CN220443494U - Adsorption tower and by-product silicon oil and potassium fluoride recovery separation purifier - Google Patents
Adsorption tower and by-product silicon oil and potassium fluoride recovery separation purifier Download PDFInfo
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- CN220443494U CN220443494U CN202321832178.3U CN202321832178U CN220443494U CN 220443494 U CN220443494 U CN 220443494U CN 202321832178 U CN202321832178 U CN 202321832178U CN 220443494 U CN220443494 U CN 220443494U
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- filling layer
- adsorbent
- motor
- filling
- tower body
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- 238000001179 sorption measurement Methods 0.000 title claims abstract description 29
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 title claims abstract description 24
- 235000003270 potassium fluoride Nutrition 0.000 title claims abstract description 12
- 239000011698 potassium fluoride Substances 0.000 title claims abstract description 12
- 238000000926 separation method Methods 0.000 title claims abstract description 9
- 239000006227 byproduct Substances 0.000 title claims abstract description 8
- 238000011084 recovery Methods 0.000 title claims abstract description 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title abstract description 3
- 239000003921 oil Substances 0.000 title abstract description 3
- 229910052710 silicon Inorganic materials 0.000 title abstract description 3
- 239000010703 silicon Substances 0.000 title abstract description 3
- 239000003463 adsorbent Substances 0.000 claims abstract description 75
- 238000007789 sealing Methods 0.000 claims abstract description 29
- 230000005540 biological transmission Effects 0.000 claims abstract description 21
- 238000000746 purification Methods 0.000 claims abstract description 6
- 230000001681 protective effect Effects 0.000 claims description 12
- 229920002545 silicone oil Polymers 0.000 claims description 9
- 229920001971 elastomer Polymers 0.000 claims description 8
- 230000008878 coupling Effects 0.000 claims description 4
- 238000010168 coupling process Methods 0.000 claims description 4
- 238000005859 coupling reaction Methods 0.000 claims description 4
- 230000009471 action Effects 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 230000000149 penetrating effect Effects 0.000 abstract description 2
- 229920006395 saturated elastomer Polymers 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 230000004075 alteration Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
The utility model relates to the technical field of adsorption towers, in particular to an adsorption tower and a byproduct silicon oil and potassium fluoride recovery, separation and purification device, which comprises: the tower body is characterized in that a filling layer is fixed on the inner wall of the tower body, a cavity is formed in the filling layer, blades are rotatably connected in the cavity of the filling layer, an adsorbent inlet and outlet are formed in the side face of the filling layer, the adsorbent inlet and outlet are communicated with an adsorbent replacement port, and the adsorbent replacement port is formed in the surface of the tower body; the beneficial effects are as follows: the top end of the top cover of the filling layer on the uppermost layer is provided with a motor, a transmission shaft penetrating through all the filling layers is driven to rotate, blades are driven to rotate in each layer of filling layers through a rotating disc on the rotation shaft, sealing blocks on the surfaces of the filling layers needing to be replaced with adsorbents are opened, the adsorbents in the filling layers are thrown out of the adsorption tower from the adsorbent inlet and outlet and the adsorbent replacement port by utilizing the action of centrifugal force, new adsorbents are added, and replacement of the adsorbents without disassembling the tower is achieved, so that a large amount of manpower is saved.
Description
Technical Field
The utility model relates to the field of adsorption towers, in particular to an adsorption tower and a byproduct silicone oil and potassium fluoride recovery, separation and purification device.
Background
The adsorption tower is a device for filling solid adsorbent in the tower, so that certain components in gas or liquid entering the tower are adsorbed by the porous structure of the adsorbent, thereby realizing component separation.
In the prior art, when silicone oil and potassium fluoride are recovered, separated and purified, an adsorption tower with a plurality of adsorbents is adopted, the adsorbents with different types of substances capable of being adsorbed are utilized, an adsorbent filling layer is placed in a certain sequence, then gas or liquid containing the silicone oil and the potassium fluoride is introduced into the adsorption tower to fully contact with each layer of adsorbent, after the adsorption is completed, the adsorbent filling layer is detached from the adsorption tower, and then the silicone oil and the potassium fluoride are separated from the adsorbents by adopting a plurality of methods, so that the separated and purified silicone oil and potassium fluoride can be obtained.
However, when the adsorption treatment is performed, the adsorbent must be stopped immediately after reaching the saturated state, and the service time of each layer of adsorbent reaching the saturated state is different, in the prior art, when the adsorbent positioned at the lower layer reaches the saturated state in advance, the adsorbent filling layers positioned at the upper layer are required to be completely removed, and the adsorbent filling layers reaching the saturated state can be removed to replace the adsorbent and then be packaged one by one to continue the adsorption treatment, which leads to a great amount of manpower waste.
Disclosure of Invention
The utility model aims to provide an adsorption tower and a recovery, separation and purification device for byproduct silicone oil and potassium fluoride, so as to solve the problems in the background technology.
In order to achieve the above purpose, the present utility model provides the following technical solutions: an adsorption tower is provided with a plurality of adsorption columns,
comprising the following steps: the tower body is fixed with the filling layer on the inner wall of tower body, has seted up the cavity in the filling layer, swivelling joint has the blade in the cavity of filling layer, and the adsorbent inlet and outlet has been seted up to the side of filling layer, and the adsorbent inlet and outlet link up with the adsorbent change mouth, and the adsorbent is changed the mouth and is seted up on the surface of tower body.
Preferably, the filling layer is provided with two sets of, and two sets of filling layers distribute from top to bottom, and the top of filling layer is fixed with the filling layer top cap, and the through-hole has all been seted up to the centre of filling layer and filling layer top cap, and the top of filling layer top cap that is located the upper strata is fixed with motor protective housing, and motor protective housing's top is connected with motor protective cover, and motor protective cover's bottom mounting has rubber seal, and rubber seal's bottom supports on motor protective housing's top surface.
Preferably, the motor protective housing is annular cylinder structure, be fixed with the motor in the motor protective housing, be connected with the shaft coupling on the motor shaft of motor, the bottom of shaft coupling is connected with the transmission shaft, the surface cover of transmission shaft is established and is fixed with the bearing inner ring, the bearing inner ring is annular cylinder structure, swivelling joint has ball and waterproof seal on the outer ring surface of bearing inner ring, waterproof seal is equipped with two sets of, two sets of waterproof seal are about ball symmetric distribution, the ball is equipped with the multiunit, the ball is kept away from the bearing outer ring with waterproof seal and is equipped with the bearing outer ring on the one end surface of bearing inner ring, the bearing outer ring is annular cylinder structure, the outer ring of bearing outer ring is fixed in the through-hole of the filling layer top cap of upper strata, the transmission shaft still swivelling joint is in the through-hole of seting up in the middle of other filling layer top caps and the filling layer.
Preferably, a plurality of groups of blades are arranged in each group of filling layers, one ends of the plurality of groups of blades are fixed on the surface of the same group of rotating discs, the rotating discs are of annular cylinder structures, the inner rings of the rotating discs are sleeved on the surface of the transmission shaft, key grooves are formed in the positions, corresponding to the inner rings of the rotating discs and the transmission shaft, of the rotating discs, and flat keys are movably inserted in the key grooves.
Preferably, a boss is arranged at the position of the adsorbent inlet and outlet arranged on the surface of the filling layer, a guide hole is arranged on the boss, a guide rod is movably inserted in the guide hole, a sealing block is fixed at one end of the guide rod extending out of the guide hole, one end of the sealing block, which is fixed with the guide rod, is propped against the surface of the boss, the sealing block is movably inserted in the adsorbent replacement port, a boss is arranged at the position of the tower body, which is provided with the adsorbent replacement port, and a screw connection is arranged between the sealing block and the boss on the surface of the tower body.
A recovery, separation and purification device for byproduct silicone oil and potassium fluoride comprises an adsorption tower.
Compared with the prior art, the utility model has the beneficial effects that:
according to the adsorption tower and the recovery, separation and purification device for byproduct silicone oil and potassium fluoride, the motor is arranged at the top end of the top cover of the uppermost filling layer to drive the transmission shaft penetrating through all the filling layers to rotate, the rotating disc drives the blades to rotate in each filling layer on the rotation shaft, the sealing blocks on the surface of the filling layer needing to be replaced with the adsorbent are opened, the adsorbent in the filling layer is thrown out of the adsorption tower from the adsorbent inlet and outlet and the adsorbent replacement opening by utilizing the action of centrifugal force, and then new adsorbent is added, so that the replacement of the adsorbent without disassembling the tower is realized, and a great deal of manpower is saved.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is an enlarged schematic view of the structure A in FIG. 1;
FIG. 3 is a schematic view of a multi-layer fill layer structure;
FIG. 4 is a schematic cross-sectional view of a multi-layer fill layer;
FIG. 5 is an enlarged schematic view of the structure shown at B in FIG. 4;
FIG. 6 is a schematic diagram of the internal structure of the filling layer;
FIG. 7 is a schematic diagram of a plugging structure of a sealing block;
fig. 8 is an enlarged schematic view of the structure at C in fig. 7.
In the figure: the tower body 1, the adsorbent replacement port 2, the sealing block 3, the filling layer 4, the filling layer top cover 5, the motor protection shell 6, the rubber sealing ring 7, the motor protection cover 8, the transmission shaft 9, the motor 10, the coupler 11, the bearing outer ring 12, the ball 13, the waterproof sealing ring 14, the bearing inner ring 15, the flat key 16, the rotary disk 17, the blades 18, the retainer 19, the guide hole 20 and the guide rod 21.
Detailed Description
In order to make the objects, technical solutions, and advantages of the present utility model more apparent, the embodiments of the present utility model will be further described in detail with reference to the accompanying drawings. It should be understood that the specific embodiments described herein are some, but not all, embodiments of the present utility model, are intended to be illustrative only and not limiting of the embodiments of the present utility model, and that all other embodiments obtained by persons of ordinary skill in the art without making any inventive effort are within the scope of the present utility model.
Example 1
Referring to fig. 1-8, the present utility model provides a technical solution: an adsorption column comprising: the tower body 1 is fixed with filling layer 4 on the inner wall of tower body 1, has seted up the cavity in the filling layer 4, its characterized in that: the cavity of the filling layer 4 is rotatably connected with blades 18, the side surface of the filling layer 4 is provided with an adsorbent inlet and outlet 19, the adsorbent inlet and outlet 19 is communicated with the adsorbent replacement port 2, and the adsorbent replacement port 2 is arranged on the surface of the tower body 1.
Example two
On the basis of the first embodiment, in order to prevent the absorbed gas or liquid from invading the motor and causing damage to the motor, the top end of the filling layer top cover 5 located on the upper layer is fixed with the motor protection shell 6, the top end of the motor protection shell 6 is connected with the motor protection cover 8, the bottom end of the motor protection cover 8 is fixed with the rubber seal ring 7, the bottom end of the rubber seal ring 7 is propped against the top end surface of the motor protection shell 6, the motor protection shell 6 is of an annular cylinder structure, the motor 10 is fixed in the motor protection shell 6, the motor shaft of the motor 10 is connected with the coupler 11, the bottom end of the coupler 11 is connected with the transmission shaft 9, the surface of the transmission shaft 9 is sleeved and fixed with the bearing inner ring 15, the bearing inner ring 15 is of an annular cylinder structure, the outer ring surface of the bearing inner ring 15 is rotationally connected with the balls 13 and the waterproof seal ring 14, the waterproof seal ring 14 is provided with two groups, the two groups of waterproof seal rings 14 are symmetrically distributed about the balls 13, the balls 13 and the waterproof seal ring 14 are sleeved with the bearing outer ring 12 on one end surface far away from the bearing inner ring 15, the bearing outer ring 12 is of the annular cylinder structure, and the outer ring of the bearing outer ring 12 is of the annular ring is fixed in the through hole of the filling layer top cover 5 on the upper layer.
Example III
On the basis of the second embodiment, in order to realize that one motor drives blades in each filling layer to rotate, the transmission shaft 9 is also rotationally connected in through holes formed in the middle of the top cover 5 of other filling layers and the filling layer 4, a plurality of groups of blades 18 are arranged in each group of filling layers 4, one ends of the plurality of groups of blades 18 are fixed on the surface of the same group of rotating discs 17, the rotating discs 17 are in an annular cylinder structure, the inner rings of the rotating discs 17 are sleeved on the surface of the transmission shaft 9, key grooves are formed in the positions corresponding to the inner rings of the rotating discs 17 and the transmission shaft 9, and flat keys 16 are movably inserted in the key grooves.
Example IV
On the basis of the third embodiment, in order to throw out the adsorbent in the specific filling layer, a boss is arranged at a position on the surface of the filling layer 4, on which the adsorbent inlet and outlet 19 is formed, a guide hole 20 is formed on the boss, a guide rod 21 is movably inserted in the guide hole 20, one end of the guide rod 21 extending out of the guide hole 20 is fixed with a sealing block 3, one end of the sealing block 3, on which the guide rod 21 is fixed, abuts against the boss surface, the sealing block 3 is movably inserted in the adsorbent replacing port 2, a boss is arranged at a position on the tower body 1, on which the adsorbent replacing port 2 is formed, and a screw connection is arranged between the sealing block 3 and the boss on the surface of the tower body 1.
In actual use, the rotation speed of the motor 10 fixed in the motor protection shell 6 is in high and low grade, screws used for connecting the motor protection shell 8 and the motor protection shell 6 are screwed up before the adsorption tower performs adsorption work, so that the bottom end of the rubber sealing ring 7 is pressed on the surface of the motor protection shell 6, and meanwhile, the tightness of a waterproof bearing consisting of the bearing outer ring 12, the ball 13, the waterproof sealing ring 14 and the bearing inner ring 15 is checked, so that adsorbed gas is prevented from entering the inside of the motor protection shell 6, and damage is caused to the motor 10; when the adsorbent needs to be replaced on a filling layer 4 of a certain layer, screws on the surface of a sealing block 3 of the layer are detached from the surface of a tower body 1, then the sealing block 3 of the layer is pulled outwards, the sealing block 3 is withdrawn from an adsorbent replacing port 2, a guide rod 21 extends out of a guide hole 20 for a certain distance, a container for receiving the adsorbent is ready below the sealing block 3, then a motor 10 is made to run in a high grade, a motor shaft of the motor 10 drives a transmission shaft 9 to rotate at a high speed through a coupler 11, the transmission shaft 9 penetrates through a through hole in the middle of a top cover 5 of the filling layer to drive a rotary disc 17 in each layer 4 to rotate through a flat key 16, the adsorbent is filled between each group of blades 18, the rotary disc 17 drives the blades 18 to rotate at a high speed, the blades 18 push the adsorbent to rotate around the axis of the transmission shaft 9, under the action of centrifugal force, the adsorbent is thrown outwards, then is thrown out of the adsorbent from the adsorbent inlet 19 and the adsorbent replacing port 2, drops into the prepared container on the inner wall of the sealing block 3, the motor is driven by the coupler 11, the rotary disc 9 drives the rotary disc 17 in the middle of the filling layer 4 to rotate at a high speed through the flat key 16, the rotary disc 17 is completely rotates around the axis of the adsorbent replacing port 9, and the adsorbent is thrown into the adsorbent is completely replaced at the position of the adsorbent replacing port 2, and the adsorbent is completely replaced in the low speed, and the position of the adsorbent is completely replaced by the adsorbent layer 4, and the adsorbent is completely and replaced by the adsorbent layer is completely, and replaced by the adsorbent layer is slowly, and the adsorbent is thrown and the adsorbent is slowly, and the adsorbent is completely and replaced.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. An adsorption column comprising: the tower body (1), be fixed with filling layer (4) on the inner wall of tower body (1), seted up the cavity in filling layer (4), its characterized in that: the cavity of the filling layer (4) is rotationally connected with a blade (18), the side surface of the filling layer (4) is provided with an adsorbent inlet and outlet (19), the adsorbent inlet and outlet (19) is communicated with the adsorbent replacement port (2), and the adsorbent replacement port (2) is arranged on the surface of the tower body (1).
2. An adsorption column according to claim 1, wherein: the filling layer (4) is provided with two sets of, and two sets of filling layer (4) distribute from top to bottom, and the top of filling layer (4) is fixed with filling layer top cap (5), and the through-hole has all been seted up in the centre of filling layer (4) and filling layer top cap (5), and the top of filling layer top cap (5) that is located the upper strata is fixed with motor protective housing (6), and motor protective housing (6) top is connected with motor protective housing (8), and motor protective housing (8) bottom mounting has rubber seal (7), and the bottom of rubber seal (7) supports on motor protective housing (6) top surface.
3. An adsorption column according to claim 2, wherein: the motor protection shell (6) is annular cylinder structure, be fixed with motor (10) in motor protection shell (6), be connected with shaft coupling (11) on the motor shaft of motor (10), the bottom of shaft coupling (11) is connected with transmission shaft (9), the surface cover of transmission shaft (9) is established and is fixed with bearing inner ring (15), bearing inner ring (15) are annular cylinder structure, swivelling joint has ball (13) and waterproof sealing ring (14) on the outer ring surface of bearing inner ring (15), waterproof sealing ring (14) are equipped with two sets of, two sets of waterproof sealing ring (14) are about ball (13) symmetric distribution, ball (13) are equipped with the multiunit, ball (13) and waterproof sealing ring (14) keep away from on the one end surface cover of bearing inner ring (15) and are equipped with bearing outer ring (12), bearing outer ring (12) are annular cylinder structure, the outer ring of bearing outer ring (12) is fixed in the through-hole of filling layer top cap (5) on the upper strata, transmission shaft (9) still swivelling joint is in the through-hole of seting up in the middle of other filling layer top cap (5) and filling layer (4).
4. An adsorption column according to claim 1, wherein: the novel rotary disc is characterized in that a plurality of groups of blades (18) are arranged in each group of filling layers (4), one ends of the plurality of groups of blades (18) are fixed on the surface of the same group of rotary discs (17), the rotary discs (17) are of annular cylinder structures, the inner rings of the rotary discs (17) are sleeved on the surface of the transmission shaft (9), key grooves are formed in the positions, corresponding to the inner rings of the rotary discs (17) and the transmission shaft (9), of the rotary discs, and flat keys (16) are movably inserted in the key grooves.
5. An adsorption column according to claim 1, wherein: the filling layer (4) is characterized in that a boss is arranged at the position of the adsorbent inlet and outlet (19) formed in the surface of the filling layer (4), a guide hole (20) is formed in the boss, a guide rod (21) is movably inserted in the guide hole (20), one end of the guide rod (21) extending out of the guide hole (20) is fixedly provided with a sealing block (3), one end of the sealing block (3) fixedly provided with the guide rod (21) is abutted to the surface of the boss, the sealing block (3) is movably inserted in the adsorbent replacement port (2), a boss is arranged at the position of the tower body (1) provided with the adsorbent replacement port (2), and a screw connection is arranged between the sealing block (3) and the boss on the surface of the tower body (1).
6. A recovery, separation and purification device for byproduct silicone oil and potassium fluoride is characterized in that: an adsorption column comprising any one of claims 1-5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321832178.3U CN220443494U (en) | 2023-07-12 | 2023-07-12 | Adsorption tower and by-product silicon oil and potassium fluoride recovery separation purifier |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321832178.3U CN220443494U (en) | 2023-07-12 | 2023-07-12 | Adsorption tower and by-product silicon oil and potassium fluoride recovery separation purifier |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220443494U true CN220443494U (en) | 2024-02-06 |
Family
ID=89739298
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321832178.3U Active CN220443494U (en) | 2023-07-12 | 2023-07-12 | Adsorption tower and by-product silicon oil and potassium fluoride recovery separation purifier |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220443494U (en) |
-
2023
- 2023-07-12 CN CN202321832178.3U patent/CN220443494U/en active Active
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