CN220460655U - Device for continuous reaction of m-cresol alkylation - Google Patents
Device for continuous reaction of m-cresol alkylation Download PDFInfo
- Publication number
- CN220460655U CN220460655U CN202321137955.2U CN202321137955U CN220460655U CN 220460655 U CN220460655 U CN 220460655U CN 202321137955 U CN202321137955 U CN 202321137955U CN 220460655 U CN220460655 U CN 220460655U
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- stirring
- piece
- continuous reaction
- fixedly connected
- tank
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 38
- RLSSMJSEOOYNOY-UHFFFAOYSA-N m-cresol Chemical compound CC1=CC=CC(O)=C1 RLSSMJSEOOYNOY-UHFFFAOYSA-N 0.000 title claims abstract description 30
- 230000029936 alkylation Effects 0.000 title claims abstract description 15
- 238000005804 alkylation reaction Methods 0.000 title claims abstract description 15
- 238000003756 stirring Methods 0.000 claims abstract description 49
- 238000007599 discharging Methods 0.000 claims abstract description 23
- 238000007789 sealing Methods 0.000 claims abstract description 19
- 238000004140 cleaning Methods 0.000 claims abstract description 18
- 238000010438 heat treatment Methods 0.000 claims abstract description 10
- 238000000926 separation method Methods 0.000 claims abstract description 10
- 230000000149 penetrating effect Effects 0.000 claims description 3
- 239000000376 reactant Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 4
- 239000000126 substance Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000003776 cleavage reaction Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004044 response Effects 0.000 description 2
- 230000007017 scission Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000004992 fission Effects 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000005215 recombination Methods 0.000 description 1
- 230000006798 recombination Effects 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model provides a device for continuous reaction of m-cresol alkylation, which relates to the technical field of reaction, and comprises an integral structure and a discharging structure, wherein the discharging structure is positioned at the position, close to the bottom, of the outer surface of the front side of the integral structure; the integrated structure comprises a stirring tank and a heating separation tank, wherein the top of the stirring tank is slidably connected with a sealing cover, the center of the inner top of the sealing cover is rotationally connected with a rotating shaft, the bottom end face of the rotating shaft is fixedly connected with a stirring piece, and the inner surface of the stirring piece is slidably connected with a cleaning piece.
Description
Technical Field
The utility model relates to the technical field of reaction, in particular to a device for continuous reaction of m-cresol alkylation.
Background
The response is a response due to an event, such as: chemical reactions, optical reactions, reflection reactions, chain reactions, force and reaction nuclear fission, nuclear fusion, etc., chemical changes are defined as the synthesis of macromolecules when one contacts another, or the separation of molecules into more than two small molecules by cleavage, or atomic recombination within the molecule, and chemical reactions are usually associated with the formation of chemical bonds and cleavage in order to form a change, with particular attention paid to chemical reactions not changing the nuclei in any way, but rather being limited to electron cloud interactions outside the atoms, although nuclear deformation may trigger chemical reactions, nuclear reactions are independent of chemical reactions.
The existing continuous reaction device has poor reaction effect, and possibly because the reaction quantity is relatively large, the reactants cannot be well mixed, so that the reaction is slow, the reaction is possibly insufficient, and the overall yield is reduced.
Disclosure of Invention
The utility model aims to solve the problems that the reaction effect is poor, the reaction quantity is large, the reactants cannot be well mixed, the reaction is slow, the reaction is insufficient, and the overall yield is reduced, and the device for continuous reaction of m-cresol alkylation is provided.
In order to achieve the above purpose, the present utility model adopts the following technical scheme: an apparatus for continuous reaction of m-cresol alkylation, comprising a monolithic structure and a discharging structure, wherein the discharging structure is positioned on the front outer surface of the monolithic structure near the bottom;
the utility model discloses a stirring tank, including the integrated configuration, the integrated configuration includes agitator tank and heating knockout drum, the top sliding connection of agitator tank has sealed lid, the interior top center department of sealed lid rotates and is connected with the rotation axis, the bottom terminal surface fixedly connected with stirring of rotation axis, the internal surface sliding connection of stirring has the clearance piece, the relative one side of clearance piece and stirring is provided with the spring, the top both sides position screw thread of sealed lid runs through and is provided with the bolt, one side surface of agitator tank is close to the bottom position and runs through and be provided with pipeline, the top of sealed lid is located the fixed mounting of position of rotation axis has the motor.
Preferably, one end of the spring is fixedly connected with the outer surface of the cleaning piece, the other end of the spring is fixedly connected with the inner surface of the stirring piece, one end of the rotating shaft penetrates through the surface of the sealing cover and is fixedly connected with the driving end of the motor, and the other end of the rotating shaft is fixedly connected with the top surface of the stirring piece.
Preferably, the outer surface of the cleaning member is slidably connected to the inner surface wall of the agitator tank.
Preferably, the top of the sealing cover is provided with a threaded hole at the position of the bolt, the inner surface wall of the threaded hole is in threaded connection with the outer surface of the bolt, and the bottom end surface thread of the bolt penetrates through the surface of the stirring tank.
Preferably, a feed pipe penetrates through the top of the sealing cover near the front side.
Preferably, the discharging structure comprises a discharging pipe, an electromagnetic valve is fixedly arranged on the outer surface of the discharging pipe, and the inside of the discharging pipe is communicated with the inside of the heating separation tank.
Compared with the prior art, the utility model has the advantages and positive effects that,
1. in the utility model, a user can pour reactants into the stirring tank through the feeding pipe, after pouring, the motor starts to operate, so that the rotating shaft can rotate, and when the rotating shaft can rotate, the stirring piece and the cleaning piece can be driven to rotate together, and then the stirring piece can stir the reactions, so that the two reactants can be mixed together better.
2. In the utility model, the cleaning piece can clean the inner wall of the stirring tank while stirring, so that attached residues on the inner wall can be prevented, the cleaning piece can clean the inner wall more forcefully by using the expanding force of the spring, and the sealing cover, the motor, the rotating shaft, the cleaning piece and the stirring piece are integrated, so that after a user unscrews the bolt, the sealing cover can be separated from the stirring tank, and the stirring piece can be replaced conveniently by the user.
Drawings
FIG. 1 is a schematic diagram showing the perspective structure of an apparatus for continuous reaction of m-cresol alkylation according to the present utility model;
FIG. 2 is a schematic cross-sectional view of the structure of FIG. 1 showing an apparatus for continuous reaction of m-cresol alkylation according to the present utility model;
fig. 3 is an enlarged view at a in fig. 2.
Legend description: 1. an integral structure; 2. a discharging structure; 101. a stirring tank; 102. a feed pipe; 103. sealing cover; 104. a motor; 105. a rotation shaft; 106. a stirring member; 107. a spring; 108. cleaning the piece; 109. a delivery conduit; 110. heating the separation tank; 111. a threaded hole; 112. a bolt; 201. a discharge pipe; 202. a solenoid valve.
Detailed Description
In order that the above objects, features and advantages of the utility model will be more clearly understood, a further description of the utility model will be rendered by reference to the appended drawings and examples. It should be noted that, in the case of no conflict, the embodiments of the present application and the features in the embodiments may be combined with each other.
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present utility model, however, the present utility model may be practiced otherwise than as described herein, and therefore the present utility model is not limited to the specific embodiments of the disclosure that follow.
Example 1 as shown in fig. 1 to 3, an apparatus for continuous reaction of m-cresol alkylation comprises a monolithic structure 1 and a discharging structure 2, wherein the discharging structure 2 is positioned on the front outer surface of the monolithic structure 1 near the bottom; the integrated structure 1 comprises a stirring tank 101 and a heating separation tank 110, wherein the top of the stirring tank 101 is slidably connected with a sealing cover 103, a rotating shaft 105 is rotatably connected to the center of the inner top of the sealing cover 103, a stirring piece 106 is fixedly connected to the bottom end face of the rotating shaft 105, a cleaning piece 108 is slidably connected to the inner surface of the stirring piece 106, a spring 107 is arranged on the opposite side of the cleaning piece 108 and the stirring piece 106, bolts 112 are arranged at the positions of the two sides of the top of the sealing cover 103 in a threaded penetrating manner, a conveying pipeline 109 is arranged at the position, close to the bottom, of the outer surface of one side of the stirring tank 101 in a penetrating manner, and a motor 104 is fixedly arranged at the position of the rotating shaft 105 at the top of the sealing cover 103.
The effect achieved in the whole embodiment 1 is that, as shown in fig. 2 and 3, when the rotation shaft 105 is rotated by the motor 104, the stirring member 106 is driven to rotate first, and then the cleaning member 108 is driven together, so that the stirring operation can be performed and the cleaning operation can be performed at the same time, and no gap exists at the joint of the sealing cover 103 and the stirring tank 101 in the later use process.
In embodiment 2, as shown in fig. 1-3, one end of a spring 107 is fixedly connected with the outer surface of a cleaning member 108, the other end of the spring 107 is fixedly connected with the inner surface of a stirring member 106, one end of a rotating shaft 105 penetrates through the surface of a sealing cover 103 and is fixedly connected with the driving end of a motor 104, the other end of the rotating shaft 105 is fixedly connected with the top surface of the stirring member 106, the outer surface of the cleaning member 108 is slidably connected with the inner surface wall of a stirring tank 101, a threaded hole 111 is formed in the top of the sealing cover 103 at the position of a bolt 112, the inner surface wall of the threaded hole 111 is in threaded connection with the outer surface of the bolt 112, the bottom end surface of the bolt 112 penetrates through the surface of the stirring tank 101, a feeding pipe 102 is arranged near the front side of the top of the sealing cover 103, a discharging structure 2 comprises a discharging pipe 201, an electromagnetic valve 202 is fixedly arranged on the outer surface of the discharging pipe 201, and the inside of the discharging pipe 201 is communicated with the inside of the heating separation tank 110.
The effect that its whole embodiment 2 reached is, the screw hole 111 and the mutual cooperation of bolt 112 then realize that its sealed lid 103 can be connected more closely with agitator tank 101, and then improves holistic leakproofness, and the setting of solenoid valve 202, the user of being convenient for opens or closes discharging pipe 201.
Working principle: after the two reactants are poured into the stirring tank 101 through the feeding pipe 102, the motor 104 of the stirring tank can start to operate at first, so that the rotating shaft 105 can rotate, the rotating shaft 105 can drive the stirring piece 106 to rotate together when rotating, the stirring piece 106 can rotate and then drive the cleaning piece 108 to rotate together, stirring operation and cleaning operation can be performed at one time, further, the two reactants can be mixed more uniformly, no residue exists on the inner wall of the stirring tank 101, the reaction can be conveyed into the heating separation tank 110 through the conveying pipeline 109 for evaporation separation after stirring, the electromagnetic valve 202 can be opened by the user after the operation is finished, and the reactants in the heating separation tank 110 can be discharged to the outside through the discharging pipe 201.
The present utility model is not limited to the above-mentioned embodiments, and any equivalent embodiments which can be changed or modified by the technical content disclosed above can be applied to other fields, but any simple modification, equivalent changes and modification made to the above-mentioned embodiments according to the technical substance of the present utility model without departing from the technical content of the present utility model still belong to the protection scope of the technical solution of the present utility model.
Claims (6)
1. An apparatus for the continuous reaction of m-cresol alkylation comprising:
the device comprises an integral structure (1) and a discharging structure (2), wherein the discharging structure (2) is positioned at a position, close to the bottom, of the outer surface of the front side of the integral structure (1);
overall structure (1) is including agitator tank (101) and heating knockout drum (110), the top sliding connection of agitator tank (101) has sealed lid (103), the interior top center department of sealed lid (103) rotates and is connected with rotation axis (105), the bottom terminal surface fixedly connected with stirring piece (106) of rotation axis (105), the internal surface sliding connection of stirring piece (106) has clearance piece (108), the opposite one side of clearance piece (108) and stirring piece (106) is provided with spring (107), the top both sides position screw thread of sealed lid (103) runs through and is provided with bolt (112), one side surface of agitator tank (101) is close to the bottom position and runs through and be provided with pipeline (109), the top of sealed lid (103) is located the position fixed mounting of rotation axis (105) has motor (104).
2. The apparatus for continuous reaction of m-cresol alkylation according to claim 1, wherein: one end of the spring (107) is fixedly connected with the outer surface of the cleaning piece (108), the other end of the spring (107) is fixedly connected with the inner surface of the stirring piece (106), one end of the rotating shaft (105) penetrates through the surface of the sealing cover (103) and is fixedly connected with the driving end of the motor (104), and the other end of the rotating shaft (105) is fixedly connected with the top surface of the stirring piece (106).
3. The apparatus for continuous reaction of m-cresol alkylation according to claim 1, wherein: the outer surface of the cleaning piece (108) is in sliding connection with the inner surface wall of the stirring tank (101).
4. The apparatus for continuous reaction of m-cresol alkylation according to claim 1, wherein: screw holes (111) are formed in the positions, located on the top of the sealing cover (103), of the bolts (112), the inner surface wall of each screw hole (111) is in threaded connection with the outer surface of each bolt (112), and the bottom end face threads of each bolt (112) penetrate through the surface of the stirring tank (101).
5. The apparatus for continuous reaction of m-cresol alkylation according to claim 1, wherein: a feed pipe (102) is arranged at the top of the sealing cover (103) near the front side in a penetrating way.
6. The apparatus for continuous reaction of m-cresol alkylation according to claim 1, wherein: the discharging structure (2) comprises a discharging pipe (201), an electromagnetic valve (202) is fixedly arranged on the outer surface of the discharging pipe (201), and the inside of the discharging pipe (201) is communicated with the inside of the heating separation tank (110).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321137955.2U CN220460655U (en) | 2023-05-09 | 2023-05-09 | Device for continuous reaction of m-cresol alkylation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321137955.2U CN220460655U (en) | 2023-05-09 | 2023-05-09 | Device for continuous reaction of m-cresol alkylation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220460655U true CN220460655U (en) | 2024-02-09 |
Family
ID=89799257
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321137955.2U Active CN220460655U (en) | 2023-05-09 | 2023-05-09 | Device for continuous reaction of m-cresol alkylation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220460655U (en) |
-
2023
- 2023-05-09 CN CN202321137955.2U patent/CN220460655U/en active Active
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