liquid discharging pipe and a collecting bottle;
the collecting plate is arranged in the distillation chamber, a plurality of through holes are formed in the collecting plate, a plurality of liquid discharge grooves are formed in the collecting plate, one ends of the liquid discharge grooves are gathered into a total liquid discharge groove, a liquid discharge port is formed in the contact part of the distillation chamber and the liquid discharge groove, the electromagnetic valve is arranged in the liquid discharge port, the liquid discharge pipe is connected with the liquid discharge port, and the collecting bottle is arranged on the base and connected with the liquid discharge pipe.
Preferably, the lower surface of base is equipped with two pairs of universal wheels, every the last brake block that all is equipped with of universal wheel.
Preferably, the whole heating chamber is higher than the distillation chamber.
The utility model has the following beneficial effects:
1. the operation is simple: the device adopts an automatic control system, can automatically operate according to set parameters, and reduces the complexity of manual operation.
2. The production efficiency is high: through the plate-type structure and the heating plate in the distillation tower, the separation effect of the raw materials is better, and the production efficiency is improved.
3. The product purity is high: through reasonable device design and operation parameters, the purity of the product is ensured. Meanwhile, the recovery system inside the device can avoid the loss of raw materials and improve the yield.
Drawings
The utility model is described in further detail below with reference to the drawings and the detailed description.
FIG. 1 is a schematic diagram of a distillation apparatus for producing hydroxy phenylpropionic acid according to the present utility model;
FIG. 2 is a side view of the distillation chamber of the present utility model;
fig. 3 is a top view of the collection plate of the present utility model.
Reference numerals in the drawings denote:
1. a base; 2. a heating chamber; 3. a heating sheet; 4. a distillation chamber; 5. a panel structure; 6. a temperature sensor; 7. a timer; 8. a cooling cavity; 9. a cooling liquid; 10. a heat radiation fin; 11. a metal conduit; 12. a fan; 13. a collection plate; 14. an electromagnetic valve; 15. a liquid discharge pipe; 16. a collection bottle; 17. a liquid outlet; 18. a universal wheel; 19. a brake pad.
Description of the embodiments
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1-3, a distillation apparatus for producing hydroxy phenylpropionic acid comprises a base 1, a distillation mechanism and a collection mechanism arranged on the base 1;
the distillation mechanism comprises a heating chamber 2, a heating plate 3, a distillation chamber 4, a plate structure 5,
A temperature sensor 6 and a timer 7;
the heating chamber 2 is arranged on the base 1, the distillation chamber 4 is arranged on the base 1 and is connected with the heating chamber 2 through a conduit, the heating plate 3 is arranged on the inner lower surface of the distillation chamber 4, the plate-type structure 5 is arranged in the distillation chamber 4 and is connected with the heating plate 3, the temperature sensor 6 is arranged in the distillation chamber 4, and the timer 7 is arranged in the distillation chamber 4;
the collecting mechanism is used for cooling and collecting the evaporated hydroxy phenylpropionic acid.
The plate structure 5 is a plurality of vertically arranged parallel plates, and a series of slits and holes are formed among the parallel plates so as to increase the gas-liquid contact area and promote the separation effect.
The collecting mechanism comprises a cooling cavity 8, cooling liquid 9, radiating fins 10, a plurality of metal pipes 11, a fan 12 and a collecting part;
the cooling cavity 8 is arranged on the inner upper surface of the distillation chamber 4, the cooling liquid 9 is arranged in the cooling cavity 8, two ends of a plurality of metal pipes 11 are at least partially inserted into the cooling cavity 8 in an opening mode, the cooling ends of the metal pipes 11 are arranged on the upper surface of the distillation chamber 4, the cooling fins 10 are arranged on the cooling ends of the metal pipes 11, the fan 12 is arranged on the cooling fins 10, and at least part of the collecting part is arranged in the distillation chamber 4 and used for collecting cooled liquid.
The collecting part comprises a collecting plate 13, a plurality of liquid discharging tanks, a plurality of through holes, an electromagnetic valve 14, a liquid discharging pipe 15 and a collecting bottle 16;
the collecting plate 13 is arranged in the distillation chamber 4, a plurality of through holes are formed in the collecting plate 13, a plurality of liquid discharge grooves are formed in the collecting plate 13, one ends of the liquid discharge grooves are gathered into a total liquid discharge groove, a liquid discharge port 17 is formed in the contact part of the distillation chamber 4 and the liquid discharge groove, the electromagnetic valve 14 is arranged in the liquid discharge port, the liquid discharge pipe 15 is connected with the liquid discharge port 17, and the collecting bottle 16 is arranged on the base 1 and is connected with the liquid discharge pipe 15.
Two pairs of universal wheels 18 are arranged on the lower surface of the base 1, and a brake block 19 is arranged on each universal wheel 18.
The whole heating chamber 2 is higher than the distillation chamber.
Working principle:
the distillation process of the hydroxyphenylpropionic acid can be performed by the following steps:
preparing raw materials: the mixture containing the hydroxyphenylpropionic acid is prepared and may be a reaction product or other mixture containing the hydroxyphenylpropionic acid.
Heating raw materials: the feedstock is heated to a suitable temperature to evaporate. The temperature of heating should be above the boiling point of the hydroxyphenylpropionic acid, but below any other possible decomposition temperature.
Distillation chamber 4 separation: the heated feedstock is fed into a distillation chamber 4. The distillation chamber 4 is typically internally provided with packing or plate structures 5 to increase the contact area and promote the separation effect. By the action of heat and evaporation, the hydroxyphenylpropionic acid evaporates to the top of the distillation column.
Condensing the hydroxy phenylpropionic acid: the vaporized hydroxyphenylpropionic acid was cooled by a collecting mechanism and converted into a liquid form. The cooling inside the collection mechanism is usually performed by cooling water or other cooling medium, and the vaporized gaseous hydroxy phenylpropionic acid is condensed.
Collecting the hydroxy phenylpropionic acid: the condensed hydroxyphenylpropionic acid may accumulate in the collection bottle 16. The collection bottle 16 is used to collect and store the hydroxyphenylpropionic acid for further processing or storage.
Throughout the distillation process, it is necessary to control the heating temperature and the operating parameters of the distillation chamber to achieve optimal separation and purification of the hydroxyphenylpropionic acid. This includes controlling heating temperature, pressure and flow rate of the distillation column, etc. In addition, proper distillation equipment and operating conditions are required to be selected according to actual requirements so as to ensure the efficiency and product quality of the distillation process.
Function of the internal components:
firstly, the base 1 is driven to move through the universal wheel 18, when the base moves to a designated working place, the universal wheel 18 can be fixedly limited through the brake pad 19, the shaking condition during working is avoided, raw materials can be initially heated in the heating chamber 2, the raw materials enter the distillation chamber 4 through the guide pipe after being heated, distillation treatment is carried out in the distillation chamber 4 after being heated, the heating plate 3 is heated, the plate-type structure increases the contact area of gas and liquid and promotes the separation effect, then the temperature can be sensed through the temperature sensor 6, the heating time of the heating plate 3 can be timed through the timer 7, vaporized hydroxy-benzene propionic acid enters the cooled area through the collecting plate 13 for cooling, the vapor is cooled into liquid which drops into the collecting groove on the collecting plate 13 and finally summarized in the collecting groove, the liquid is discharged through the electromagnetic valve 14 and enters the collecting bottle 16, the cooling device in the collecting mechanism is used for cooling liquid 9 for heating and cooling, and the cooling liquid 9 can be conducted by the cooling fin 10 and the fan 12 through the metal guide pipe 11 for a long time.
It is apparent that the above examples are given by way of illustration only and are not limiting of the embodiments. Other variations or modifications of the above teachings will be apparent to those of ordinary skill in the art. It is not necessary here nor is it exhaustive of all embodiments. While still being apparent from variations or modifications that may be made by those skilled in the art are within the scope of the utility model.
Claims (6)
1. The distilling device for producing the hydroxy phenylpropionic acid is characterized by comprising a base (1), a distilling mechanism and a collecting mechanism, wherein the distilling mechanism and the collecting mechanism are arranged on the base (1);
the distillation mechanism comprises a heating chamber (2), a heating plate (3), a distillation chamber (4), a plate structure (5),
A temperature sensor (6) and a timer (7);
the heating chamber (2) is arranged on the base (1), the distillation chamber (4) is arranged on the base (1) and is connected with the heating chamber (2) through a guide pipe, the heating plate (3) is arranged on the inner lower surface of the distillation chamber (4), the plate-type structure (5) is arranged in the distillation chamber (4) and is connected with the heating plate (3), the temperature sensor (6) is arranged in the distillation chamber (4), and the timer (7) is arranged in the distillation chamber (4);
the collecting mechanism is used for cooling and collecting the evaporated hydroxy phenylpropionic acid.
2. A distillation apparatus for producing hydroxyphenylpropionic acid, according to claim 1, wherein the plate structure (5) is a plurality of vertically aligned parallel plates, and a series of slits and holes are formed between the plurality of parallel plates to increase a gas-liquid contact area and promote separation.
3. The distillation apparatus for producing hydroxyphenylpropionic acid according to claim 1, wherein the collecting means comprises a cooling chamber (8), a cooling liquid (9), a heat radiating fin (10), a plurality of metal pipes (11), a fan (12), and a collecting portion;
the cooling cavity (8) is arranged on the inner upper surface of the distillation chamber (4), the cooling liquid (9) is arranged inside the cooling cavity (8), two ends of a plurality of metal pipes (11) are at least partially inserted into the cooling cavity (8) in an opening mode, the cooling ends of the metal pipes (11) are arranged on the upper surface of the distillation chamber (4), the radiating fins (10) are arranged on the cooling ends of the metal pipes (11), the fan (12) is arranged on the radiating fins (10), and at least part of the collecting part is arranged in the distillation chamber (4) and used for collecting cooled liquid.
4. A distillation apparatus for producing hydroxyphenylpropionic acid as claimed in claim 3, wherein the collecting portion comprises a collecting plate (13), a plurality of liquid discharge tanks, a plurality of through holes, a solenoid valve (14), a liquid discharge pipe (15), and a collecting bottle (16);
the collecting plate (13) is arranged in the distillation chamber (4), a plurality of through holes are formed in the collecting plate (13), a plurality of liquid discharge grooves are formed in the collecting plate (13), one ends of the liquid discharge grooves are gathered into a total liquid discharge groove, a liquid discharge port (17) is formed in the contact part of the distillation chamber (4) and the liquid discharge groove, the electromagnetic valve (14) is arranged in the liquid discharge port, the liquid discharge pipe (15) is connected with the liquid discharge port (17), and the collecting bottle (16) is arranged on the base (1) and is connected with the liquid discharge pipe (15).
5. The distillation apparatus for producing hydroxyphenylpropionic acid according to claim 1, wherein two pairs of universal wheels (18) are provided on the lower surface of the base (1), and a brake pad (19) is provided on each universal wheel (18).
6. The distillation apparatus for producing hydroxyphenylpropionic acid according to claim 1, wherein the heating chamber (2) is integrally formed to have a height higher than that of the distillation chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322347389.4U CN220736223U (en) | 2023-08-31 | 2023-08-31 | Distillation plant is used in production of hydroxy benzene propionic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322347389.4U CN220736223U (en) | 2023-08-31 | 2023-08-31 | Distillation plant is used in production of hydroxy benzene propionic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220736223U true CN220736223U (en) | 2024-04-09 |
Family
ID=90559651
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202322347389.4U Active CN220736223U (en) | 2023-08-31 | 2023-08-31 | Distillation plant is used in production of hydroxy benzene propionic acid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220736223U (en) |
-
2023
- 2023-08-31 CN CN202322347389.4U patent/CN220736223U/en active Active
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