CN220357022U - Degradable microporous material degradation performance detection device - Google Patents
Degradable microporous material degradation performance detection device Download PDFInfo
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- CN220357022U CN220357022U CN202321634972.7U CN202321634972U CN220357022U CN 220357022 U CN220357022 U CN 220357022U CN 202321634972 U CN202321634972 U CN 202321634972U CN 220357022 U CN220357022 U CN 220357022U
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- 238000001514 detection method Methods 0.000 title claims abstract description 71
- 239000012229 microporous material Substances 0.000 title claims abstract description 44
- 238000005297 material degradation process Methods 0.000 title claims abstract description 21
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 68
- 238000006243 chemical reaction Methods 0.000 claims abstract description 67
- 238000003756 stirring Methods 0.000 claims abstract description 55
- 239000000463 material Substances 0.000 claims description 21
- 238000012360 testing method Methods 0.000 claims description 9
- 230000015556 catabolic process Effects 0.000 claims description 7
- 238000006731 degradation reaction Methods 0.000 claims description 7
- 239000011521 glass Substances 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 230000009286 beneficial effect Effects 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 238000000034 method Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 238000007599 discharging Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000010669 acid-base reaction Methods 0.000 description 1
- 238000004630 atomic force microscopy Methods 0.000 description 1
- 239000007857 degradation product Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000003808 methanol extraction Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000012667 polymer degradation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000002411 thermogravimetry Methods 0.000 description 1
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- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
Abstract
The utility model provides a degradable microporous material degradation performance detection device, which belongs to the technical field of performance detection and comprises a reaction kettle, a detection mechanism, a stirring mechanism and a reagent structure, wherein the detection mechanism penetrates through the reaction kettle and is arranged in the reaction kettle, the detection mechanism is used for detecting microporous materials in the reaction kettle, the stirring mechanism is arranged in the reaction kettle and is used for stirring the microporous materials in the reaction kettle, the reagent structure is arranged in the stirring mechanism, the reagent structure comprises a reagent pipeline, a perforation and a reagent pipe, the reagent pipeline is arranged in the stirring mechanism, one end of the reagent pipeline is connected to the perforation, and the reagent structure is used for introducing reagents into the reaction kettle.
Description
Technical Field
The utility model belongs to the technical field of performance detection, and particularly relates to a degradation performance detection device for a degradable microporous material.
Background
With the increasing awareness of global environmental protection, more and more research into polymeric materials has focused on degradable polymeric materials and attempted to be applied to various fields, particularly in the fields of disposable materials and biomedical science. Degradable polymeric materials have important advantages including degradability, environmental friendliness and biocompatibility. Degradability means that the polymer can be degraded by the natural environment. By environmentally friendly it is meant that the polymer degradation products do not cause environmental pollution.
As the demand for degradable materials increases, attention is increasingly paid. And the degradation performance test and evaluation of the degradable material become a key technology. Currently, researchers have adopted a number of methods to test their degradation properties for different degradable materials, such as mass spectrometry, thermogravimetric analysis, methanol extraction, atomic force microscopy, etc. However, these methods have disadvantages such as high equipment cost, long test time, low test accuracy, and the like. Therefore, there is an urgent need for a simple, convenient, and accurate method for testing the degradation properties of degradable materials.
In the existing detection of the performance of the degradation material, the problems of long detection time and low detection precision exist.
Disclosure of Invention
In view of the above, the utility model provides a degradable microporous material degradation performance detection device, which can solve the problems of long detection time and low detection precision.
The utility model is realized in the following way:
the utility model provides a degradable microporous material degradation performance detection device which comprises a reaction kettle, a detection mechanism, a stirring mechanism and a reagent structure, wherein the detection mechanism penetrates through the reaction kettle and is arranged in the reaction kettle, the detection mechanism is used for detecting microporous materials in the reaction kettle, the stirring mechanism is arranged in the reaction kettle and is used for stirring the microporous materials in the reaction kettle, the reagent structure is arranged in the stirring mechanism, the reagent structure comprises a reagent pipeline, a perforation and a reagent pipe, the reagent pipeline is arranged in the stirring mechanism, one end of the reagent pipeline is connected to the perforation, and the reagent structure is used for guiding reagents into the reaction kettle.
The technical effects of the degradable microporous material degradation performance detection device provided by the utility model are as follows: the reaction kettle can provide enough space for the reaction of microporous materials and reagents, the reaction kettle has the effect of providing reaction efficiency, the microporous materials reacting with the reagents can be detected to a certain extent by arranging the detection mechanism, the detection precision can be greatly improved by adjusting the detection mechanism, the microporous materials and the reagents in the reaction kettle can be fully stirred by arranging the stirring mechanism, the detection efficiency and the detection precision are improved, the reagent structure is arranged, the microporous materials can be degraded, and the reagents and the microporous materials can be fully mixed when being stirred by arranging the reagent pipeline and perforation, so that the effect of complete mixing is achieved.
On the basis of the technical scheme, the degradable microporous material degradation performance detection device can be improved as follows:
the stirring mechanism comprises a motor, a stirring shaft and stirring blades, wherein the motor is fixedly connected to the top end of the reaction kettle, the stirring shaft is fixedly connected to an output shaft of the motor, a placing groove is formed in the stirring shaft, the reagent tube is arranged in the placing groove, the stirring blades are fixedly connected to the bottom end of the stirring shaft, and a plurality of perforations are formed in the stirring blades and used for fully mixing reagents with microporous materials.
The beneficial effects of adopting above-mentioned improvement scheme are: through the output shaft and the (mixing) shaft fixed connection that set up the motor, can drive the (mixing) shaft, can realize the rotation of stirring leaf through setting up the (mixing) shaft to stir the micropore material in the reation kettle, this structure has easy operation, effect that facilitates the use.
Further, the detection mechanism comprises a temperature controller and a temperature sensing plate, wherein the temperature controller is fixedly connected to the upper surface of the reaction kettle, and the temperature sensing plate is fixedly connected to the bottom of the temperature controller.
The beneficial effects of adopting above-mentioned improvement scheme are: the temperature in the reaction kettle can be detected by arranging the temperature controller and the temperature sensing plate, and the temperature in the reaction kettle can be adjusted.
Further, the detection mechanism further comprises an acidity detection electrode and a data recorder, wherein the data recorder is fixedly connected to the upper surface of the reaction kettle, and the bottom of the data recorder is fixedly connected with the acidity detection electrode.
The beneficial effects of adopting above-mentioned improvement scheme are: the acidity in the reaction kettle can be detected by arranging the acidity detection electrode and the data recorder.
Further, the temperature sensing plate is electrically connected with the temperature controller, and the temperature sensing plate and the temperature controller are used for detecting and adjusting the temperature in the reaction kettle.
The beneficial effects of adopting above-mentioned improvement scheme are: through setting up the electric connection of temperature controller and temperature sensing board, can realize using its temperature sensing board of temperature controller control, have the effect of simplified operation.
Further, the acidity detection electrode is electrically connected with the data recorder, and the acidity detection electrode and the data recorder are used for detecting acidity in the reaction kettle.
The beneficial effects of adopting above-mentioned improvement scheme are: the acidity detection electrode is electrically connected with the data recorder, so that data detected by the acidity detection electrode can be fed back to the data recorder, and the effect of convenient observation is achieved.
Further, a feed inlet is formed in the outer side wall of the reaction kettle, and a sealing cover is arranged on the feed inlet.
The beneficial effects of adopting above-mentioned improvement scheme are: through setting up sealed lid, can carry out the protection of certain degree to the environment in the reation kettle, make its internal environment keep unchanged, improved the reliability of detection data.
Further, a discharge port is arranged at the bottom of the reaction kettle and used for discharging mixed materials in the reaction kettle.
Further, the acidity detection electrode is a glass pH electrode.
The beneficial effects of adopting above-mentioned improvement scheme are: the method has high sensitivity and accuracy, so as to realize the real-time monitoring of the acid-base reaction.
Further, the stirring blade is arc-shaped.
The beneficial effects of adopting above-mentioned improvement scheme are: through setting up stirring leaf shape, make its shape of laminating reation kettle more, the stirring is more even.
Compared with the prior art, the degradable microporous material degradation performance detection device provided by the utility model has the beneficial effects that: the reaction kettle can provide enough space for the reaction of microporous materials and reagents, the reaction kettle has the effect of providing reaction efficiency, the microporous materials reacting with the reagents can be detected to a certain extent by arranging the detection mechanism, the detection precision can be greatly improved by adjusting the detection mechanism, the microporous materials and the reagents in the reaction kettle can be fully stirred by arranging the stirring mechanism, the detection efficiency and the detection precision are improved, the reagent structure is arranged, the microporous materials can be degraded, and the reagents and the microporous materials can be fully mixed when being stirred by arranging the reagent pipeline and perforation, so that the effect of complete mixing is achieved.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present utility model, the drawings that are needed in the description of the embodiments of the present utility model will be briefly described below, it being obvious that the drawings in the following description are only some embodiments of the present utility model, and that other drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a schematic structural diagram of a degradable microporous material degradation performance detection device;
FIG. 2 is a schematic diagram of the structure of a degradable microporous material degradation performance detection device in front view;
FIG. 3 is a schematic diagram of the structure of a front section of a degradable microporous material degradation performance detecting device;
FIG. 4 is a schematic diagram of a device for detecting degradation of a degradable microporous material;
in the drawings, the list of components represented by the various numbers is as follows:
1. a reaction kettle; 11. a feed inlet; 12. a discharge port; 2. a detection mechanism; 21. an acidity detection electrode; 22. a temperature controller; 23. a temperature sensing plate; 24. a data recorder; 3. a stirring mechanism; 31. a motor; 32. a stirring shaft; 33. stirring the leaves; 4. a reagent structure; 41. a reagent conduit; 42. perforating; 43. a reagent tube.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the embodiments of the present utility model more apparent, the technical solutions of the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model, and it is apparent that the described embodiments are some embodiments of the present utility model, but not all embodiments. All other embodiments, based on the embodiments of the utility model, which are apparent to those of ordinary skill in the art without inventive faculty, are intended to be within the scope of the utility model.
Thus, the following detailed description of the embodiments of the utility model, as presented in the figures, is not intended to limit the scope of the utility model, as claimed, but is merely representative of selected embodiments of the utility model. All other embodiments, based on the embodiments of the utility model, which are apparent to those of ordinary skill in the art without inventive faculty, are intended to be within the scope of the utility model.
It should be noted that: like reference numerals and letters denote like items in the following figures, and thus once an item is defined in one figure, no further definition or explanation thereof is necessary in the following figures.
In the description of the present utility model, it should be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", etc. indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings are merely for convenience in describing the present utility model and simplifying the description, and do not indicate or imply that the apparatus or elements referred to must have a specific orientation, be configured and operated in a specific orientation, and thus should not be construed as limiting the present utility model.
As shown in fig. 1-4, the degradable microporous material degradation performance detection device provided by the utility model comprises a reaction kettle 1, a detection mechanism 2, a stirring mechanism 3 and a reagent structure 4, wherein the detection mechanism 2 penetrates through the reaction kettle 1 and is arranged in the reaction kettle 1, the detection mechanism 2 is used for detecting microporous materials in the reaction kettle 1, the stirring mechanism 3 is arranged in the reaction kettle 1, the stirring mechanism 3 is used for stirring the microporous materials in the reaction kettle 1, the stirring mechanism 3 is provided with the reagent structure 4, the reagent structure 4 comprises a reagent pipeline 41, a perforation 42 and a reagent pipe 43, the reagent pipeline 41 is arranged in the stirring mechanism 3, one end of the reagent pipeline 41 is connected to the perforation 42, and the reagent structure 4 is used for guiding reagents into the reaction kettle 1.
When the device is used, firstly, the reagent tube 43 is placed in a placing groove formed in the stirring shaft 32, the reagent tube 43 is communicated with the reagent pipeline 41, the reagent flows out through the perforation 42, then the material is poured into the reaction kettle 1 through the feed inlet 11, then the motor 31 is started to fully stir the material and the reagent in the reaction kettle 1, then the acidity in the reaction kettle 1 is obtained through the observation data recorder 24, meanwhile, the temperature in the reaction kettle 1 can be controlled through the temperature controller 22, and finally, after the detection is finished, the motor 31 is stopped, and the material is poured out through the discharge outlet 12.
Wherein, in above-mentioned technical scheme, rabbling mechanism 3 includes motor 31, (mixing) shaft 32 and stirring leaf 33, and motor 31 fixed connection is on the top of reation kettle 1, and fixedly connected with (mixing) shaft 32 is gone up to motor 31's output shaft, has seted up the standing groove on the (mixing) shaft 32, is provided with reagent pipe 43 in the standing groove, and the bottom fixedly connected with stirring leaf 33 of (mixing) shaft 32, has seted up a plurality of perforation 42 on the stirring leaf 33 for with reagent and micropore material intensive mixing.
When the motor 31 is started, the stirring shaft 32 fixedly connected with the output shaft is driven to rotate, so that the stirring blade 33 is driven to rotate, and the reagent in the stirring blade 33 flows out through the perforation 42 and is uniformly mixed with the material in the reaction kettle 1.
Further, in the above technical scheme, the detection mechanism 2 includes a temperature controller 22 and a temperature sensing plate 23, the temperature controller 22 is fixedly connected to the upper surface of the reaction kettle 1, and the temperature sensing plate 23 is fixedly connected to the bottom of the temperature controller 22.
Further, in the above technical scheme, the detecting mechanism 2 further includes an acidity detecting electrode 21 and a data recorder 24, the data recorder 24 is fixedly connected to the upper surface of the reaction kettle 1, and the acidity detecting electrode 21 is fixedly connected to the bottom of the data recorder 24.
Further, in the above technical solution, the temperature sensing plate 23 is electrically connected with the temperature controller 22, and the temperature sensing plate 23 and the temperature controller 22 are used for detecting and adjusting the temperature in the reaction kettle 1.
Further, in the above technical solution, the acidity detecting electrode 21 is electrically connected to the data recorder 24, and the acidity detecting electrode 21 and the data recorder 24 are used for detecting acidity in the reaction kettle 1.
Further, in the above technical scheme, a feed inlet 11 is formed in the outer side wall of the reaction kettle 1, and a sealing cover is arranged on the feed inlet 11.
Further, in the above technical scheme, the bottom of the reaction kettle 1 is provided with a discharge port 12, and the discharge port 12 is used for discharging mixed materials in the reaction kettle 1.
Further, in the above-described embodiment, the acidity detection electrode 21 is a glass pH electrode.
Further, in the above-described embodiments, the stirring vane 33 is arc-shaped.
Specifically, the method comprises the following specific operation steps: when the device is used, firstly, the reagent tube 43 is placed in a placing groove formed in the stirring shaft 32, the reagent tube 43 is communicated with the reagent pipeline 41, the reagent flows out through the perforation 42, then the material is poured into the reaction kettle 1 through the feed inlet 11, then the motor 31 is started to fully stir the material and the reagent in the reaction kettle 1, then the acidity in the reaction kettle 1 is obtained through the observation data recorder 24, meanwhile, the temperature in the reaction kettle 1 can be controlled through the temperature controller 22, and finally, after the detection is finished, the motor 31 is stopped, and the material is poured out through the discharge outlet 12.
The foregoing is merely illustrative of the present utility model, and the present utility model is not limited thereto, and any person skilled in the art will readily recognize that variations or substitutions are within the scope of the present utility model. Therefore, the protection scope of the utility model is subject to the protection scope of the claims.
Claims (10)
1. The utility model provides a degradable microporous material degradation performance detection device, includes reation kettle (1), detection mechanism (2), rabbling mechanism (3) and reagent structure (4), detection mechanism (2) pass reation kettle (1), set up in the inside of reation kettle (1), detection mechanism (2) are used for detecting microporous material in reation kettle (1), rabbling mechanism (3) set up in inside reation kettle (1), rabbling mechanism (3) are used for the stirring microporous material in reation kettle (1), be provided with in rabbling mechanism (3) reagent structure (4), a serial communication port, reagent structure (4) include reagent pipeline (41), perforation (42) and reagent pipe (43), reagent pipeline (41) are seted up in rabbling mechanism (3), reagent pipeline (41) one end is connected on perforation (42), reagent structure (4) are used for leading-in reagent in reation kettle (1).
2. The degradable microporous material degradation performance detection device according to claim 1, wherein the stirring mechanism (3) comprises a motor (31), a stirring shaft (32) and stirring blades (33), the motor (31) is fixedly connected to the top end of the reaction kettle (1), the stirring shaft (32) is fixedly connected to an output shaft of the motor (31), a placing groove is formed in the stirring shaft (32), the reagent tube (43) is arranged in the placing groove, the stirring blades (33) are fixedly connected to the bottom end of the stirring shaft (32), and a plurality of perforations (42) are formed in the stirring blades (33) and used for fully mixing reagents with microporous materials.
3. The degradable microporous material degradation performance detection device according to claim 2, wherein the detection mechanism (2) comprises a temperature controller (22) and a temperature sensing plate (23), the temperature controller (22) is fixedly connected to the upper surface of the reaction kettle (1), and the temperature sensing plate (23) is fixedly connected to the bottom of the temperature controller (22).
4. A degradable microporous material degradation property detection device according to claim 3, wherein the detection mechanism (2) further comprises an acidity detection electrode (21) and a data recorder (24), the data recorder (24) is fixedly connected to the upper surface of the reaction kettle (1), and the acidity detection electrode (21) is fixedly connected to the bottom of the data recorder (24).
5. The degradable microporous material degradation performance detection apparatus according to claim 4, wherein the temperature sensing plate (23) is electrically connected to the temperature controller (22), and the temperature sensing plate (23) and the temperature controller (22) are used for detecting and adjusting the temperature in the reaction kettle (1).
6. The degradable microporous material degradation performance testing apparatus according to claim 5, wherein the acidity testing electrode (21) is electrically connected with the data recorder (24), and the acidity testing electrode (21) and the data recorder (24) are used for testing acidity in the reaction kettle (1).
7. The degradable microporous material degradation performance detection device according to claim 6, wherein a feed inlet (11) is formed in the outer side wall of the reaction kettle (1), and a sealing cover is arranged on the feed inlet (11).
8. The degradable microporous material degradation performance detection device according to claim 7, wherein a discharge port (12) is arranged at the bottom of the reaction kettle (1), and the discharge port (12) is used for removing mixed materials in the reaction kettle (1).
9. The degradation performance detection apparatus for a degradable microporous material according to claim 8, wherein the acidity detection electrode (21) is a glass pH electrode.
10. The degradable microporous material degradation performance testing apparatus according to claim 9, wherein the stirring blade (33) is arc-shaped.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321634972.7U CN220357022U (en) | 2023-06-27 | 2023-06-27 | Degradable microporous material degradation performance detection device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321634972.7U CN220357022U (en) | 2023-06-27 | 2023-06-27 | Degradable microporous material degradation performance detection device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220357022U true CN220357022U (en) | 2024-01-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321634972.7U Active CN220357022U (en) | 2023-06-27 | 2023-06-27 | Degradable microporous material degradation performance detection device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220357022U (en) |
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2023
- 2023-06-27 CN CN202321634972.7U patent/CN220357022U/en active Active
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