CN220238563U - Iron oxide red production facility - Google Patents

Iron oxide red production facility Download PDF

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Publication number
CN220238563U
CN220238563U CN202321657394.9U CN202321657394U CN220238563U CN 220238563 U CN220238563 U CN 220238563U CN 202321657394 U CN202321657394 U CN 202321657394U CN 220238563 U CN220238563 U CN 220238563U
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CN
China
Prior art keywords
stirring
iron oxide
oxide red
tank body
bearing
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CN202321657394.9U
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Chinese (zh)
Inventor
刘涛
卢绪恒
程龙
廖文举
高中国
李政
厉金镑
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Shandong Chunguang Technology Group Co ltd
Shandong Chunguang Magnetoelectric Technology Co ltd
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Shandong Chunguang Technology Group Co ltd
Shandong Chunguang Magnetoelectric Technology Co ltd
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Abstract

The utility model provides iron oxide red production equipment which comprises a mounting frame, a tank body, a stirring mechanism, a heating mechanism and a controller, wherein the stirring mechanism comprises a stirring motor, a stirring piece and a connecting frame; the utility model discloses iron oxide red production equipment, which belongs to the technical field of chemical reaction devices and can fully mix ammonium bicarbonate dry powder with ferrous sulfate solution to prepare iron oxide red.

Description

Iron oxide red production facility
Technical Field
The utility model relates to iron oxide red production equipment, and belongs to the technical field of chemical reaction devices.
Background
The iron oxide red is one of the raw materials of the manganese zinc ferrite particles, has good heat resistance, does not change color at 500 ℃, does not change chemical structure at 1200 ℃ and is extremely stable; can absorb ultraviolet light in sunlight, so the coating is protected; the paint is resistant to dilute acid, alkali, water and solvent, so that the paint has good weather resistance. A large amount of ferrous sulfate (2.5-4 t of ferrous sulfate is produced in the production process of titanium dioxide in China) is produced, the value of the ferrous sulfate is not high, and most of the ferrous sulfate is not fully utilized except a small amount of the ferrous sulfate which is used for water purifying agents, fertilizers, feed additives and the like, so that the environment is polluted and the resources of Baobao are wasted.
The device for preparing iron oxide red synthesis by using iron oxide red crystal seeds in the prior art CN113896246A discloses that a driving motor drives two transmission mechanisms to rotate through a connecting mechanism, the two transmission mechanisms simultaneously drive two stirring shafts to rotate from two ends, and then a stirring rod is driven to stir and process processing liquid in a synthesis box body fully, the two ends of the stirring shaft are in stress states, the stress inside the stirring shaft can be reduced, the stress on the stirring shaft is uniform, the situation that one end of the stirring shaft is not damaged due to the stress can not occur, the stress is uniform, the situation that the stirring shaft cannot be damaged can not occur, when the driving motor drives the two transmission mechanisms to rotate through the connecting mechanism, a rotating shaft drives a worm on the rotating shaft to rotate, the worm drives a worm wheel to rotate, the worm wheel drives the rotating rod to rotate, the rotating rod drives two driving bevel gears to rotate, and the two driving bevel gears drive corresponding driven bevel gears to rotate, so that the stirring rod is driven to rotate. Only the process of promoting the synthesis reaction by mechanical stirring is disclosed, the efficiency is low, and a simple stirring mechanism in the equipment cannot be suitable for the process of preparing the iron oxide red from the ferrous sulfate.
Disclosure of Invention
The utility model aims to provide iron oxide red production equipment which can fully mix ammonium bicarbonate dry powder with ferrous sulfate solution to prepare iron oxide red.
The technical scheme for solving the technical problems is as follows: an iron oxide red production facility comprising: the device comprises a mounting frame, a tank body, a stirring mechanism, a heating mechanism and a controller, wherein the tank body is mounted on the mounting frame, a charging port and an exhaust port are formed in the top of the tank body, and a discharging port is formed in the bottom of the tank body; the stirring mechanism comprises a stirring motor, a stirring piece and a connecting frame, wherein the connecting frame is fixed on the mounting frame and positioned above the tank body, the stirring motor is fixed on the connecting frame, a through hole is formed in the top of the tank body, the stirring piece is rotationally connected to the through hole, the stirring end of the stirring piece is positioned in the tank body, and the driving end of the stirring piece is in transmission connection with the stirring motor through a transmission assembly; the heating mechanism comprises a steam generator, an annular pipe and a conveying pipe, wherein the annular pipe is fixed on the inner wall of the tank body, the annular pipe is provided with an air inlet and a plurality of air outlets, the tank body is provided with a perforation, one end of the conveying pipe passes through the perforation in a sealing manner and is communicated with an output port of the steam generator, the other end of the conveying pipe is communicated with the air inlet, and the air outlets can be immersed into mixed materials in the tank body; the controller is electrically connected with the stirring motor and the steam generator respectively.
The beneficial effects of the utility model are as follows: adding ammonium bicarbonate dry powder and ferrous sulfate solution into the tank body from a charging port, and driving a stirring piece by a stirring motor to mix the ammonium bicarbonate dry powder and the ferrous sulfate solution so as to promote chemical reaction to form ferrous carbonate suspension; the steam generator conveys high-temperature steam into the annular pipe through the conveying pipe, a plurality of air outlets on the annular pipe are immersed into mixed liquid of ammonium bicarbonate dry powder and ferrous sulfate solution, the high-temperature steam sprayed from the air outlets increases the temperature of the mixed liquid, the solubility of ferrous sulfate is increased, the reaction speed is further increased, the sprayed high-temperature steam can stir the mixed liquid to be uniformly mixed, the reaction speed is further increased to obtain ferrous carbonate suspension, and the ferrous carbonate suspension is rapidly oxidized into ferrous hydroxide; high-temperature steam is discharged out of the tank body from the exhaust port after being discharged out of the mixed liquid; and opening a discharge opening after the reaction is finished, discharging ferrous hydroxide, and drying to obtain iron oxide red, wherein the ferrous hydroxide is easily oxidized by air.
On the basis of the technical scheme, the utility model can be improved as follows.
Further, the heating mechanism further comprises a plurality of branch pipes and a plurality of steam spray heads, one ends of the branch pipes are correspondingly communicated with the air outlets, the other ends of the branch pipes are correspondingly communicated with the steam spray heads, and the steam spray heads can be immersed into the mixed materials.
The beneficial effect of adopting the further scheme is that: high-temperature steam is sprayed out from a plurality of steam spray nozzles through a plurality of branch pipes, a plurality of spray holes are formed in the steam spray nozzles, the steam spray nozzles are immersed in the mixed materials, the contact area between the steam sprayed out of the spray holes and the mixed materials can be increased, the heating speed is high, and the reaction rate is improved.
Further, the heating mechanism further comprises a steam heating pipe spirally wound on the tank body, the input end of the steam heating pipe is communicated with the output port of the steam generator, and the output end of the steam heating pipe is communicated with the water tank.
The beneficial effect of adopting the further scheme is that: the steam heating pipe spiral winding can heat the jar body on the outer wall of jar body, improves the internal rate of heating up of jar to can keep warm the jar body, the input is located the output top, can make high temperature steam stay longer time in the steam heating pipe, fully carries out heat transfer.
Further, the stirring piece comprises a plurality of stirring blades and a stirring shaft, the stirring shaft penetrates through the through hole in a sealing mode and is connected to the through hole in a rotating mode, the upper end of the stirring shaft is connected with the stirring motor in a transmission mode through the transmission assembly, and the stirring blades are fixed on the shaft body of the stirring shaft.
Further, the stirring blades are divided into two layers along the axial direction of the stirring shaft, and the two stirring blades corresponding to the two layers are vertically arranged.
The beneficial effect of adopting the further scheme is that: the stirring motor drives the stirring shaft to rotate through the transmission assembly, and the stirring shaft drives the stirring blade to rotate so as to mix materials and enable the materials to fully react; the stirring blades corresponding to the two layers are vertically arranged, so that the stirring effect can be improved.
Further, the inclination angle of the plurality of stirring blades is 40-50 degrees.
The beneficial effect of adopting the further scheme is that: when the stirring blade runs, the mixed materials are pushed to the bottom of the tank, so that the mixing effect is improved, and the reaction speed is improved.
Further, the transmission assembly comprises a speed reducer, a first coupler, a second coupler and a first bearing, the speed reducer is mounted on the connecting frame, the stirring motor is in transmission connection with the speed reducer through the first coupler, the speed reducer is in transmission connection with the stirring shaft through the second coupler, the outer ring of the first bearing is fixedly connected with the inner wall of the through hole, and the inner ring of the first bearing is fixedly connected with the stirring shaft.
Further, the speed reducer is a worm gear speed reducer.
Further, the stirring device also comprises a plurality of flow baffle plates, wherein a plurality of flow baffle plates are fixed on the inner wall of the tank body at equal intervals, and the plate surfaces of the flow baffle plates are perpendicular to the tangential direction of the rotating surface of the stirring blade.
The beneficial effect of adopting the further scheme is that: the stirring blade stirs the mixed material, and the baffle plate can block in its flow direction, makes its part form the torrent, improves the mixing effect, improves reaction rate.
Further, the stirring device also comprises a bearing seat and a second bearing, wherein the bearing seat is fixed at the bottom of the tank body, the outer ring of the second bearing is fixed on the bearing seat, and the bottom end of the stirring shaft is fixedly connected with the inner ring of the second bearing.
The beneficial effect of adopting the further scheme is that: the rotation stability of the stirring shaft is improved.
Drawings
FIG. 1 is a front view of an iron oxide red production facility provided by the present utility model;
FIG. 2 is a longitudinal sectional view of an iron oxide red production facility provided by the utility model;
fig. 3 is a left side view of an iron oxide red production apparatus provided by the present utility model.
In the drawings, the list of components represented by the various numbers is as follows:
1-tank, 11-charging port, 12-exhaust port, 13-discharge port, 14-support, 2-stirring mechanism, 21-stirring motor, 22-stirring piece, 221-stirring blade, 222-stirring shaft, 23-connecting frame, 3-heating mechanism, 31-annular pipe, 32-conveying pipe, 33-branch pipe, 34-steam nozzle, 35-steam heating pipe, 351-input end, 352-output end, 4-transmission component, 41-speed reducer, 5-baffle plate and 6-bearing seat.
Detailed Description
The principles and features of the present utility model are described below with reference to the drawings, the examples are illustrated for the purpose of illustrating the utility model and are not to be construed as limiting the scope of the utility model.
The utility model aims to provide iron oxide red production equipment which solves the problems existing in the prior art and can fully mix ammonium bicarbonate dry powder with ferrous sulfate solution to prepare iron oxide red.
In order that the above-recited objects, features and advantages of the present utility model will become more readily apparent, a more particular description of the utility model will be rendered by reference to the appended drawings and appended detailed description.
The utility model provides iron oxide red production equipment, as shown in figures 1-3, comprising: the device comprises a mounting frame, a tank body 1, a stirring mechanism 2, a heating mechanism 3 and a controller, wherein the tank body 1 is mounted on the mounting frame, a charging port 11 and an exhaust port 12 are formed in the top of the tank body, and a discharging port 13 is formed in the bottom of the tank body; the stirring mechanism 2 comprises a stirring motor 21, a stirring piece 22 and a connecting frame 23, the connecting frame 23 is fixed on the mounting frame and is positioned above the tank body 1, the stirring motor 21 is fixed on the connecting frame 23, a through hole is formed in the top of the tank body 1, the stirring piece 22 is rotationally connected to the through hole, a stirring end of the stirring piece is positioned in the tank body 1, and a driving end of the stirring piece is in transmission connection with the stirring motor 21 through a transmission component 4; the heating mechanism 3 comprises a steam generator, an annular pipe 31 and a conveying pipe 32, wherein the annular pipe 31 is fixed on the inner wall of the tank body 1, the annular pipe 31 is provided with an air inlet and a plurality of air outlets, the tank body 1 is provided with a perforation, one end of the conveying pipe 32 passes through the perforation in a sealing manner and is communicated with an output port of the steam generator, the other end of the conveying pipe is communicated with the air inlet, and the plurality of air outlets can be immersed into mixed materials in the tank body 1; the controller is electrically connected to the agitator motor 21 and the steam generator, respectively.
The utility model provides iron oxide red production equipment, which is characterized in that ammonium bicarbonate dry powder and ferrous sulfate solution are added into a tank body 1 from a feed inlet 11, a stirring motor 21 drives a stirring piece 22 to mix the ammonium bicarbonate dry powder and the ferrous sulfate solution, and chemical reaction is promoted to generate ferrous carbonate suspension; the steam generator conveys high-temperature steam into the annular pipe 31 through the conveying pipe 32, a plurality of air outlets on the annular pipe 31 are immersed into mixed liquid of ammonium bicarbonate dry powder and ferrous sulfate solution, the high-temperature steam sprayed from the air outlets increases the temperature of the mixed liquid, the solubility of ferrous sulfate is increased, the reaction speed is further increased, the sprayed high-temperature steam can stir the mixed liquid to be uniformly mixed, the reaction speed is further increased to obtain ferrous carbonate suspension, and the ferrous carbonate suspension is rapidly oxidized into ferrous hydroxide; the high-temperature steam is discharged out of the tank body 1 from the exhaust port 12 after being discharged from the mixed liquid; after the reaction is finished, a discharge opening 13 is opened, the ferrous hydroxide is discharged, and after drying, the ferrous hydroxide is easily oxidized by air, so that iron oxide red is obtained.
Preferably, the stirring motor 21 is a three-phase variable frequency asynchronous motor.
Preferably, the material of the can 1 is SUS304 stainless steel.
Preferably, thermal insulation rock wool is laid on the outer side wall of the tank body 1.
Preferably, a plurality of supports 14 are fixed to the outer side wall of the tank 1, and the plurality of supports 14 are fixed to the mounting frame.
In an embodiment of the present utility model, the heating mechanism 3 further includes a plurality of branch pipes 33 and a plurality of steam spray nozzles 34, wherein one ends of the plurality of branch pipes 33 are correspondingly communicated with the plurality of air outlets, and the other ends of the plurality of branch pipes are correspondingly communicated with the plurality of steam spray nozzles 34, and the plurality of steam spray nozzles 34 can be immersed in the mixture.
High-temperature steam is sprayed out of the steam spray nozzles 34 through the branch pipes 33, a plurality of spray holes are formed in the steam spray nozzles 34, the steam spray nozzles 34 are immersed in the mixed material, the contact area between the steam sprayed out of the spray holes and the mixed material can be increased, the heating speed is high, and the reaction rate is improved.
In an embodiment of the present utility model, the heating mechanism 3 further includes a steam heating pipe 35 spirally wound on the tank 1, an input end 351 of the steam heating pipe 35 is communicated with an output port of the steam generator, and an output end 352 is communicated with the water tank.
The steam heating pipe 35 spiral winding can heat the jar body 1 on the outer wall of jar body 1, improves the internal rate of heating up of jar body 1 to can keep warm jar body 1, input 351 is located the output 352 top, can make high temperature steam stay longer in steam heating pipe 35, fully carries out heat transfer.
Preferably, the output end 352 is provided with a drain valve which is communicated with the water tank, the waste heat is utilized to increase the temperature of water in the water tank, and warm water can be used for cleaning equipment.
In a specific embodiment of the present utility model, the stirring member 22 includes a plurality of stirring blades 221 and a stirring shaft 222, the stirring shaft 222 passes through the through hole in a sealing manner and is rotatably connected to the through hole, the upper end of the stirring shaft 222 is in transmission connection with the stirring motor 21 through the transmission assembly 4, and the plurality of stirring blades 221 are fixed on the shaft body of the stirring shaft 222.
In one embodiment of the present utility model, the plurality of stirring blades 221 are divided into two layers along the axial direction of the stirring shaft 222, and the two corresponding stirring blades 221 of the two layers are vertically arranged.
The stirring motor 21 drives the stirring shaft 222 to rotate through the transmission assembly 4, and the stirring shaft 222 drives the stirring blade 221 to rotate so as to mix materials and enable the materials to fully react; the stirring effect can be improved by arranging the stirring blades 221 corresponding to the two layers vertically.
In one embodiment of the present utility model, the plurality of stirring blades 221 have an inclination angle of 40 ° to 50 °.
When the stirring blade 221 operates, the mixed material is pushed to the bottom of the tank, so that the mixing effect is improved, and the reaction speed is improved.
Preferably, the inclination angle of the stirring vane 221 is 45 °.
In a specific embodiment of the present utility model, the transmission assembly 4 includes a speed reducer 41, a first coupling, a second coupling and a first bearing, the speed reducer 41 is installed on the connecting frame 23, the stirring motor 21 is in transmission connection with the speed reducer 41 through the first coupling, the speed reducer 41 is in transmission connection with the stirring shaft 222 through the second coupling, an outer ring of the first bearing is fixedly connected with an inner wall of the through hole, and an inner ring of the first bearing is fixedly connected with the stirring shaft 222.
Preferably, the first coupling and the second coupling are disposed at the outer portion of the can 1, thereby preventing the first coupling and the second coupling from being corroded.
In an embodiment of the present utility model, the speed reducer 41 is a worm gear speed reducer 41.
In an embodiment of the present utility model, the stirring tank further includes a plurality of flow blocking plates 5, wherein the flow blocking plates 5 are fixed on the inner wall of the tank 1 at equal intervals, and the plate surface of the flow blocking plates is perpendicular to the tangential direction of the rotating surface of the stirring blade 221.
The stirring blades 221 stir the mixed materials, and the baffle plates can block the flowing direction of the mixed materials, so that turbulence is formed locally, the mixing effect is improved, and the reaction speed is improved.
In a specific embodiment of the present utility model, the stirring device further comprises a bearing seat 6 and a second bearing, the bearing seat 6 is fixed at the bottom of the tank body 1, the outer ring of the second bearing is fixed on the bearing seat 6, and the bottom end of the stirring shaft 222 is fixedly connected with the inner ring of the second bearing.
The stability of rotation of the stirring shaft 222 is improved.
Preferably, the bearing seat 6 is made of nylon.
The foregoing description of the preferred embodiments of the utility model is not intended to limit the utility model to the precise form disclosed, and any such modifications, equivalents, and alternatives falling within the spirit and scope of the utility model are intended to be included within the scope of the utility model.

Claims (10)

1. An iron oxide red production facility, characterized by comprising:
a mounting frame;
the tank body (1), the tank body (1) is installed on the installation frame, the top is provided with a charging port (11) and an exhaust port (12), and the bottom is provided with a discharge port (13);
the stirring mechanism (2), the stirring mechanism (2) comprises a stirring motor (21), a stirring piece (22) and a connecting frame (23), the connecting frame (23) is fixed on the mounting frame and positioned above the tank body (1), the stirring motor (21) is fixed on the connecting frame (23), a through hole is formed in the top of the tank body (1), the stirring piece (22) is rotationally connected to the through hole, the stirring end of the stirring piece is positioned in the tank body (1), and the driving end of the stirring piece is in transmission connection with the stirring motor (21) through a transmission assembly (4);
the heating mechanism (3), the heating mechanism (3) comprises a steam generator, an annular pipe (31) and a conveying pipe (32), the annular pipe (31) is fixed on the inner wall of the tank body (1), the annular pipe (31) is provided with an air inlet and a plurality of air outlets, the tank body (1) is provided with a perforation, the conveying pipe (32) passes through the perforation in a sealing way, one end of the conveying pipe is communicated with an output port of the steam generator, the other end of the conveying pipe is communicated with the air inlet, and the air outlets can be immersed into mixed materials in the tank body (1);
and the controller is electrically connected with the stirring motor (21) and the steam generator respectively.
2. An iron oxide red production apparatus according to claim 1, wherein the heating mechanism (3) further comprises a plurality of branch pipes (33) and a plurality of steam spray heads (34), one ends of the plurality of branch pipes (33) are correspondingly communicated with the plurality of air outlets, the other ends thereof are correspondingly communicated with the plurality of steam spray heads (34), and the plurality of steam spray heads (34) can be immersed in the mixture.
3. An iron oxide red production apparatus as claimed in claim 2, wherein the heating means (3) further comprises a steam heating pipe (35) spirally wound around the tank (1), the input end (351) of the steam heating pipe (35) being in communication with the output of the steam generator, and the output end (352) being in communication with a pool of water.
4. The iron oxide red production equipment according to claim 1, wherein the stirring piece (22) comprises a plurality of stirring blades (221) and a stirring shaft (222), the stirring shaft (222) passes through the through hole in a sealing manner and is rotationally connected with the through hole, the upper end of the stirring shaft (222) is in transmission connection with the stirring motor (21) through the transmission assembly (4), and the stirring blades (221) are fixed on the shaft body of the stirring shaft (222).
5. An iron oxide red production apparatus according to claim 4, wherein a plurality of said stirring blades (221) are divided into two layers in an axial direction of said stirring shaft (222), and two corresponding stirring blades (221) of the two layers are vertically arranged.
6. An iron oxide red production apparatus according to claim 4, wherein the plurality of stirring blades (221) are inclined at an angle of 40 ° to 50 °.
7. The iron oxide red production equipment according to claim 4, wherein the transmission assembly (4) comprises a speed reducer (41), a first coupler, a second coupler and a first bearing, the speed reducer (41) is installed on the connecting frame (23), the stirring motor (21) is in transmission connection with the speed reducer (41) through the first coupler, the speed reducer (41) is in transmission connection with the stirring shaft (222) through the second coupler, the outer ring of the first bearing is fixedly connected with the inner wall of the through hole, and the inner ring of the first bearing is fixedly connected with the stirring shaft (222).
8. An iron oxide red production facility according to claim 7, characterized in that the speed reducer (41) is a worm gear speed reducer.
9. The iron oxide red production equipment according to claim 4, further comprising a plurality of flow baffle plates (5), wherein the flow baffle plates (5) are fixed on the inner wall of the tank body (1) at equal intervals, and the plate surfaces of the flow baffle plates are perpendicular to the tangential direction of the rotating surface of the stirring blade (221).
10. The iron oxide red production equipment according to claim 4, further comprising a bearing seat (6) and a second bearing, wherein the bearing seat (6) is fixed at the bottom of the tank body (1), an outer ring of the second bearing is fixed on the bearing seat (6), and the bottom end of the stirring shaft (222) is fixedly connected with an inner ring of the second bearing.
CN202321657394.9U 2023-06-28 2023-06-28 Iron oxide red production facility Active CN220238563U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202321657394.9U CN220238563U (en) 2023-06-28 2023-06-28 Iron oxide red production facility

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202321657394.9U CN220238563U (en) 2023-06-28 2023-06-28 Iron oxide red production facility

Publications (1)

Publication Number Publication Date
CN220238563U true CN220238563U (en) 2023-12-26

Family

ID=89234984

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202321657394.9U Active CN220238563U (en) 2023-06-28 2023-06-28 Iron oxide red production facility

Country Status (1)

Country Link
CN (1) CN220238563U (en)

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