CN220079150U - Vacuum distillation classifying condenser - Google Patents
Vacuum distillation classifying condenser Download PDFInfo
- Publication number
- CN220079150U CN220079150U CN202321655521.1U CN202321655521U CN220079150U CN 220079150 U CN220079150 U CN 220079150U CN 202321655521 U CN202321655521 U CN 202321655521U CN 220079150 U CN220079150 U CN 220079150U
- Authority
- CN
- China
- Prior art keywords
- temperature control
- condensing chamber
- chamber
- furnace body
- side heating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000005292 vacuum distillation Methods 0.000 title claims abstract description 19
- 238000009833 condensation Methods 0.000 claims abstract description 32
- 230000005494 condensation Effects 0.000 claims abstract description 32
- 238000010438 heat treatment Methods 0.000 claims abstract description 30
- 229910052751 metal Inorganic materials 0.000 claims abstract description 20
- 239000002184 metal Substances 0.000 claims abstract description 20
- 238000001704 evaporation Methods 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 6
- 230000008020 evaporation Effects 0.000 claims abstract description 4
- 238000000926 separation method Methods 0.000 abstract description 8
- 238000007664 blowing Methods 0.000 abstract description 2
- 150000002739 metals Chemical class 0.000 description 7
- 238000009835 boiling Methods 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 229910001297 Zn alloy Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a vacuum distillation classifying condenser, which comprises: the device comprises a furnace body, a temperature control condensing chamber, a plurality of layers of multistage condensing chambers, a side heating module and a furnace cover, wherein the temperature control condensing chamber is arranged at the bottom of the furnace body and is communicated with an evaporating chamber; the side heating module is arranged in the temperature control condensing chamber and fixed on the side wall of the furnace body, and is used for preserving heat of the temperature control condensing chamber and performing secondary evaporation on metal liquid in the temperature control condensing chamber; the multistage condensing chambers are detachably arranged above the temperature control condensing chambers, the multistage condensing chambers of the layers are arranged in the vertical direction, and the furnace cover is detachably arranged at the top of the furnace body; this vacuum distillation fractional condenser adopts the mode of side heating to leave the headspace for need not to take out the heat-generating body when blowing out, can realize work such as ejection of compact, can effectively improve work efficiency, and, adopt the multistage condensation chamber structure of a plurality of layers of vertical distribution, can realize the separation collection of multiple metal.
Description
Technical Field
The utility model relates to the technical field of metallurgical equipment, in particular to a vacuum distillation classifying condenser. Carrying out
Background
The vacuum distillation furnace condenser is mainly used for cooling and collecting metal vapor. In chinese patent CN216473410U, a vacuum distillation furnace for separating zinc from zinc alloy is disclosed, specifically a condensing chamber insulated by a top insulated graphite electrode is disclosed, but the condensing chamber has the following problems:
1. only can realize the separation of two metals, and can not realize the separation and collection of multiple metals;
2. the material can only be taken out of the discharge opening at the bottom in liquid form.
Disclosure of Invention
Aiming at the problems, the inventor provides a vacuum distillation fractional condenser, which adopts a side heating mode to leave a top space, so that the work such as discharging can be realized without taking out a heating body when the furnace is stopped, the working efficiency can be effectively improved, and in addition, the separation and collection of various metals can be realized by adopting a plurality of layers of multistage condensing chamber structures which are vertically distributed.
Specifically, the utility model is realized as follows:
a vacuum distillation staged condenser comprising:
a furnace body;
the temperature control condensing chamber is arranged at the bottom of the furnace body and is communicated with the evaporating chamber;
the side heating module is arranged in the temperature control layer condensation chamber and fixed on the side wall of the furnace body, and is used for preserving heat of the temperature control condensation chamber and performing secondary evaporation on metal liquid in the temperature control condensation chamber;
the multi-stage condensing chambers are arranged above the temperature control condensing chambers and are arranged in the vertical direction, and the multi-stage condensing chambers are detachably arranged on the furnace body; the multistage condensing chamber includes: the secondary condensation chambers, the tertiary condensation chambers, the quaternary condensation chambers and the like are arranged according to actual conditions.
The furnace cover is detachably arranged at the top of the furnace body.
Further, the side heating module includes:
the side heating body is arranged on the side wall of the temperature control condensing chamber;
the electrode penetrates into the temperature control condensing chamber from the outer side of the furnace body and is fixedly connected with the side heating body, so that the side heating body is hung in the temperature control condensing chamber.
Further, the side heating body is in a shape of a loop.
Further, the temperature control condensing chamber is connected with the multistage condensing chamber through a steam channel.
The working principle of the utility model is as follows:
after the metal gas volatilized in the evaporating chamber enters the temperature-control condensing chamber, the side heating body is used for preserving heat of the temperature-control condensing chamber, high-boiling point metal is condensed into liquid, low-boiling point metal solution keeps in a gaseous state, the upper multi-stage condensing chamber moves, the temperature of the temperature-control condensing chamber gradually decreases to the upper-stage condensing chamber, a temperature gradient is formed, and then metals with different boiling points are condensed and collected in condensing chambers of different levels, so that separation and collection of various metals are realized.
After the separation is completed, the furnace cover at the top is taken down, and then the metal collected inside can be taken out.
Compared with the prior art, the utility model has the beneficial effects that:
(1) This vacuum distillation fractional condenser adopts the mode of side heating, need not to take out the heat-generating body when blowing out, can realize work such as ejection of compact, can effectively improve work efficiency.
(2) The detachable top cover and the multistage condensing chamber design can effectively improve the efficiency of routine maintenance, and the ejection of compact and the clearance of solid material of also being convenient for.
(3) The multi-level condensation chamber structure can realize the separation and collection of various metals.
Drawings
FIG. 1 is a schematic diagram of a vacuum distillation stage condenser in example 1;
FIG. 2 is a schematic view showing the structure of a vacuum distillation classifying condenser in example 1;
FIG. 3 is an exploded view of the vacuum distillation stage condenser of example 1;
fig. 4 is a top view of the temperature controlled condensing chamber in example 1.
Reference numerals:
1-a furnace body; 11-airway; 12-furnace cover; 2-a temperature control condensing chamber; a 3-secondary condensing chamber; 41-electrode; 42-side heating element; 5-steam channel.
Detailed Description
The utility model will be described in further detail below with reference to the drawings by means of specific embodiments.
Example 1
As shown in fig. 1-4, the present embodiment provides a vacuum distillation classifying condenser comprising: furnace body 1, accuse temperature condensation chamber 2, side heating module that generates heat, a plurality of multistage condensation chamber and bell 12, wherein, accuse temperature condensation chamber 2 locates furnace body 1 bottom, and communicate with the evaporating chamber of vacuum distillation stove through air flue 11, multistage condensation chamber is layered structure and arranges in accuse temperature condensation chamber 2 top, and communicates with it through steam channel 5, the multistage condensation chamber of upper strata carries out second grade volatile condensation in proper order, tertiary volatile condensation, …, N level volatile condensation, and then collects the metal condensation of different boiling points in the condensation chamber of different grades, realizes the separation collection of multiple metal. The furnace cover 12 and the multi-stage condensation chambers are all detachably arranged so as to take out the metals collected in the condensation chambers of each stage.
For easy understanding, in this embodiment, the multistage condensation chamber is only provided with the secondary condensation chamber 3, metal vapor (primary volatile matter) evaporated from the evaporation chamber enters the temperature-controlled condensation chamber 2 through the air passage 11, the temperature-controlled condensation chamber 2 is insulated by the side heating module, and the metal liquid (obtained by condensing the primary volatile matter) in the temperature-controlled condensation chamber 2 is secondarily evaporated, and the secondary volatile matter goes upward and enters the secondary condensation chamber 3 to be condensed and collected.
Further, the side heating module includes: the side heating unit 42 and the electrode 41, wherein the electrode 41 penetrates into the temperature control condensation chamber 2 from the outer side of the furnace body 1 and is fixedly connected with the side heating unit 2, so that the side heating unit 42 is hung in the temperature control condensation chamber 2, and the side heating unit 41 is in a shape of a loop, so that the area of the side heating unit 41 is increased, and the heating effect of the side heating unit is improved.
The foregoing description of the utility model has been presented for purposes of illustration and description, and is not intended to be limiting. Several simple deductions, modifications or substitutions may also be made by a person skilled in the art to which the utility model pertains, based on the idea of the utility model.
Claims (4)
1. A vacuum distillation staged condenser comprising:
a furnace body (1);
the temperature control condensing chamber (2) is arranged at the bottom of the furnace body (1) and is communicated with the evaporating chamber;
the side heating module is arranged in the temperature control condensing chamber (2) and is fixed on the side wall of the furnace body (1) and used for preserving heat of the temperature control condensing chamber (2) and performing secondary evaporation on metal liquid in the temperature control condensing chamber (2);
the multi-stage condensation chambers are arranged above the temperature control condensation chambers (2) and are arranged in the vertical direction, and the multi-stage condensation chambers are detachably arranged on the furnace body (1);
the furnace cover (12) is detachably arranged at the top of the furnace body (1).
2. The vacuum distillation split condenser as claimed in claim 1, wherein the side heating heat generating module comprises:
a side heating body (42) arranged on the side wall of the temperature control condensing chamber (2);
the electrode (41) penetrates into the temperature control condensing chamber (2) from the outer side of the furnace body (1) and is fixedly connected with the side heating element (42), so that the side heating element (42) is hung in the temperature control condensing chamber (2) in a side mode.
3. The vacuum distillation classifying condenser according to claim 2, wherein said side heating element (42) has a loop shape.
4. Vacuum distillation stage condenser according to claim 1, characterized in that the temperature-controlled condensing chamber (2) is connected to the multistage condensing chamber by means of a steam channel (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321655521.1U CN220079150U (en) | 2023-06-27 | 2023-06-27 | Vacuum distillation classifying condenser |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321655521.1U CN220079150U (en) | 2023-06-27 | 2023-06-27 | Vacuum distillation classifying condenser |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220079150U true CN220079150U (en) | 2023-11-24 |
Family
ID=88816399
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321655521.1U Active CN220079150U (en) | 2023-06-27 | 2023-06-27 | Vacuum distillation classifying condenser |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220079150U (en) |
-
2023
- 2023-06-27 CN CN202321655521.1U patent/CN220079150U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105817461B (en) | A kind of device of waste and old circuit board electronic component high added value recycling | |
| CN205718530U (en) | A kind of fractional condensaion dish structure being applicable to vacuum distilling | |
| CN206103371U (en) | Spherical concentrator in vacuum | |
| CN220079150U (en) | Vacuum distillation classifying condenser | |
| EP1177026A2 (en) | Horizontal distillation apparatus and method | |
| CN102706144A (en) | Fractional condensation vacuum furnace | |
| CN203700465U (en) | Device for purifying metallic sodium | |
| US9540709B2 (en) | Vacuum refining furnace | |
| CN107723472A (en) | A kind of small intermittent-type reduction distillation device | |
| CN104694763B (en) | A kind of method that utilization molecular distillation equipment prepares high purity metal caesium | |
| US20070137997A1 (en) | Ethanol continuous flow boiler | |
| CN207062352U (en) | A kind of vacuum drying oven of two sections of distillations multi-stage condensing | |
| EP2698438A1 (en) | Tantalum-material multilevel distillation crucible and distillation process | |
| US2239371A (en) | Separation of metals by distillation | |
| CN204063931U (en) | A kind of condensing unit being applicable to intermittent vacuum stove | |
| JPH10244250A (en) | Non-boiling type distillation-purification device | |
| CN103801102B (en) | A kind of variable post of many gradients imitates rectifier unit | |
| KR0185587B1 (en) | Boiling liquefied gas | |
| WO1995024956A1 (en) | Distillation apparatus | |
| US4498959A (en) | Cooling attachment for solar distiller | |
| CN111041228A (en) | Method and equipment for integrated refining of crude zinc | |
| CN209270873U (en) | A kind of sensitive materials falling film evaporation device | |
| JP2008168183A (en) | Vapor-liquid separator and water producing device | |
| CN207210519U (en) | A kind of metallic lithium vacuum distillation purification device | |
| US2458253A (en) | Apparatus for metals distillation |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |