CN220194801U - Amidine reaction kettle for preparing diazinon - Google Patents
Amidine reaction kettle for preparing diazinon Download PDFInfo
- Publication number
- CN220194801U CN220194801U CN202223316940.0U CN202223316940U CN220194801U CN 220194801 U CN220194801 U CN 220194801U CN 202223316940 U CN202223316940 U CN 202223316940U CN 220194801 U CN220194801 U CN 220194801U
- Authority
- CN
- China
- Prior art keywords
- fixedly connected
- rotating
- kettle
- uniformly
- kettle body
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 27
- FHIVAFMUCKRCQO-UHFFFAOYSA-N diazinon Chemical compound CCOP(=S)(OCC)OC1=CC(C)=NC(C(C)C)=N1 FHIVAFMUCKRCQO-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 150000001409 amidines Chemical class 0.000 title claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 20
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract description 40
- 229910021529 ammonia Inorganic materials 0.000 abstract description 19
- 238000003756 stirring Methods 0.000 description 6
- 230000002349 favourable effect Effects 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- CEIPQQODRKXDSB-UHFFFAOYSA-N ethyl 3-(6-hydroxynaphthalen-2-yl)-1H-indazole-5-carboximidate dihydrochloride Chemical compound Cl.Cl.C1=C(O)C=CC2=CC(C3=NNC4=CC=C(C=C43)C(=N)OCC)=CC=C21 CEIPQQODRKXDSB-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000006358 imidation reaction Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses an amidine reaction kettle for preparing diazinon, which comprises a kettle body, wherein the top of the kettle body is detachably connected with a kettle cover, the bottom of the kettle body is uniformly and fixedly connected with supporting legs, the top of the kettle cover is fixedly connected with a supporting frame, the top of the supporting frame is fixedly connected with a motor, an output shaft of the motor is fixedly connected with a rotating shaft, the other end of the rotating shaft extends to the bottom of the kettle body, and the circumferential side surface of the rotating shaft is uniformly and fixedly connected with ten rotating plates. According to the utility model, the device is vertically placed on a horizontal working surface through the arranged annular pipe, the kettle cover is opened, liquid is placed in the kettle body, the kettle cover is closed, the ammonia pipe is connected to the sleeve, ammonia is introduced into the annular pipe through the first pipe, the ammonia is discharged into the kettle body through the opening on the annular pipe, the motor is started, the motor drives the rotating shaft to rotate, the rotating shaft drives the rotating plate to rotate, and the rotating plate drives the chute to rotate.
Description
Technical Field
The utility model relates to the technical field of reaction kettles, in particular to an amidination reaction kettle for preparing diazinon.
Background
When the imidate hydrochloride is subjected to amidination, ammonia gas is generally introduced into a reaction kettle to react, as in the patent of 201821994934.1, the imidation reaction kettle for preparing diazinon is named, a worm and a stirrer are driven to rotate by a stepping motor, the imidate hydrochloride solution is stirred by the stirrer to sufficiently and rapidly react with the ammonia gas, and simultaneously, heat in a reaction barrel can be rapidly discharged by the rotation of a fan blade on a worm wheel and a rotating rod driven by the worm, so that the reaction is ensured to be smoothly carried out; however, the patent directly introduces ammonia into the reaction kettle, so that the concentration of the ammonia in a certain area in the reaction kettle is too high, and the concentration of the ammonia in other areas is too low, thereby affecting the reaction efficiency of the amidination reaction.
Disclosure of Invention
The utility model aims to solve the defects in the prior art, and provides an amidine reaction kettle for preparing diazinon.
In order to achieve the above purpose, the present utility model adopts the following technical scheme:
an amidine reaction kettle for preparing diazinon comprises a kettle body, wherein the top of the kettle body is detachably connected with a kettle cover, and the bottom of the kettle body is uniformly and fixedly connected with supporting legs.
Preferably, the top fixedly connected with support frame of cauldron lid, the top fixedly connected with motor of support frame, the output shaft fixedly connected with pivot of motor, the other end of pivot extends to the bottom of the cauldron body, the even fixedly connected with ten rotor plates of circumference side of pivot, the equal fixedly connected with of circumference side of pivot is at least two connecting plates that are located between the rotor plate, evenly has offered the chute between the two sides of connecting plate and rotor plate.
Preferably, the connecting block aligned with the connecting plate is uniformly and fixedly connected with on the inner wall of the circumferential side surface of the kettle body, the annular pipe encircling the rotating shaft is fixedly connected with on the other side of the connecting block, a circle of rotating groove aligned with the connecting plate is formed in the circumferential side surface of the annular pipe, one side of the connecting plate extends to the inside of the annular pipe, the bottom of the connecting plate is rotationally connected to the bottom of the rotating groove, the bottom of the rotating groove is rotationally connected with the rotating ring, and one end of the rotating ring is fixedly connected to one surface of the connecting plate.
Preferably, the circumference side of the annular tube is uniformly provided with holes, the inner wall of the circumference side of the annular tube is uniformly and fixedly connected with lugs which are aligned with the holes in a staggered way, and the inside of the annular tube is provided with rotating blocks.
Preferably, the side of the rotating block is provided with a supporting groove, the side of the connecting plate is slidably connected to the side of the supporting groove, and springs are fixedly connected between the bottom and the top of the supporting groove and the bottom and the top of the connecting plate.
Preferably, one side fixedly connected with of the rotating plate encircles the annular plate of pivot, and the fluting has evenly been seted up at the top of annular plate, has seted up the helicla flute that is located annular plate inside between two adjacent flutings, and the spiral direction of two helicla flute in two annular plates is opposite, and the equal fixedly connected with swash plate in top and bottom of two annular plates.
Preferably, the circumference side inner wall fixedly connected with pipeline one of ring pipe, circumference side sliding connection in the top of cauldron lid of pipeline one, the one end sliding connection of pipeline one has the sleeve pipe, the bottom fixedly connected with pump machine of the cauldron body, the inlet fixedly connected with pipeline three of pump machine, the other end of pipeline three extends to the bottom inner wall of the cauldron body, the liquid outlet fixedly connected with pipeline two of pump machine.
Compared with the prior art, the utility model provides an amidine reaction kettle for preparing diazinon, which has the following beneficial effects:
through the ring pipe that sets up, place the device on the horizontal working face vertically, open the kettle cover, put into the cauldron body with liquid, close the kettle cover, with ammonia pipe connection on the sleeve pipe, let into the ring pipe with ammonia through pipeline one, ammonia is discharged to the cauldron body through the trompil on the ring pipe, the starter motor, the motor drives the pivot and rotates, the pivot drives the pivoted plate and rotates, the pivoted plate drives the chute and rotates, pivoted plate and chute drive liquid stirring, improve the degree of consistency of liquid, the pivot drives the connecting plate and rotates, the connecting plate drives the pivoted block and rotates, the pivoted block is interrupted the touching lug, make the pivoted block reciprocate, the aperture is stopped up to the pivoted block interval, make ammonia interval blowout from the trompil, be favorable to preventing that ammonia from being too high in same regional content of piece, make ammonia can be even spread and react in the cauldron body, improve reaction efficiency, the pivot drives the annular plate and rotates, the swash plate stirs the liquid, make ammonia scatter fast, improve the degree of consistency of device internal reaction, the annular plate drives the helicoidal groove on the upper and lower two-layer annular plate drives liquid respectively and flows to cauldron body top and vertical direction, be favorable to mixing the liquid in the direction of reaction.
Drawings
FIG. 1 is a schematic diagram of the overall structure of an amidine reaction kettle for preparing diazinon according to the present utility model;
FIG. 2 is a schematic diagram of the internal structure of an amidine reaction kettle for preparing diazinon according to the present utility model;
FIG. 3 is a schematic view of an annular plate structure of an amidine reaction kettle for preparing diazinon according to the present utility model;
fig. 4 is an enlarged schematic view of the structure at a in fig. 2.
In the figure: 1-kettle body, 2-pipeline I, 3-sleeve, 4-kettle cover, 5-support frame, 6-motor, 7-rotating shaft, 8-sloping plate, 9-spiral groove, 10-grooving, 11-annular plate, 12-pipeline II, 13-pump, 14-supporting leg, 15-connecting plate, 16-annular pipe, 17-connecting block, 18-rotating ring, 19-chute, 20-rotating plate, 21-pipeline III, 22-supporting groove, 23-lug, 24-opening, 25-spring and 26-rotating block.
Detailed Description
Example 1:
referring to fig. 1, 2, 3 and 4, an amidinate reaction kettle for preparing diazinon comprises a kettle body 1, wherein a kettle cover 4 is detachably connected to the top of the kettle body 1, and supporting legs 14 are uniformly and fixedly connected to the bottom of the kettle body 1.
According to the utility model, the top of the kettle cover 4 is fixedly connected with the support frame 5, the top of the support frame 5 is fixedly connected with the motor 6, the output shaft of the motor 6 is fixedly connected with the rotating shaft 7, the other end of the rotating shaft 7 extends to the bottom of the kettle body 1, ten rotating plates 20 are uniformly and fixedly connected to the circumferential side surface of the rotating shaft 7, at least two connecting plates 15 positioned between the rotating plates 20 are fixedly connected to the circumferential side surface of the rotating shaft 7, and inclined grooves 19 are uniformly formed between the connecting plates 15 and two sides of the rotating plates 20.
The even fixedly connected with of circumference side inner wall of cauldron body 1 and connecting block 17 of connecting plate 15 alignment, the opposite side fixedly connected with of connecting block 17 encircles the annular pipe 16 of pivot 7, the round rotation groove of being aligned with connecting plate 15 has been seted up to the circumference side of annular pipe 16, one side of connecting plate 15 extends to the inside of annular pipe 16, the bottom of connecting plate 15 rotates to be connected in the bottom of rotation groove, the bottom of rotation groove rotates to be connected with swivel becket 18, the one end fixed connection of swivel becket 18 is in the one side of connecting plate 15.
The circumference side of the annular tube 16 is uniformly provided with holes 24, the inner wall of the circumference side of the annular tube 16 is uniformly and fixedly connected with lugs 23 which are aligned with the holes 24 in a staggered way, and a rotating block 26 is arranged inside the annular tube 16.
The side of the rotating block 26 is provided with a supporting groove 22, the side of the connecting plate 15 is slidably connected to the side of the supporting groove 22, and springs 25 are fixedly connected between the bottom and the top of the supporting groove 22 and the bottom and the top of the connecting plate 15.
One side of the rotating plate 20 is fixedly connected with an annular plate 11 encircling the rotating shaft 7, grooves 10 are uniformly formed in the top of the annular plate 11, spiral grooves 9 positioned inside the annular plate 11 are formed between two adjacent grooves 10, the rotation directions of the two spiral grooves 9 in the two annular plates 11 are opposite, and inclined plates 8 are uniformly and fixedly connected to the top and the bottom of the two annular plates 11.
The circumference side inner wall fixedly connected with pipeline one 2 of ring pipe 16, the circumference side sliding connection of pipeline one 2 is in the top of cauldron lid 4, and the one end sliding connection of pipeline one 2 has sleeve pipe 3, and the bottom fixedly connected with pump 13 of cauldron body 1, the inlet fixedly connected with pipeline three 21 of pump 13, the other end of pipeline three 21 extends to the bottom inner wall of cauldron body 1, the liquid outlet fixedly connected with pipeline two 12 of pump 13.
Working principle: the device is vertically placed on a horizontal working surface, the kettle cover 4 is opened, liquid is placed in the kettle body 1, the kettle cover 4 is closed, ammonia is connected to the sleeve pipe 3 through the first pipeline 2, ammonia is discharged into the kettle body 1 through the opening 24 on the annular pipe 16, the motor 6 is started, the motor 6 drives the rotating shaft 7 to rotate, the rotating shaft 7 drives the rotating plate 20 to rotate, the rotating plate 20 drives the chute 19 to rotate, the rotating plate 20 and the chute 19 drive liquid stirring, the uniformity of the liquid is improved, the rotating shaft 7 drives the connecting plate 15 to rotate, the connecting plate 15 drives the rotating block 26 to rotate, the rotating block 26 intermittently touches the convex block 23, the rotating block 26 moves up and down, the opening 24 is blocked by the rotating block 26 at intervals, ammonia is sprayed out of the opening 24 at intervals, ammonia is prevented from being excessively high in the same area content, ammonia can be uniformly dispersed in the kettle body 1, the reaction efficiency is improved, the rotating shaft 7 drives the annular plate 11 to rotate, the rotating plate 8 stirs the liquid, the ammonia is rapidly scattered, the inside the device is improved, the annular plate 11 drives the spiral groove 9 to drive the spiral groove 9 to move up and down, the liquid flows in the vertical direction on the liquid stirring direction, and the liquid is fully stirred up and down in the direction of the liquid is favorable for the liquid stirring direction.
The foregoing is only a preferred embodiment of the present utility model, but the scope of the present utility model is not limited thereto, and any person skilled in the art, who is within the scope of the present utility model, should make equivalent substitutions or modifications according to the technical scheme of the present utility model and the inventive concept thereof, and should be covered by the scope of the present utility model.
Claims (4)
1. An amidine reaction kettle for preparing diazinon comprises a kettle body (1), and is characterized in that the top of the kettle body (1) is detachably connected with a kettle cover (4), the bottom of the kettle body (1) is uniformly and fixedly connected with a supporting leg (14), the top of the kettle cover (4) is fixedly connected with a supporting frame (5), the top of the supporting frame (5) is fixedly connected with a motor (6), an output shaft of the motor (6) is fixedly connected with a rotating shaft (7), the other end of the rotating shaft (7) extends to the bottom of the kettle body (1), ten rotating plates (20) are uniformly and fixedly connected to the circumferential side surface of the rotating shaft (7), at least two connecting plates (15) positioned between the rotating plates (20) are uniformly and fixedly connected to the circumferential side surface of the rotating shaft (7), a chute (19) is uniformly and fixedly connected with a connecting block (17) aligned with the connecting plate (15) on the inner wall of the circumferential side surface of the kettle body (1), a pipe (16) encircling the rotating shaft (7) is fixedly connected with the other side of the connecting block (17), a ring-shaped side surface of the ring-shaped pipe (16) is provided with a ring-shaped groove aligned with the connecting plate (15) and is connected with the bottom of the connecting plate (15) which is aligned with the rotating groove (15), the bottom of the rotating groove is rotationally connected with a rotating ring (18), one end of the rotating ring (18) is fixedly connected with one surface of a connecting plate (15), the circumferential side surface of the annular tube (16) is uniformly provided with holes (24), the inner wall of the circumferential side surface of the annular tube (16) is uniformly and fixedly connected with lugs (23) which are aligned with the holes (24) in a staggered mode, and a rotating block (26) is arranged in the annular tube (16).
2. The amidine reaction kettle for preparing diazinon according to claim 1, wherein the side surface of the rotating block (26) is provided with a supporting groove (22), the side surface of the connecting plate (15) is slidably connected to the side surface of the supporting groove (22), and springs (25) are fixedly connected between the bottom and the top of the supporting groove (22) and the bottom and the top of the connecting plate (15).
3. The amidine reaction kettle for preparing diazinon according to claim 2, wherein one side of the rotating plate (20) is fixedly connected with an annular plate (11) encircling the rotating shaft (7), grooves (10) are uniformly formed in the top of the annular plate (11), spiral grooves (9) positioned inside the annular plate (11) are formed between two adjacent grooves (10), the rotation directions of the two spiral grooves (9) in the two annular plates (11) are opposite, and inclined plates (8) are uniformly and fixedly connected to the top and the bottom of the two annular plates (11).
4. The amidine reaction kettle for preparing diazinon according to claim 3, wherein the inner wall of the circumferential side surface of the annular tube (16) is fixedly connected with a first pipeline (2), the circumferential side surface of the first pipeline (2) is slidably connected to the top of the kettle cover (4), one end of the first pipeline (2) is slidably connected with a sleeve (3), the bottom of the kettle body (1) is fixedly connected with a pump (13), a liquid inlet of the pump (13) is fixedly connected with a third pipeline (21), the other end of the third pipeline (21) extends to the inner wall of the bottom of the kettle body (1), and a liquid outlet of the pump (13) is fixedly connected with a second pipeline (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223316940.0U CN220194801U (en) | 2022-12-12 | 2022-12-12 | Amidine reaction kettle for preparing diazinon |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223316940.0U CN220194801U (en) | 2022-12-12 | 2022-12-12 | Amidine reaction kettle for preparing diazinon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220194801U true CN220194801U (en) | 2023-12-19 |
Family
ID=89138431
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202223316940.0U Active CN220194801U (en) | 2022-12-12 | 2022-12-12 | Amidine reaction kettle for preparing diazinon |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220194801U (en) |
-
2022
- 2022-12-12 CN CN202223316940.0U patent/CN220194801U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN207271385U (en) | A kind of modified Ball-stirring mill circulatory system | |
| CN208389904U (en) | A kind of agricultural liquids fertilizer high-efficiency mixing device | |
| CN220194801U (en) | Amidine reaction kettle for preparing diazinon | |
| CN206562436U (en) | A kind of enzyme digestion reaction kettle extracted for Moringa | |
| CN208428468U (en) | A kind of blender for building | |
| CN210496058U (en) | High-efficiency stirrer | |
| CN208694861U (en) | A kind of blender for sewage treatment | |
| CN216303312U (en) | Water treatment facilities water inlet charge device | |
| CN207254128U (en) | A kind of dosing agitating device of sewage disposal | |
| CN214261621U (en) | Agitating unit is used in fruit food production | |
| CN107570067A (en) | UV gloss oil high-efficiency stirring equipment is used in a kind of air detection instrument shell production | |
| CN206027540U (en) | High -efficient practical liquid mixer | |
| CN210159550U (en) | High-speed mixer | |
| CN210620356U (en) | High-efficient mixed processing apparatus of catalytic oxidation agent sewage | |
| CN213651985U (en) | Supercritical water oxidation treatment device for organic wastewater | |
| CN208211401U (en) | Tumbler is used in a kind of production of pressed salted duck | |
| CN220696495U (en) | Stirrer | |
| CN218465767U (en) | Rapid cooling device for wine tank | |
| CN219722543U (en) | Enzyme preparation refining stirring and dissolving device | |
| CN209646329U (en) | A kind of blender for sewage treatment | |
| CN216654212U (en) | Agitating unit is used in water clarifier production | |
| CN212609607U (en) | Stirring impeller for water treatment | |
| CN214182797U (en) | Sludge mixing stirrer | |
| CN220634333U (en) | Reaction kettle for emulsion preparation | |
| CN213966077U (en) | Synthetic multi-rod mixing device of using of environmental protection reagent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |