CN220496410U - Full-automatic water bath condensation reflux extractor - Google Patents
Full-automatic water bath condensation reflux extractor Download PDFInfo
- Publication number
- CN220496410U CN220496410U CN202321944799.0U CN202321944799U CN220496410U CN 220496410 U CN220496410 U CN 220496410U CN 202321944799 U CN202321944799 U CN 202321944799U CN 220496410 U CN220496410 U CN 220496410U
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- Prior art keywords
- water bath
- box body
- reflux
- lifting
- sliding plate
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 65
- 238000010992 reflux Methods 0.000 title claims abstract description 57
- 238000009833 condensation Methods 0.000 title claims abstract description 25
- 230000005494 condensation Effects 0.000 title claims abstract description 25
- 239000000376 reactant Substances 0.000 claims abstract description 12
- 230000036632 reaction speed Effects 0.000 claims abstract description 6
- 238000009434 installation Methods 0.000 claims description 15
- 238000003760 magnetic stirring Methods 0.000 claims description 13
- 241001417523 Plesiopidae Species 0.000 claims description 3
- 239000011521 glass Substances 0.000 abstract description 9
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 230000001105 regulatory effect Effects 0.000 abstract description 3
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000007810 chemical reaction solvent Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 230000001133 acceleration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
Abstract
The utility model provides a full-automatic water bath condensation reflux extractor which comprises a control box body, wherein a water bath box body is arranged on one side surface of the control box body, a water bath pot is arranged on the upper surface of the water bath box body, a support column is arranged on the other side surface of the water bath box body, an upper support rod is arranged on the top ends of the water bath box body and the support column, a lifting reflux mechanism is arranged on the top ends of the upper support rod, and the front page of the lifting reflux mechanism is only provided with a limit clamp, so that the problem that the reaction speed of reactants in a spherical glass condensation pipe can be regulated and controlled only by changing the temperature of the spherical glass condensation pipe in a cold water bath tank and the operation of heating condensation reflux cannot be performed, and the application range is limited when the reactants in different types of condensation reflux are faced is solved.
Description
Technical Field
The utility model mainly relates to the technical field of plastic manufacturing, in particular to a full-automatic water bath condensation reflux extractor.
Background
In order to accelerate the chemical reaction which is slow or difficult to carry out in the laboratory, a reflux and condensation device is often adopted to ensure the reaction to be complete and prevent the reactants, products or solvents from volatilizing and escaping the system. The existing laboratory is manually built, is complex and cumbersome, and is not suitable for carrying out condensation reflux reaction on a large number of samples at the same time.
In the application publication number CN202022171667.1, application publication date 2021.06.22, entitled "a fatty acid methyl esterification System", the utility model patent application comprises: spherical glass condenser pipe, sample bottle, hot water bath, cooling cycle water machine, its characterized in that, it still includes: the device realizes the integral lifting of the spherical glass condenser tube and the sample bottle by utilizing the lifting mechanism, thereby facilitating the installation and the disassembly of the sample bottle and the operation; the utility model is provided with the cold water bath, which can rapidly cool the sample, and simultaneously, the cold water bath and the spherical glass condenser tube share the same cooling water machine, thereby saving the cost,
however, when stirring is performed, the reaction speed of reactants in the spherical glass condenser tube can be regulated and controlled only by changing the temperature of the spherical glass condenser tube in the cold water bath, and the operation of heating, condensing and refluxing cannot be performed, so that the application range is limited when different types of reactants are subjected to condensing and refluxing.
Disclosure of Invention
1. Technical problem to be solved by the utility model
The utility model provides a full-automatic water bath condensation reflux extractor, which is used for solving the problems that the reaction speed of reactants in a spherical glass condenser tube can be regulated and controlled only by changing the temperature of the spherical glass condenser tube in a cold water bath tank in the background, and the operation of heating condensation reflux can not be performed, and the application range is limited when different types of condensation reflux reactants are faced.
2. Technical proposal
In order to achieve the above purpose, the technical scheme provided by the utility model is as follows: a full-automatic water bath condensation reflux extractor is characterized in that: including the control box, control box one side surface is provided with the water bath box, water bath box top surface is provided with the water bath, water bath box opposite side surface is provided with the support column, water bath box and support column top are provided with the bracing piece, go up the bracing piece, the top is provided with lift reflux mechanism, lift reflux mechanism surface first page only spacing clamp.
Further, the limiting clamp is provided with a plurality of limiting clamps on the surface of the lifting reflux mechanism, and the limiting clamps are sequentially arranged on the surface of the lifting reflux mechanism and correspond to the position of the lower water bath kettle.
Further, the water bath box is including the cavity box, cavity box lower extreme surface is equipped with the spout, the spout surface is provided with interior embedded groove body, interior embedded groove body inside swing joint has the telescopic link, interior embedded groove body inside telescopic link surface is provided with reset spring, the telescopic link other end sets up swing joint has the sliding plate, the sliding plate both sides are provided with the slip spacing, the sliding plate top is provided with magnetic stirring device.
Further, expansion round heads are arranged at two ends of the telescopic rod, two ends of the telescopic rod are respectively limited inside the embedded groove body and the sliding plate, and the magnetic stirring device above the sliding plate after the sliding plate completely enters the hollow box body is located below the water bath.
Further, the lifting reflux mechanism comprises an upper end box body, a telescopic oil cylinder is arranged on the lower end surface of the upper end box body, a lifting installation block is arranged on the lower end surface of the telescopic oil cylinder, a fixing clamp is fixedly connected with the surface of the lifting installation block, a reflux pipe is arranged on the surface of the fixing clamp, a bath bottle is arranged at the bottom end of the reflux pipe, and a reflux hose is arranged on the surface of the reflux pipe.
Further, the reflux pipe and the bath bottle are fixed on one side surface of the lifting installation block through the fixing clamp, and the telescopic oil cylinder drives the lifting installation block to ascend or descend and simultaneously drives the bath bottle to enter or leave the water bath kettle.
Further, the reactants in the bath bottle are stirred by a magnetic stirring device below the water bath kettle so as to accelerate the reaction speed.
3. Advantageous effects
Compared with the prior art, the technical scheme provided by the utility model has the following beneficial effects:
the utility model has reasonable design, when the condensation reflux operation is needed, the reaction solvent is injected into the plurality of bath bottles, the reflux pipe above the reaction solvent is arranged and fixed on the surface of the clamp, the lifting installation block is driven to descend into the water bath kettle by starting the telescopic oil cylinder, thereby realizing the purpose of synchronous experiment in position and automatic lifting for cooling after the experiment is finished,
simultaneously, under the action of a reset spring in the condensation reflux process, the telescopic rod is driven to recycle the sliding plate and the magnetic stirring device above the sliding plate to be pulled back to the lower part of the water bath, and reactants in the surface bath bottle of the water bath are stirred, so that the reaction efficiency is improved.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is a schematic side view of a water bath cabinet according to the present utility model;
FIG. 3 is a schematic perspective view of the lifting reflow mechanism of the present utility model;
fig. 4 is a schematic view of a return tube according to the present utility model.
Reference numerals
1. A control box body; 2. a water bath box body; 201. a hollow box body; 202. a groove body is embedded; 203. a telescopic rod; 204. a return spring; 205. a sliding plate; 206. sliding a limit bar; 207. a magnetic stirring device; 3. a water bath kettle; 4. a support column; 5. an upper support rod; 6. a lifting reflux mechanism; 601. an upper end case; 602. a telescopic oil cylinder; 603. lifting the mounting block; 604. fixing the clamp; 605. a return pipe; 606. bath bottle; 607. a return hose; 7. and (5) limiting the clamping hoop.
Detailed Description
In order that the utility model may be readily understood, a more particular description of the utility model will be rendered by reference to specific embodiments thereof which are illustrated in the appended drawings, in which, however, the utility model may be embodied in many different forms and are not limited to the embodiments described herein, but are instead provided for the purpose of providing a more thorough and complete disclosure of the utility model.
In the description of the present utility model, it should be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "page", "bottom", "inner", "outer", "clockwise", "counterclockwise", etc. indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings are merely for convenience in describing the present utility model and simplifying the description, and do not indicate or imply that the devices or elements referred to must have a specific orientation, be configured and operated in a specific orientation, and thus should not be construed as limiting the present utility model.
Furthermore, the terms "first," "second," and the like, are used for descriptive purposes only and are not to be construed as indicating or implying a relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defining "a first" or "a second" may explicitly or implicitly include one or more such feature. In the description of the present utility model, the meaning of "a plurality" is two or more, unless explicitly defined otherwise.
In the present utility model, unless explicitly stated and limited otherwise, the terms "mounted," "connected," "secured," "provided," and the like are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; can be directly connected or indirectly connected through an intermediate medium, and can be communication between two elements. The specific meaning of the above terms in the present utility model can be understood by those of ordinary skill in the art according to the specific circumstances.
Examples
Referring to fig. 1-4, a full-automatic water bath condensation reflux extractor, including control box 1, control box 1 one side surface is provided with water bath box 2, water bath box 2 top surface is provided with water bath 3, water bath box 2 opposite side surface is provided with support column 4, water bath box 2 and support column 4 top are provided with bracing piece 5, go up bracing piece 5, the top is provided with lift reflux mechanism 6, lift reflux mechanism 6 surface top page only has spacing clamp 7, spacing clamp 7 is provided with a plurality of on lift reflux mechanism 6 surface, and arranges in proper order at lift reflux mechanism 6 surface, corresponds each other with lower extreme water bath 3 positions, and this device carries out the stirring acceleration reaction to the inside of bath bottle 606 through magnetic stirring device 207 in water bath box 2.
The water bath box body 2 comprises a hollow box body 201, a chute is arranged on the lower end surface of the hollow box body 201, an embedded groove body 202 is arranged on the surface of the chute, a telescopic rod 203 is movably connected inside the embedded groove body 202, a reset spring 204 is arranged on the surface of the telescopic rod 203 inside the embedded groove body 202, a sliding plate 205 is movably connected with the other end of the telescopic rod 203, sliding limiting strips 206 are arranged on two sides of the sliding plate 205, a magnetic stirring device 207 is arranged above the sliding plate 205, expanding round heads are arranged at two ends of the telescopic rod 203, the two ends of the telescopic rod 203 are respectively limited inside the embedded groove body 202 and the sliding plate 205, and a magnetic stirring device 207 above the sliding plate 205 completely enters the hollow box body 201 is positioned below the water bath pot 3.
In the embodiment, under the action of the return spring 204 in the condensation and reflux process, the telescopic rod 203 is driven to recycle the sliding plate 205 and the magnetic stirring device 207 above the sliding plate to the lower part of the water bath 3, and reactants in the bath bottle 606 on the surface of the water bath 3 are stirred, so that the reaction efficiency is improved.
The lifting reflux mechanism 6 comprises an upper end box 601, a telescopic cylinder 602 is arranged on the lower end surface of the upper end box 601, a lifting installation block 603 is arranged on the lower end surface of the telescopic cylinder 602, a fixing clamp 604 is fixedly connected with the surface of the lifting installation block 603, a reflux pipe 605 is arranged on the surface of the fixing clamp 604, a bath bottle 606 is arranged at the bottom end of the reflux pipe 605, a reflux hose 607 is arranged on the surface of the reflux pipe 605, the reflux pipe 605 and the bath bottle 606 are fixed on one side surface of the lifting installation block 603 through the fixing clamp 604, the telescopic cylinder 602 drives the lifting installation block 603 to ascend or descend and simultaneously drives the bath bottle 606 to enter or leave the interior of the water bath 3, and reactants in the bath bottle 606 are stirred through a magnetic stirring device 207 below the water bath 3 so as to accelerate the reaction speed.
In this embodiment, when the condensation reflux operation is needed, the reaction solvent is injected into the plurality of bath bottles 606, and meanwhile, the reflux pipe 605 above the reaction solvent is installed on the surface of the fixed clamp 604, and the lifting installation block 603 is driven to descend into the water bath 3 by starting the telescopic oil cylinder 602, so that the purpose of cooling by automatic lifting after the experiment is finished can be achieved.
The foregoing examples merely illustrate certain embodiments of the utility model and are described in more detail and are not to be construed as limiting the scope of the utility model; it should be noted that it is possible for a person skilled in the art to make several variants and modifications without departing from the concept of the utility model, all of which fall within the scope of protection of the utility model; accordingly, the scope of protection of the present utility model is to be determined by the appended claims.
Claims (6)
1. A full-automatic water bath condensation reflux extractor is characterized in that: comprises a control box body (1), a water bath box body (2) is arranged on one side surface of the control box body (1), a water bath pot (3) is arranged on the upper surface of the water bath box body (2), a support column (4) is arranged on the other side surface of the water bath box body (2), an upper support rod (5) is arranged at the top ends of the water bath box body (2) and the support column (4), a lifting reflux mechanism (6) is arranged at the top end of the upper support rod (5), a limiting clamp (7) is arranged on the front page of the surface of the lifting reflux mechanism (6),
the water bath box body (2) comprises a hollow box body (201), a chute is arranged on the lower end surface of the hollow box body (201), an embedded groove body (202) is arranged on the surface of the chute, a telescopic rod (203) is movably connected to the inside of the embedded groove body (202), a reset spring (204) is arranged on the surface of the telescopic rod (203) inside the embedded groove body (202), a sliding plate (205) is movably connected to the other end of the telescopic rod (203), sliding limiting strips (206) are arranged on two sides of the sliding plate (205), and a magnetic stirring device (207) is arranged above the sliding plate (205).
2. The fully automatic water bath condensation reflux extractor as set forth in claim 1, wherein: the limiting clamp (7) is arranged on the surface of the lifting reflux mechanism (6) in a plurality, and is sequentially arranged on the surface of the lifting reflux mechanism (6) and corresponds to the position of the lower water bath kettle (3).
3. The fully automatic water bath condensation reflux extractor as set forth in claim 1, wherein: expansion round heads are arranged at two ends of the telescopic rod (203), two ends of the telescopic rod (203) are respectively limited inside the embedded groove body (202) and the sliding plate (205), and the magnetic stirring device (207) above the sliding plate (205) after the sliding plate completely enters the hollow box body (201) is located below the water bath pot (3).
4. The fully automatic water bath condensation reflux extractor as set forth in claim 1, wherein: lifting reflux mechanism (6) is including upper end box (601), upper end box (601) lower extreme surface is provided with flexible hydro-cylinder (602), flexible hydro-cylinder (602) lower extreme surface is provided with lift installation piece (603), lift installation piece (603) fixed surface is connected with fixed clamp (604), fixed clamp (604) surface mounting has back flow (605), back flow (605) bottom is provided with bath bottle (606), back flow (605) surface is provided with reflux hose (607).
5. The fully automatic water bath condensation reflux extractor as set forth in claim 4, wherein: the reflux pipe (605) and the bath bottle (606) are fixed on one side surface of the lifting installation block (603) through the fixing clamp (604), and the lifting installation block (603) is driven to ascend or descend through the telescopic oil cylinder (602) and meanwhile the bath bottle (606) is driven to enter or leave the water bath kettle (3).
6. The fully automatic water bath condensation reflux extractor as set forth in claim 4, wherein: the reactants in the bath bottle (606) are stirred by a magnetic stirring device (207) below the water bath kettle (3) so as to accelerate the reaction speed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321944799.0U CN220496410U (en) | 2023-07-24 | 2023-07-24 | Full-automatic water bath condensation reflux extractor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321944799.0U CN220496410U (en) | 2023-07-24 | 2023-07-24 | Full-automatic water bath condensation reflux extractor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220496410U true CN220496410U (en) | 2024-02-20 |
Family
ID=89865953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321944799.0U Active CN220496410U (en) | 2023-07-24 | 2023-07-24 | Full-automatic water bath condensation reflux extractor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220496410U (en) |
-
2023
- 2023-07-24 CN CN202321944799.0U patent/CN220496410U/en active Active
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| GR01 | Patent grant |