CN220371803U - Drum-type washing deionization equipment for nano rare earth oxide - Google Patents
Drum-type washing deionization equipment for nano rare earth oxide Download PDFInfo
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- CN220371803U CN220371803U CN202321654453.7U CN202321654453U CN220371803U CN 220371803 U CN220371803 U CN 220371803U CN 202321654453 U CN202321654453 U CN 202321654453U CN 220371803 U CN220371803 U CN 220371803U
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- Prior art keywords
- barrel
- stirring
- rare earth
- rotating motor
- reaction
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- 238000005406 washing Methods 0.000 title claims abstract description 38
- 229910001404 rare earth metal oxide Inorganic materials 0.000 title claims abstract description 23
- 238000002242 deionisation method Methods 0.000 title claims abstract description 14
- 238000003756 stirring Methods 0.000 claims abstract description 55
- 238000006243 chemical reaction Methods 0.000 claims abstract description 32
- 230000005611 electricity Effects 0.000 claims abstract description 8
- 230000005540 biological transmission Effects 0.000 claims description 3
- 230000001360 synchronised effect Effects 0.000 claims description 2
- 230000003028 elevating effect Effects 0.000 claims 1
- 230000005684 electric field Effects 0.000 abstract description 12
- 239000008188 pellet Substances 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 7
- 239000007788 liquid Substances 0.000 abstract description 6
- 230000009471 action Effects 0.000 abstract description 5
- 150000002500 ions Chemical class 0.000 abstract description 4
- 229910001415 sodium ion Inorganic materials 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 238000000034 method Methods 0.000 description 5
- 229910052761 rare earth metal Inorganic materials 0.000 description 5
- 150000002910 rare earth metals Chemical class 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 206010053615 Thermal burn Diseases 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 206010019345 Heat stroke Diseases 0.000 description 1
- 150000004703 alkoxides Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
Landscapes
- Water Treatment By Electricity Or Magnetism (AREA)
Abstract
The utility model provides drum-type washing deionization equipment for nano rare earth oxide, which comprises a reaction barrel, a rotating motor, a conductive electrode and a stirring barrel, wherein the reaction barrel is arranged on the bottom of the reaction barrel; the conductive electrode outputs positive electrode wiring and negative electrode wiring respectively, a plurality of pellets are filled in the stirring barrel, the stirring barrel and the pellets can conduct electricity, one stirring barrel is connected with the positive electrode wiring, and the other stirring barrel is connected with the negative electrode wiring. The utility model has reasonable structural design, and the rotating motor is utilized to drive the stirring barrel to rotate relative to the reaction barrel, thereby realizing the drum-type washing operation; an electric field force is introduced to form an electric field with positive electrodes pointing to negative electrodes in the feed liquid, and positive and negative ions move towards positive (positive) tiny balls and are adsorbed on the balls under the action of the electric field force, and sodium ions move towards negative (negative) tiny balls and are adsorbed, so that the effect of washing and deionizing is achieved.
Description
Technical Field
The utility model relates to the technical field of rare earth oxide preparation, in particular to drum-type water washing deionization equipment for nano rare earth oxide.
Background
Rare earth is an important mineral resource. The nano rare earth integrates rare earth characteristics and nano characteristics, and is a hot spot for utilizing rare earth resources. The nano rare earth oxide is an important constituent of the nano rare earth material. In the preparation process of the nano rare earth oxide, a sol-gel method, an alkoxide method, a complex precipitation method, a homogeneous precipitation method, a hydrothermal method, a hydrolysis method, a thermal decomposition method and the like can be adopted. In the preparation of nano rare earth oxides, water washing is generally used to remove ions.
Traditional washing deionized water requires manual washing, the environment is stuffy, hot water is easy to scald personnel, feed liquid is heavy and easy to heatstroke, and the situation that local washing is uneven can also occur. For this situation, CN211035262U discloses a rare earth oxide production water washing device, which conveys multiple groups of rare earth oxide solutions or rare earth oxide solutions with different components into different placing cavities through two feeding hoppers to wash, improves the washing efficiency of a washing box body, and drives a filter plate to rotate through a rotating motor, so that the rare earth oxide in the rare earth oxide solution can be uniformly placed on the filter plate to carry out washing operation. The washing device designed in this way adopts the cooperation of the motor and the washing mechanism to replace manual washing, but has no special design in the deionization operation and has room for improvement.
Disclosure of Invention
The utility model aims to solve the technical problems that: in order to overcome the defects of the prior art, the utility model provides the drum-type washing deionization equipment for the nano rare earth oxide, which utilizes the action of an electric field force to realize the washing deionization operation of the nano rare earth oxide through the cooperation of a rotating motor and a conductive electrode, has high working efficiency and good product quality, and effectively reduces the water consumption.
The technical scheme adopted for solving the technical problems is as follows: a drum-type washing deionization device for nano rare earth oxide comprises a reaction barrel, a rotating motor, a conductive electrode and a stirring barrel; the conductive electrode outputs positive electrode wiring and negative electrode wiring respectively, the number of the stirring barrels is two, a plurality of small balls are filled in the stirring barrels, the stirring barrels and the small balls can conduct electricity, one stirring barrel is connected with the positive electrode wiring, and the other stirring barrel is connected with the negative electrode wiring; the top of the reaction barrel is provided with an opening, the rotating motor is arranged above the opening, the output end of the rotating motor stretches into the opening, the two stirring barrels are separated and are simultaneously arranged in the reaction barrel, and the stirring barrels are respectively connected with the output end of the rotating motor in a transmission way and are driven to rotate by the rotating motor.
In the scheme, through the arrangement of the conductive electrode, after the stirring barrel filled with the pellets is connected with the electrode, electrons are lost from the pellets on one side of the positive electrode due to the existence of the electromotive force of the electrode, and positive electricity is displayed; the ball on one side of the negative electrode cleans electrons and displays negative electricity. Thus, an electric field is formed in the feed liquid from the positive electrode to the negative electrode. Under the action of electric field force, the chloride ions move to the positive (negative) tiny spheres and are adsorbed on the spheres, and the sodium ions move to the (negative) tiny spheres and are adsorbed to achieve the effect of removal.
In order to further save labor, a lifter is arranged above the reaction barrel, the rotating motor is fixed at the output end of the lifter, and the lifter synchronously drives the stirring barrel to do lifting motion relative to the reaction barrel by driving the rotating motor.
Preferably, the stirring barrel is of a cylindrical barrel structure with a semicircular radial section, the barrel wall and the barrel bottom of the cylindrical barrel structure are made of grid plates, the two stirring barrels are arranged in the reaction barrel in a central symmetry mode by taking the axis of the reaction barrel as a symmetry line, and the radius of the semicircular section of the cylindrical barrel structure is smaller than the inner diameter of the reaction barrel.
The drum-type washing deionization device for the nano rare earth oxide has the beneficial effects that the drum-type washing deionization device for the nano rare earth oxide is reasonable in structural design, and the rotating motor is utilized to drive the stirring barrel to rotate relative to the reaction barrel, so that drum-type washing operation is realized; the stirring barrel is divided, the stirring barrel is respectively connected with the pellets on two sides of the division through the conductive electrodes, an electric field with the positive electrode pointing to the negative electrode is formed in the feed liquid, positive and negative ions move towards the positive (positive) minimum pellets and are adsorbed on the pellets under the action of the electric field, sodium ions move towards the (negative) negative pellets and are adsorbed to achieve the effect of removing ions, the product quality is effectively improved, the working efficiency is improved, the manpower is fully liberated, manual water washing is not needed, the water consumption is reduced, the scalding of personnel is avoided, and the labor intensity is better reduced.
Drawings
The utility model will be further described with reference to the drawings and examples.
Fig. 1 is a schematic view of the structure of the preferred embodiment of the present utility model (the arrow direction is the rotation direction of the stirring barrel).
In the figure, 1, a reaction barrel 2, a stirring barrel 3, a small ball 4, a conductive electrode 5, a rotary motor 6 and a lifter.
Detailed Description
The utility model will now be described in further detail with reference to the accompanying drawings. The drawings are simplified schematic representations which merely illustrate the basic structure of the utility model and therefore show only those features which are relevant to the utility model, and orientation and reference (e.g., up, down, left, right, etc.) may be used solely to aid in the description of the features in the drawings. The following detailed description is, therefore, not to be taken in a limiting sense, and the scope of the claimed subject matter is defined only by the appended claims and equivalents thereof.
The drum-type water-washing deionization equipment for nano rare earth oxide shown in fig. 1 is the optimal embodiment of the utility model.
The apparatus comprises a reaction tank 1, a rotary motor 5, a conductive electrode 4 and a stirring tank 2. The reaction barrel 1 has an opening at the top and a solution feed opening at the bottom. The upper part corresponding to the open position of the reaction barrel 1 can be provided with a lifter 6, the rotating motor 5 is positioned above the open position and fixed at the output end of the lifter 6, the output end of the rotating motor 5 stretches into the open position, the number of the stirring barrels 2 is two, the two stirring barrels 2 are separated and arranged in the reaction barrel 1 at the same time, and the stirring barrels 2 are respectively connected with the output end of the rotating motor 5 in a transmission way and are driven to rotate by the rotating motor 5. The elevator 6 is through driving rotating electrical machines 5 and synchronous drive will be equipped with the agitator 2 of ball 3 in with reaction barrel 1, elevator 6 and rotating electrical machines 5's setting can make the washing operation need not artifical washing, has effectively liberated the manpower, when improving work efficiency, has reduced the high temperature scald risk when artifical washing.
On the basis of releasing manpower, the embodiment also introduces the effect of electric field force, further improves the effect of washing and deionizing, and optimizes the product quality. Specifically, the conductive electrodes 4 are respectively output with positive and negative electrode wirings. The stirring barrel 2 is filled with a plurality of pellets 3, and both the stirring barrel 2 and the pellets 3 can conduct electricity. Of the two stirring barrels 2, one stirring barrel 2 is connected with a positive electrode wiring, and the other stirring barrel 2 is connected with a negative electrode wiring.
In practical design, the stirring barrels 2 are cylindrical barrel structures with semicircular radial sections, the barrel walls and barrel bottoms of the cylindrical barrel structures are made of grid plates, the two stirring barrels 2 are symmetrically distributed in the reaction barrel 1 by taking the axis of the reaction barrel 1 as a symmetry line, the two stirring barrels 2 are spaced, and the prepared nano oxide solution is filled in the space among the stirring barrels 2, the small balls 3 and the inner wall of the reaction barrel 1. Meanwhile, in this embodiment, the conductive electrode 4 is disposed below the rotating motor 5, and the conductive electrode 4 is connected with the two stirring tanks 2 respectively, and the connection needs to ensure that the rotation of the rotating motor 5 to drive the stirring tanks 5 to rotate for washing does not interfere with the connection between the conductive electrode 4 and the stirring tanks 5.
During the washing operation, the prepared nano oxide solution is pumped into the reaction barrel 1, the stirring device with the conductive pellets 3 is lowered into the reaction barrel 1 by the lifter 6, the conductive electrode 4 is opened, the left grid stirring barrel 2 is communicated with the anode, and the right grid stirring barrel 2 is communicated with the cathode. The small balls 3 are made of conductive materials, and after the stirring barrel 2 provided with the small balls 3 is connected with an electrode, electrons are lost from the small balls 3 on one side of the positive electrode due to the existence of electrode electromotive force, and positive electricity is displayed; the ball 3 on one side of the negative electrode is used for cleaning the electrons and displaying negative electricity. Thus, an electric field is formed in the feed liquid from the positive electrode to the negative electrode. Under the action of electric field force, the chloride ions move to the positive (positive) tiny balls 3 and are adsorbed on the small balls 3, and the sodium ions move to the negative tiny balls 3 and are adsorbed to achieve the effect of removal.
Meanwhile, the rotating motor 5 can be synchronously started, the rotating motor 5 drives the stirring barrel 2 to rotate, and a drum-type washing operation is formed, so that feed liquid is fully contacted with the pellets 3 in the grid stirring barrel 2, the effect of washing the inner parts with water is further improved, the operation of washing with water to remove sodium chloride ions can be performed on nano rare earth oxide, manual washing is not needed, manpower is fully liberated, the labor intensity is reduced, personnel scalding is avoided, electric field force is effectively utilized, and water consumption is reduced for colleagues who improve the product quality.
With the above-described preferred embodiments according to the present utility model as an illustration, the above-described descriptions can be used by persons skilled in the relevant art to make various changes and modifications without departing from the scope of the technical idea of the present utility model. The technical scope of the present utility model is not limited to the description, but must be determined according to the scope of claims.
Claims (3)
1. A drum-type washing deionization device for nano rare earth oxide is characterized in that: comprises a reaction barrel (1), a rotating motor (5), a conductive electrode (4) and a stirring barrel (2); the conductive electrode (4) is respectively provided with an anode wiring and a cathode wiring, the number of the stirring barrels (2) is two, a plurality of small balls (3) are filled in the stirring barrels (2), the stirring barrels (2) and the small balls (3) can conduct electricity, one stirring barrel (2) is connected with the anode wiring, and the other stirring barrel (2) is connected with the cathode wiring;
the top of the reaction barrel (1) is provided with an opening, the rotating motor (5) is arranged above the opening, the output end of the rotating motor (5) stretches into the opening, the two stirring barrels (2) are separated and are arranged in the reaction barrel (1) at the same time, and the stirring barrels (2) are respectively connected with the output end of the rotating motor (5) in a transmission way and are driven to rotate by the rotating motor (5).
2. The nano rare earth oxide drum-type water-washing deionization apparatus as claimed in claim 1, wherein: the reaction barrel (1) top be equipped with lift (6), rotating electrical machines (5) then fix the output at lift (6), lift (6) through driving rotating electrical machines (5) and synchronous drive agitator (2) and do elevating movement for reaction barrel (1).
3. The nano rare earth oxide drum-type water-washing deionization apparatus as claimed in claim 1, wherein: the stirring barrels (2) are cylindrical barrel structures with semicircular radial sections, the barrel walls and barrel bottoms of the cylindrical barrel structures are made of grid plates, the two stirring barrels (2) are symmetrically distributed in the reaction barrel (1) by taking the axis of the reaction barrel (1) as a symmetry line, and the semicircular radius of the sections of the cylindrical barrel structures is smaller than the inner diameter of the reaction barrel (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321654453.7U CN220371803U (en) | 2023-06-27 | 2023-06-27 | Drum-type washing deionization equipment for nano rare earth oxide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321654453.7U CN220371803U (en) | 2023-06-27 | 2023-06-27 | Drum-type washing deionization equipment for nano rare earth oxide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220371803U true CN220371803U (en) | 2024-01-23 |
Family
ID=89560022
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321654453.7U Active CN220371803U (en) | 2023-06-27 | 2023-06-27 | Drum-type washing deionization equipment for nano rare earth oxide |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220371803U (en) |
-
2023
- 2023-06-27 CN CN202321654453.7U patent/CN220371803U/en active Active
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