CN220125537U - A enrichment facility for extracting flavonoid - Google Patents
A enrichment facility for extracting flavonoid Download PDFInfo
- Publication number
- CN220125537U CN220125537U CN202321264945.5U CN202321264945U CN220125537U CN 220125537 U CN220125537 U CN 220125537U CN 202321264945 U CN202321264945 U CN 202321264945U CN 220125537 U CN220125537 U CN 220125537U
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- fixed
- air duct
- tank
- bevel gear
- sealing cover
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- 229930003935 flavonoid Natural products 0.000 title claims abstract description 15
- 150000002215 flavonoids Chemical class 0.000 title claims abstract description 15
- 235000017173 flavonoids Nutrition 0.000 title claims abstract description 15
- 238000004821 distillation Methods 0.000 claims abstract description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 39
- 238000007789 sealing Methods 0.000 claims abstract description 32
- 230000000903 blocking effect Effects 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 10
- 239000000126 substance Substances 0.000 claims abstract description 7
- 230000000149 penetrating effect Effects 0.000 claims description 5
- 238000003466 welding Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 description 8
- 239000002994 raw material Substances 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- 101100298225 Caenorhabditis elegans pot-2 gene Proteins 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model relates to the technical field of chemical industry, in particular to a concentrating device for extracting flavonoid substances, wherein a mounting seat is fixed in a water tank, and a distillation tank is fixed on the mounting seat; the stirring rod is arranged in the distillation tank, is screwed on the bottom plate of the distillation tank through a shaft and a bearing, and is connected with the built-in driving device of the mounting seat; the charging tank is fixed on the sealing cover; the pressing plate is embedded in the charging tank; the blocking block is blocked at the bottom of the charging tank and the top of the sealing cover; the heating in water bath is convenient to be carried out and is uniform; can carry out feeding in the distillation process, keep the air pressure stable and improve the practicability.
Description
Technical Field
The utility model relates to the technical field of chemical industry, in particular to a concentrating device for extracting flavonoid substances.
Background
The most commonly used method for extracting flavonoids is that the common organic solvents mainly comprise ethanol, diethyl ether, methanol, ethyl acetate and the like, wherein the ethanol is the most commonly used method for extracting flavonoids by distillation and concentration through a rotary evaporator, but the quantity of the flavonoids extracted through the rotary evaporator is relatively small, and continuous addition is inconvenient, so that a concentrating device for extracting flavonoids is now proposed.
Disclosure of Invention
The utility model aims to overcome the defects and shortcomings of the prior art and provides a concentrating device for extracting flavonoid substances, which is used for solving the problems.
In order to achieve the above purpose, the utility model adopts the following technical scheme: the device comprises a water tank, a distillation tank, a sealing cover, a first air duct, a collecting bottle, a second air duct and a vacuum pump; the water tank is internally provided with a heating device which is connected with an external power supply; a distillation tank is arranged in the water tank, and a sealing cover is arranged on the distillation tank; the right part of the sealing cover is connected with a first air duct, a condensing pipe is arranged on the first air duct, a collecting bottle is arranged on the right side of the distillation pot, and the first air duct is inserted on the collecting bottle; the first air duct is connected with a second air duct, the right end of the second air duct is connected with a vacuum pump, the vacuum pump is connected with an external power supply, and the vacuum pump is provided with a pressure gauge;
it also comprises:
the installation seat is fixed in the water tank, and the distillation pot is fixed on the installation seat;
the stirring rod is arranged in the distillation tank, is screwed on the bottom plate of the distillation tank through a shaft and a bearing, and is connected with a driving device arranged in the mounting seat;
the charging tank is fixed on the sealing cover;
the pressing plate is embedded in the charging tank;
the device comprises a blocking block, wherein the blocking block is arranged at the bottom of a charging tank and the top of a sealing cover, an inner threaded pipe is fixed at the bottom of the blocking block, a screw rod is inserted in the inner threaded pipe in a screwed manner, a first bevel gear is fixed at the bottom of the screw rod, a second bevel gear is meshed with the left end of the first bevel gear, a first rotating shaft is fixed on the left side wall of the second bevel gear, a third bevel gear is fixed at the left end of the first rotating shaft, a fourth bevel gear is meshed with the left side of the third bevel gear, a second rotating shaft is fixed at the upper end of the fourth bevel gear, the upper end of the second rotating shaft passes through the sealing cover in a screwed manner through a sealing bearing, and then is connected with an output shaft of a rotating motor, and the rotating motor is fixed on the sealing cover; the rotating motor is connected with an external power supply;
the fixed plate, the fixed plate fix on the interior roof of sealed lid, first pivot is worn to establish on the fixed plate through the bearing soon, the movable sleeve is equipped with spacing frame on the fixed plate, is fixed with the connecting rod on the right side wall of spacing frame, the other end and the internal thread pipe of connecting rod are fixed.
Preferably, the upper end of the pressing plate is fixed with a pull rod, and the upper end of the pull rod is integrally formed with a pull ring.
Preferably, the blocking block is of a conical structure, the conical structure is convenient for blocking, and the pressure is increased to reduce water leakage.
Preferably, the water tank is arranged on the right side of the collecting bottle, and the upper end of the left side of the annular wall of the water tank is fixed with the vacuum pump through the bracket; the air outlet end of the vacuum pump is connected with a third air duct, a hose is connected to the third air duct, the other end of the hose is connected with a fourth air duct, and the fourth air duct is arranged in the water tank in an extending mode.
Preferably, the drain pipe is connected with the drain pipe in a penetrating way at the left side of the bottom of the distillation tank, the solenoid valve is arranged in the drain pipe, the drain pipe is arranged from right to left from high to low, and the drain pipe penetrates through the annular wall of the water tank.
Compared with the prior art, the utility model has the beneficial effects that: the utility model provides a concentrating device for extracting flavonoid substances, which is convenient for heating in water bath and is heated uniformly; can carry out feeding in the distillation process, keep the air pressure stable and improve the practicability.
Drawings
In order to more clearly illustrate the embodiments of the utility model or the technical solutions of the prior art, the drawings which are used in the description of the embodiments or the prior art will be briefly described, it being obvious that the drawings in the description below are only some embodiments of the utility model, and that other drawings can be obtained according to these drawings without inventive faculty for a person skilled in the art.
Fig. 1 is a schematic structural view of the present utility model.
FIG. 2 is a schematic view of the structure of the utility model with the trough, retort, seal cover, mount, feed tank and platen broken away.
Fig. 3 is an enlarged view of a portion a in fig. 2.
Fig. 4 is an enlarged view of a portion B in fig. 2.
Reference numerals illustrate:
the device comprises a water tank 1, a distillation tank 2, a sealing cover 3, a first air duct 4, a collecting bottle 5, a second air duct 6, a vacuum pump 7, a mounting seat 8, a stirring rod 9, a charging tank 10, a pressing plate 11, a pull rod 12, a pull ring 13, a blocking block 14, an internally threaded pipe 15, a screw 16, a first bevel gear 17, a second bevel gear 18, a first rotating shaft 19, a third bevel gear 20, a fourth bevel gear 21, a second rotating shaft 22, a rotating motor 23, a fixed plate 24, a limiting frame 25, a connecting rod 26, a water tank 27, a third air duct 28, a hose 29, a fourth air duct 30, a drain pipe 31 and a condensing pipe 32.
Detailed Description
The utility model is further described below with reference to the accompanying drawings.
Example 1:
referring to fig. 1 to 4, the embodiment 1 comprises a water tank 1, a distillation pot 2, a sealing cover 3, a first air duct 4, a collecting bottle 5, a second air duct 6 and a vacuum pump 7; the water tank 1 is internally provided with a heating device, such as a heating rod and the like, and the heating device is connected with an external power supply; a distillation tank 2 is arranged in the water tank 1, and a sealing cover 3 is arranged on the distillation tank 2; the right part of the sealing cover 3 is connected with a first air duct 4, a condensing pipe 32 is arranged on the first air duct 4, a collecting bottle 5 is arranged on the right side of the distillation pot 2, and the first air duct 4 is inserted on the collecting bottle 5; the first air duct 4 is connected with a second air duct 6, the right end of the second air duct 6 is connected with a vacuum pump 7, the vacuum pump 7 is connected with an external power supply, and the vacuum pump 7 is provided with a pressure gauge;
it also comprises:
the distillation tank comprises a mounting seat 8, wherein the mounting seat 8 is fixed in the water tank 1, and the distillation tank 2 is fixed on the mounting seat 8;
the stirring rod 9 is arranged in the distillation tank 2, the stirring rod 9 is screwed on the bottom plate of the distillation tank 2 through a shaft and a bearing, and a driving device such as a motor is arranged in the mounting seat 8 and connected with the stirring rod 9;
a charging tank 10, wherein the charging tank 10 is fixed on the sealing cover 3;
the pressing plate 11 is embedded in the charging tank 10; the upper end of the pressing plate 11 is welded and fixed with a pull rod 12, and the upper end of the pull rod 12 is integrally formed with a pull ring 13;
the blocking block 14 is blocked at the bottom of the charging tank 10 and the top of the sealing cover 3, and the blocking block 14 is of a conical structure; the bottom of the blocking block 14 is stuck and fixed with an internal thread pipe 15 through glue, the inside of the internal thread pipe 15 is screwed and inserted with a screw 16, the bottom of the screw 16 is fixed with a first bevel gear 17, the left end of the first bevel gear 17 is meshed with a second bevel gear 18, the left side wall of the second bevel gear 18 is fixed with a first rotating shaft 19 through a bolt, the left end of the first rotating shaft 19 is fixed with a third bevel gear 20 through a bolt, the left side of the third bevel gear 20 is meshed with a fourth bevel gear 21, the upper end of the fourth bevel gear 21 is fixed with a second rotating shaft 22 through a bolt, the upper end of the second rotating shaft 22 is screwed and connected with an output shaft of a rotating motor 23 after penetrating through a sealing cover 3 through a sealing bearing, the rotating motor 23 is fixed on the sealing cover 3 through a bolt, and the specific use model of the rotating motor 23 is directly purchased and installed and used from the market according to practical use requirements; the rotary motor 23 is connected with an external power supply;
the fixed plate 24, the fixed plate 24 is fixed on the inner top plate of the sealing cover 3, the first rotating shaft 19 is rotatably connected and penetrated on the fixed plate 24 through a bearing, a limit frame 25 is movably sleeved on the fixed plate 24, a connecting rod 26 is fixed on the right side wall of the limit frame 25 through a bolt, and the other end of the connecting rod 26 is fixed with the inner threaded pipe 15;
in the embodiment 1, a heating device is started to heat water in a water tank 1, a sealing cover 3 is opened to add raw materials, the sealing cover 3 is closed, a driving device is started to enable a stirring rod to rotate, a stirring rod 9 is driven to rotate to enable the raw materials to be heated and distilled uniformly, and the air pressure in a distillation tank 2 is regulated through a vacuum pump 7 according to the indication of a pressure gauge; the distilled gas is liquefied through a first gas guide pipe 4 and then enters a collecting bottle 5 through a condensing pipe 32; during charging, the pressing plate 11 is taken out by the pull ring 13, raw materials are added into the charging tank 10, the pressing plate 11 is put back, the rotating motor 23 is started, the rotating motor 23 drives the second rotating shaft 22 to rotate, the fourth bevel gear 21, the third bevel gear 20, the first rotating shaft 19, the second bevel gear 18 and the first bevel gear 17 are driven to rotate, the screw 16 rotates, the internal threaded pipe 15 is lowered under the action of the limiting frame 25, the blocking block 14 is driven to be lowered, the pressing plate 11 moves downwards under the action of atmospheric pressure, and the raw materials are extruded into the distillation tank 2, and meanwhile, the internal air pressure is controlled through the vacuum pump 7.
Example 2:
referring to fig. 1, on the basis of embodiment 1, a water tank 27 is provided on the right side of a collection bottle 5, and the upper end of the left side of the annular wall of the water tank 27 is fixed with a vacuum pump 7 by a bracket; the air outlet end of the vacuum pump 7 is connected with a third air duct 28, a hose 29 is connected to the third air duct 28, a fourth air duct 30 is connected to the other end of the hose 29, and the fourth air duct 30 is arranged in the water tank 27 in an extending mode;
when the vacuum pump 7 is used for controlling the air pressure, the pumped air enters the water tank 27 through the fourth air duct 30, and the liquid in the water tank 27 is consistent with the liquid after the distilled air is liquefied, so that the liquid is prevented from splashing when the air pressure is regulated; after use, hose 29 and fourth air duct 30 are removed and water tank 27 is removed for cleaning.
Example 3:
referring to fig. 2, on the basis of embodiment 1, a drain pipe 31 is connected to the left side of the bottom of the distillation tank 2 in a penetrating manner, an electromagnetic valve is arranged in the drain pipe 31, the drain pipe 31 is arranged from right to left in a manner of being from high to low, and the drain pipe 31 is arranged on the annular wall of the water tank 1 in a penetrating manner;
with this embodiment, after distillation, the drain pipe 31 is opened to drain the concentrated liquid.
The working principle of the specific embodiment is as follows: starting a heating device to heat water in the water tank 1, opening a sealing cover 3 to add raw materials, closing the sealing cover 3, starting a driving device to enable a stirring rod to rotate, driving a stirring rod 9 to rotate to enable the raw materials to be heated and distilled uniformly, and adjusting the air pressure in the distillation tank 2 through a vacuum pump 7 according to the indication of a pressure gauge; the distilled gas is liquefied through a first gas guide pipe 4 and then enters a collecting bottle 5 through a condensing pipe 32; during charging, the pressing plate 11 is taken out by using the pull ring 13, raw materials are added into the charging tank 10, the pressing plate 11 is put back, the rotating motor 23 is started, the rotating motor 23 drives the second rotating shaft 22 to rotate, the fourth bevel gear 21, the third bevel gear 20, the first rotating shaft 19, the second bevel gear 18 and the first bevel gear 17 are driven to rotate, the screw 16 is driven to rotate, the internal threaded pipe 15 is driven to descend under the action of the limiting frame 25, the blocking block 14 is driven to descend, the pressing plate 11 moves downwards under the action of atmospheric pressure, the raw materials are extruded into the distillation tank 2, and meanwhile, the internal air pressure is controlled by the vacuum pump 7; when the vacuum pump 7 controls the air pressure, the pumped air enters the water tank 27 through the fourth air duct 30, and the liquid in the water tank 27 is consistent with the liquid after the distilled air is liquefied, so that the liquid is prevented from splashing when the air pressure is regulated; after the distillation, the drain pipe 31 is opened to drain the concentrated liquid.
After adopting above-mentioned structure, this concrete embodiment's beneficial effect does:
1. the built-in stirring rod 9 is arranged, so that the heating in water bath is convenient to be uniform;
2. the feeding tank 10 is arranged, so that feeding can be performed in the distillation process, the air pressure is kept stable, and the practicability is improved.
The foregoing is merely illustrative of the present utility model and not restrictive, and other modifications and equivalents thereof may occur to those skilled in the art without departing from the spirit and scope of the present utility model.
Claims (5)
1. A concentrating device for extracting flavonoid substances comprises a water tank (1), a distillation tank (2), a sealing cover (3), a first air duct (4), a collecting bottle (5), a second air duct (6) and a vacuum pump (7); a heating device is arranged in the water tank (1) and is connected with an external power supply; a distillation tank (2) is arranged in the water tank (1), and a sealing cover (3) is arranged on the distillation tank (2); the right part of the sealing cover (3) is connected with a first air duct (4), a condensing tube (32) is arranged on the first air duct (4), a collecting bottle (5) is arranged on the right side of the distillation pot (2), and the first air duct (4) is inserted on the collecting bottle (5); the first air duct (4) is connected with a second air duct (6), the right end of the second air duct (6) is connected with a vacuum pump (7), the vacuum pump (7) is connected with an external power supply, and the vacuum pump (7) is provided with a pressure gauge;
characterized in that it further comprises:
the distillation tank comprises a mounting seat (8), wherein the mounting seat (8) is fixed in a water tank (1), and a distillation tank (2) is fixed on the mounting seat (8);
the stirring rod (9) is arranged in the distillation tank (2), the stirring rod (9) is connected to the bottom plate of the distillation tank (2) in a screwed mode through a shaft and a bearing, and a driving device arranged in the mounting seat (8) is connected with the stirring rod (9);
the feeding tank (10) is fixed on the sealing cover (3);
the pressing plate (11) is embedded in the feeding tank (10);
the device comprises a blocking block (14), wherein the blocking block (14) is blocked at the bottom of a charging tank (10) and the top of a sealing cover (3), an inner threaded pipe (15) is fixed at the bottom of the blocking block (14), a screw (16) is inserted in the inner threaded pipe (15) in a screwed manner, a first bevel gear (17) is fixed at the bottom of the screw (16), a second bevel gear (18) is meshed with the left end of the first bevel gear (17), a first rotating shaft (19) is fixed on the left side wall of the second bevel gear (18), a third bevel gear (20) is fixed at the left end of the first rotating shaft (19), a fourth bevel gear (21) is meshed with the left side of the third bevel gear (20), a second rotating shaft (22) is fixed at the upper end of the fourth bevel gear (21), and the upper end of the second rotating shaft (22) is connected with an output shaft of a rotating motor (23) in a screwed manner through a sealing bearing after penetrating through the sealing cover (3), and the rotating motor (23) is fixed on the sealing cover (3); the rotating motor (23) is connected with an external power supply;
the fixed plate (24), fixed plate (24) fix on the interior roof of sealed lid (3), first pivot (19) connect soon through the bearing and wear to establish on fixed plate (24), movable sleeve is equipped with spacing frame (25) on fixed plate (24), is fixed with connecting rod (26) on the right side wall of spacing frame (25), the other end and the internal thread pipe (15) of connecting rod (26) are fixed.
2. The concentrating device for extracting flavonoids according to claim 1, wherein: the upper end welding of clamp plate (11) is fixed with pull rod (12), and the upper end integrated into one piece of pull rod (12) has pull ring (13).
3. The concentrating device for extracting flavonoids according to claim 1, wherein: the blocking block (14) is of a conical structure.
4. The concentrating device for extracting flavonoids according to claim 1, wherein: the water tank (27) is arranged on the right side of the collecting bottle (5), and the upper end of the left side of the annular wall of the water tank (27) is fixed with the vacuum pump (7) through a bracket; the air outlet end of the vacuum pump (7) is connected with a third air duct (28), the third air duct (28) is connected with a hose (29), the other end of the hose (29) is connected with a fourth air duct (30), and the fourth air duct (30) is arranged in the water tank (27) in an extending mode.
5. The concentrating device for extracting flavonoids according to claim 1, wherein: drain pipe (31) are connected with the left side of retort (2) bottom through-connection, and solenoid valve is built-in to drain pipe (31), and drain pipe (31) are from right to left and are from high to low setting, and drain pipe (31) wears to establish on the rampart of basin (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321264945.5U CN220125537U (en) | 2023-05-24 | 2023-05-24 | A enrichment facility for extracting flavonoid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321264945.5U CN220125537U (en) | 2023-05-24 | 2023-05-24 | A enrichment facility for extracting flavonoid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220125537U true CN220125537U (en) | 2023-12-05 |
Family
ID=88956664
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321264945.5U Active CN220125537U (en) | 2023-05-24 | 2023-05-24 | A enrichment facility for extracting flavonoid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220125537U (en) |
-
2023
- 2023-05-24 CN CN202321264945.5U patent/CN220125537U/en active Active
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