CN220194030U - Crystallization device for color fixing agent production - Google Patents
Crystallization device for color fixing agent production Download PDFInfo
- Publication number
- CN220194030U CN220194030U CN202321206639.6U CN202321206639U CN220194030U CN 220194030 U CN220194030 U CN 220194030U CN 202321206639 U CN202321206639 U CN 202321206639U CN 220194030 U CN220194030 U CN 220194030U
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- Prior art keywords
- crystallization
- support
- frame
- fixing agent
- reaction kettle
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- 238000002425 crystallisation Methods 0.000 title claims abstract description 97
- 230000008025 crystallization Effects 0.000 title claims abstract description 97
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 230000007246 mechanism Effects 0.000 claims abstract description 38
- 238000006243 chemical reaction Methods 0.000 claims abstract description 31
- 238000000605 extraction Methods 0.000 claims abstract description 23
- 230000003014 reinforcing effect Effects 0.000 claims description 4
- 238000005452 bending Methods 0.000 claims 1
- 239000013078 crystal Substances 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 6
- 238000001914 filtration Methods 0.000 abstract description 4
- 239000007788 liquid Substances 0.000 abstract description 4
- 239000003795 chemical substances by application Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- GEYOCULIXLDCMW-UHFFFAOYSA-N 1,2-phenylenediamine Chemical compound NC1=CC=CC=C1N GEYOCULIXLDCMW-UHFFFAOYSA-N 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 241001330002 Bambuseae Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a crystallization device for producing a color fixing agent, which comprises a crystallization reaction kettle mechanism, wherein a support mechanism is fixedly arranged at the bottom of the crystallization reaction kettle mechanism, a transverse frame mechanism is fixedly arranged on the side surface of the support mechanism, a supporting sleeve and a hydraulic pushing device are fixedly arranged at the top of the transverse frame mechanism, a telescopic sliding cylinder is longitudinally inserted in the supporting sleeve in a sliding manner, and the hydraulic pushing device is positioned in the supporting sleeve and is not connected with the supporting sleeve. The crystallization extraction basket frame provided with the meshes of the crystallization filtering fence is used as a crystallization extraction structure, the output end of the crystallization extraction basket frame is pushed to be lifted by the hydraulic pushing device, the cross transverse frame, the supporting transverse plate, the supporting bent shaft frame and the crystallization extraction basket frame are driven to be lifted, liquid is filtered out through the meshes of the crystallization filtering fence, and crystals reaching the granularity standard are lifted out, so that the effect of conveniently extracting crystals with granularity reaching the standard in real time is achieved, and the effects of facilitating subsequent full reaction and crystallization extraction are achieved.
Description
Technical Field
The utility model relates to the technical field of chemical equipment, in particular to a crystallization device for producing a color fixing agent.
Background
Phenol, 4-Methyl 1,3-phenylene diisocyanate and 4,4'
Mixing the diaminobenzene with ethyl acetate, maintaining a certain temperature, stirring and reacting to form solid, concentrating the solvent until the solvent is dry, and discharging the solid. Through technological improvement, the crystallization temperature is controlled by a program, the crystallization form is controlled, and impurities and residual unreacted raw materials are effectively removed through centrifugal separation, so that the aim of purification is fulfilled. For crystals produced in the crystallization reaction vessel, extraction is required for subsequent processing.
The Chinese patent document with the publication number of CN215387664U discloses a crystallization device, which comprises a crystallization tank, the inside of crystallization tank is provided with rabbling mechanism, the right side of crystallization tank is provided with exhaust mechanism, and rabbling mechanism includes motor, puddler and stirring piece, the top of puddler is connected with the output of motor, the one end of stirring piece is connected with the outer wall of puddler, and exhaust mechanism includes gas vent … …. Aiming at the technical scheme, the following defects exist in use: in the crystallization reaction, the existing chemical crystallization device is inconvenient to extract crystals with the granularity reaching the standard in real time, and is unfavorable for the subsequent full reaction and crystallization extraction.
For this purpose, crystallization devices for the production of fixing agents are proposed.
Disclosure of Invention
Aiming at the defects of the prior art, the utility model provides a crystallization device for producing a color fixing agent, which solves the problems that the existing chemical crystallization device is inconvenient to extract crystals with the granularity reaching the standard in real time in crystallization reaction and is unfavorable for subsequent full reaction and crystallization extraction.
In order to achieve the above purpose, the present utility model adopts the following technical scheme:
the crystallization device for producing the color fixing agent comprises a crystallization reaction kettle mechanism, a support mechanism is fixedly arranged at the bottom of the crystallization reaction kettle mechanism, a transverse frame mechanism is fixedly arranged on the side surface of the support mechanism, a supporting sleeve and a hydraulic pushing device are fixedly arranged at the top of the transverse frame mechanism, a telescopic sliding cylinder is longitudinally inserted in the supporting sleeve in a sliding manner, the hydraulic pushing device is positioned in the supporting sleeve and is not connected with the supporting sleeve, an output end of the hydraulic pushing device is fixedly connected with the bottom surface of the inner wall of the telescopic sliding cylinder, a cross transverse frame is fixedly arranged at the top of the telescopic sliding cylinder, a supporting transverse plate is fixedly arranged at the middle part of the bottom surface of the cross transverse frame, a supporting bent shaft frame is fixedly arranged at the bottom surface of the supporting transverse plate, a reinforcing hoop is fixedly arranged at the inner part of the supporting bent shaft frame, a crystallization extraction basket frame is fixedly arranged at the bottom end of the supporting bent shaft frame, and crystallization extraction basket meshes are formed by penetrating through the inside and outside of a shell of the crystallization extraction basket frame.
Preferably, the crystallization reaction kettle mechanism comprises a heat conduction kettle bottom shell, a reaction kettle body and a kettle opening ring frame, wherein the heat conduction kettle bottom shell and the kettle opening ring frame are respectively and fixedly arranged at the top and the bottom of the reaction kettle body.
Preferably, the support mechanism comprises a support leg column and a lapping foot plate, and the lapping foot plate is fixedly arranged at the bottom end of the support leg column.
Preferably, the hydraulic pushing device includes an electro-hydraulic cylinder and an output piston push rod portion provided inside the electro-hydraulic cylinder.
Preferably, the supporting and hanging bent axle frame is composed of a plurality of cylindrical bent axles, and the plurality of cylindrical bent axles are equidistantly and circumferentially distributed on the edge of the bottom surface of the supporting transverse plate.
Preferably, the crystallization filter fence mesh is circular through hole, crystallization draws the basket and is spherical sleeve column structure, the quantity of crystallization filter fence mesh is a plurality of, and a plurality of crystallization filter fence mesh equidistance encircle the casing that distributes in crystallization and draw the basket.
Compared with the prior art, the utility model has the beneficial effects that: this crystallization device that color fixing agent production was used extracts basket as crystallization through setting up the crystallization of seting up crystallization filter screen mesh and draws the structure to through setting up hydraulic pushing device in order to make its output promote flexible slide, and then drive cross crossbeams, support the crossbeams, prop up and hang bent axle frame and crystallization and draw basket to rise, filter the liquid through crystallization filter screen mesh, thereby will reach the crystallization lift of granularity standard and go out, thereby reached the effect that is convenient for reach the crystallization of standard in real time and draw, realized doing benefit to follow-up abundant reaction and crystallization and extracted effect.
Drawings
FIG. 1 is a perspective view of the structure of the present utility model;
FIG. 2 is a partial sectional perspective view of the present utility model;
fig. 3 is a partially exploded perspective view of another embodiment of the present utility model.
In the figure: the crystallization reaction kettle comprises a crystallization reaction kettle mechanism, a 2 support mechanism, a 3 transverse frame mechanism, a 4 support sleeve, a 5 telescopic slide cylinder, a 6 hydraulic pushing device, a 7 cross transverse frame, an 8 support transverse plate, 9 hanging bent axle frames, 10 reinforcing hoops, 11 crystallization extraction basket frames, 12 crystallization filter column meshes, a 101 reaction kettle body, a 102 heat conduction kettle bottom shell, a 103 kettle mouth ring frame, 201 support legs, 202 lap joint foot plates, 601 electric hydraulic cylinders and 602 output piston push rod parts.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1-3, the crystallization device for producing the fixing agent comprises a crystallization reaction kettle mechanism 1, a support mechanism 2 is fixedly arranged at the bottom of the crystallization reaction kettle mechanism 1, a transverse frame mechanism 3 is fixedly arranged on the side surface of the support mechanism 2, a supporting sleeve 4 and a hydraulic pushing device 6 are fixedly arranged at the top of the transverse frame mechanism 3, a telescopic sliding cylinder 5 is longitudinally and slidably inserted into the supporting sleeve 4, the hydraulic pushing device 6 is positioned in the supporting sleeve 4 and is not connected with the supporting sleeve, an output end of the hydraulic pushing device 6 is fixedly connected with the bottom surface of the inner wall of the telescopic sliding cylinder 5, a cross transverse frame 7 is fixedly arranged at the top of the telescopic sliding cylinder 5, a supporting transverse plate 8 is fixedly arranged at the middle part of the bottom surface of the cross transverse frame 7, a supporting bent shaft frame 9 is fixedly arranged at the bottom surface of the supporting transverse plate 8, a reinforcing hoop 10 is fixedly arranged at the inner side surface of the supporting bent shaft frame 9, a crystallization extraction basket frame 11 is fixedly arranged at the bottom end of the supporting bent shaft frame 9, and crystallization filtering bars 12 are arranged inside and outside and extend through the shell of the crystallization extraction basket frame 11.
In the utility model, the crystallization reaction kettle mechanism 1 comprises a heat conduction kettle bottom shell 102, a reaction kettle body 101 and a kettle mouth ring frame 103, wherein the heat conduction kettle bottom shell 102 and the kettle mouth ring frame 103 are respectively and fixedly arranged at the top and the bottom of the reaction kettle body 101.
In the utility model, the support mechanism 2 comprises a support leg 201 and a lapping foot plate 202, and the lapping foot plate 202 is fixedly arranged at the bottom end of the support leg 201.
In the present utility model, the hydraulic pushing device 6 includes an electro-hydraulic cylinder 601 and an output piston rod portion 602, and the output piston rod portion 602 is provided inside the electro-hydraulic cylinder 601.
In the utility model, the supporting and hanging bent axle bracket 9 consists of a plurality of cylindrical bent axles, and the plurality of cylindrical bent axles are equidistantly and circumferentially distributed on the edge of the bottom surface of the supporting transverse plate 8.
In the utility model, the crystallization filter screen holes 12 are circular through holes, the crystallization extraction basket 11 is in a spherical sleeve structure, the number of the crystallization filter screen holes 12 is a plurality, and the plurality of crystallization filter screen holes 12 are equidistantly distributed around the shell of the crystallization extraction basket 11.
When in use: when the crystals generated in the crystallization reaction kettle mechanism 1 are extracted in real time, the hydraulic pushing device 6 is started to enable the output end of the hydraulic pushing device to push the telescopic sliding cylinder 5 to lift, the telescopic sliding cylinder 5 can longitudinally slide in the supporting sleeve 4, the cross transverse frame 7 is driven to lift, namely, the supporting transverse plate 8 and the supporting bent shaft frame 9 are driven to lift, the crystal extraction basket frame 11 is driven to lift, liquid is filtered through the crystal filtering fence mesh 12, and therefore crystals reaching the granularity standard are lifted out, and the crystals are extracted in real time.
To sum up, this crystallization device that fixing agent production was used, the crystallization through setting up and set up crystallization of crystallization filter column mesh 12 draws basket 11 as crystallization extraction structure, and promote flexible smooth section of thick bamboo 5 through setting up hydraulic pushing device 6 in order to make its output promote, and then drive cross crossbeams 7, support crossbeams 8, prop up and hang bent axle frame 9 and crystallization and draw basket 11 to rise, filter out liquid through crystallization filter column mesh 12, thereby will reach the crystallization lift of granularity standard, thereby reached and be convenient for reach the effect that the crystallization that the granularity reached the standard in real time was extracted, the effect that has realized doing benefit to follow-up abundant reaction and crystallization extraction, the crystallization that has solved current chemical industry crystallization device in crystallization reaction, be unfavorable for reaching the standard crystallization in real time is difficult to follow-up abundant reaction and crystallization extraction problem.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides a crystallization device that color fixing agent production was used, includes crystallization reaction kettle mechanism (1), a serial communication port, the bottom fixed mounting of crystallization reaction kettle mechanism (1) has support mechanism (2), the side fixed surface of support mechanism (2) installs crossbeams mechanism (3), the top fixed mounting of crossbeams mechanism (3) has support sleeve (4) and hydraulic pressure thrust unit (6), the inside longitudinal sliding grafting of support sleeve (4) has flexible slide (5), and hydraulic pressure thrust unit (6) are located the inside of support sleeve (4) and are not connected with it, the output of hydraulic pressure thrust unit (6) and flexible slide (5) inner wall bottom surface fixed connection, the top fixed mounting of flexible slide (5) has cross crossbeams (7), the middle part fixed mounting of cross crossbeams (7) bottom surface has support crossbeams (8), the inside fixed mounting of support crossbeams (8) has reinforcing band (10), the inside of support cradle (9) has bending collar (10), the bottom of crystallization extraction basket (11) is fixed mounting has crystallization basket (11) to be seted up.
2. The crystallization device for producing the color fixing agent according to claim 1, wherein the crystallization reaction kettle mechanism (1) comprises a heat conduction kettle bottom shell (102), a reaction kettle body (101) and a kettle mouth ring frame (103), and the heat conduction kettle bottom shell (102) and the kettle mouth ring frame (103) are respectively fixedly installed at the top and the bottom of the reaction kettle body (101).
3. The crystallization device for producing a color fixing agent according to claim 1, wherein the support mechanism (2) comprises a support leg column (201) and a lapping foot plate (202), and the lapping foot plate (202) is fixedly installed at the bottom end of the support leg column (201).
4. The crystallization device for the production of a fixing agent according to claim 1, characterized in that the hydraulic pushing device (6) comprises an electro-hydraulic cylinder (601) and an output piston rod portion (602), the output piston rod portion (602) being arranged inside the electro-hydraulic cylinder (601).
5. The crystallization device for producing a color fixing agent according to claim 1, wherein the supporting and hanging bent shaft frame (9) is composed of a plurality of cylindrical bent shafts, and the plurality of cylindrical bent shafts are equidistantly distributed around the edge of the bottom surface of the supporting transverse plate (8).
6. The crystallization device for producing a color fixing agent according to claim 1, wherein the crystallization filter screen holes (12) are round through holes, the crystallization extraction basket frame (11) is of a spherical sleeve structure, the number of the crystallization filter screen holes (12) is multiple, and the crystallization filter screen holes (12) are equidistantly distributed around the shell of the crystallization extraction basket frame (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321206639.6U CN220194030U (en) | 2023-05-18 | 2023-05-18 | Crystallization device for color fixing agent production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321206639.6U CN220194030U (en) | 2023-05-18 | 2023-05-18 | Crystallization device for color fixing agent production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220194030U true CN220194030U (en) | 2023-12-19 |
Family
ID=89141134
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321206639.6U Active CN220194030U (en) | 2023-05-18 | 2023-05-18 | Crystallization device for color fixing agent production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220194030U (en) |
-
2023
- 2023-05-18 CN CN202321206639.6U patent/CN220194030U/en active Active
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