CN219972565U - Crystal treatment purification device - Google Patents

Abstract

The utility model belongs to the technical field of crystal preparation, in particular to a crystal treatment purification device, which comprises an outer shell, a pretreatment mechanism fixedly arranged in the outer shell, and a heat treatment mechanism fixedly arranged in the outer shell and positioned below the pretreatment mechanism, wherein a discharging mechanism is fixedly arranged on one side, close to the heat treatment mechanism, of the inner part of the outer shell, a discharging shell is fixedly arranged on the lower surface of the outer shell, a filter plate is arranged in the discharging shell, a pushing assembly is further arranged on the discharging shell, the pushing assembly comprises a shell cover arranged on the upper surface of the filter plate and a multistage pushing rod arranged outside the discharging shell, and by arranging the pushing assembly, crystals can be effectively controlled to be always contacted with the filter plate in the reciprocating movement process of the filter plate, so that the discharging speed of acetone solution is improved, the using effect of the device is improved, and the actual use requirement is met.

Description

Crystal treatment purification device

Technical Field

The utility model belongs to the technical field of crystal preparation, and particularly relates to a crystal treatment and purification device.

Background

The two-dimensional black phosphorus is considered as an all-purpose material gathering the excellent performance of the traditional two-dimensional material, and has the advantages of adjustable energy band structure, excellent electrical performance, anisotropic mechanical, thermodynamic and photoelectric properties, so that the two-dimensional black phosphorus has great research value in the fields of electrochemical energy storage, sensors, flexible electronics, photoelectric materials, ultra-light materials and the like, and is manufactured by a crystal treatment purification device;

through checking the public (bulletin) number; CN218596578U discloses a crystal treatment and purification device for black phosphorus crystal preparation, which is disclosed in the art as comprising a shell, wherein a pretreatment device is arranged in the shell near the top, and a heat treatment device is arranged below the pretreatment device; the pretreatment device body is a rotary cylinder body, and the side wall of the rotary cylinder body is provided with a blanking hole and other technical schemes, so that the risk that black phosphorus is corroded by acid liquor is avoided, the problem that alkali liquor and black phosphorus generate phosphine toxic gas is avoided, and the technical effects of green, safe and stable purification of black phosphorus are realized;

when the design is used, although the risk that black phosphorus is corroded by acid liquor is avoided, the problem that alkali liquor and black phosphorus generate phosphine toxic gas is avoided, and the purpose of purifying green, safe and stable black phosphorus is achieved;

in order to solve the above problems, the present utility model provides a crystal processing and purifying apparatus.

Disclosure of Invention

To solve the problems set forth in the background art. The utility model provides a crystal treatment and purification device which has the characteristics that a shell is covered in the reciprocating movement process of a filter plate, the crystal can be effectively controlled to be always contacted with the filter plate, the blocking of the filter plate by the crystal is reduced, and the liquid discharge speed of an acetone solution is improved, so that the use effect of the device is improved.

In order to achieve the above purpose, the present utility model provides the following technical solutions: the crystal treatment and purification device comprises an outer shell, a pretreatment mechanism fixedly installed in the outer shell, and a heat treatment mechanism fixedly installed in the outer shell and positioned below the pretreatment mechanism, wherein a discharge mechanism is fixedly installed on one side, close to the heat treatment mechanism, of the inner part of the outer shell, a discharge shell is fixedly arranged on the lower surface of the outer shell, a filter plate is arranged in the discharge shell, and a pushing component is further installed on the discharge shell;

the pushing assembly comprises a shell cover arranged on the upper surface of the filter plate, a multi-stage push rod arranged outside the discharging shell and a moving rod fixed at the output end of the multi-stage push rod, and a telescopic baffle is fixed between the discharging shell and the shell cover.

As a preferred crystal treatment and purification device, an L bracket is fixed on one side of the outer surface of the discharge shell close to the moving rod, the multi-stage push rod is fixed on the surface of the L bracket, one end of the moving rod, which is far away from the multi-stage push rod, is fixed on the surface of the shell cover, a sliding hole is formed in one side of the surface of the discharge shell close to the moving rod, and the moving rod is in sliding connection with the discharge shell through the sliding hole.

As a preferred mode of the crystal treatment and purification device, the lower surface of the shell cover is provided with a plurality of groups of exhaust holes, one side, close to the L bracket, of the surface of the discharge shell is fixedly provided with an air pump, the output end of the air pump is fixedly provided with a connecting pipe, one end, far away from the air pump, of the connecting pipe penetrates through the outer part of the discharge shell and extends to the inner part of the discharge shell and is fixedly connected with a telescopic pipe in the discharge shell, and one end, far away from the connecting pipe, of the telescopic pipe is fixedly arranged on the surface of the shell cover.

As a preferable mode of the crystal treatment purifying device, a chute is formed in one side, close to the filter plate, of the inner portion of the discharge shell, the filter plate is connected with the discharge shell in a sliding mode through the chute, a baffle plate is arranged on one side, close to the chute, of the surface of the discharge shell, two groups of fastening bolts which are symmetrically arranged are connected with the inner portion of the baffle plate in a threaded mode, and the baffle plate is connected with the discharge shell through the fastening bolts.

In one preferred embodiment of the crystal treatment and purification device of the present utility model, a sealing gasket is bonded to a side of the surface of the baffle plate, which is close to the discharge casing.

The crystal treatment purifying device is characterized by further comprising a drawing component arranged on one side of the outer shell, wherein the drawing component comprises a liquid storage tank and a water suction pump, the liquid storage tank is fixed on one side of the outer shell, which is close to the heat treatment mechanism, and the water suction pump is fixed on the upper surface of the liquid storage tank, a conveying pipe is fixed at the input end of the water suction pump, the output end of the water suction pump is fixed on the upper surface of the liquid storage tank through the input pipe, and the liquid storage tank is fixedly connected with the outer shell through a liquid discharge pipe.

In the crystal treatment and purification device, preferably, one end of the conveying pipe far away from the water suction pump is fixed on the surface of the discharge shell, and an inclined block is fixed on one side, close to the conveying pipe, inside the discharge shell.

Compared with the prior art, the utility model has the beneficial effects that:

through having set up the pushing components, when the casing cover is at filter reciprocating motion in-process, can effectually control crystal contact always with the filter, reduce the crystal and block the filter, improved acetone solution flowing back speed, thereby improve the result of use of device, satisfy the in-service use demand, and added extraction subassembly on this mechanism, automatically, draw in the liquid reserve tank to the acetone solution of exhaust inside, cyclic utilization of being convenient for need not personnel simultaneously to collect the acetone solution of exhaust, alleviate staff's intensity of labour.

Drawings

The accompanying drawings are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate the utility model and together with the embodiments of the utility model, serve to explain the utility model. In the drawings:

FIG. 1 is a schematic view of the overall structure of the present utility model;

fig. 2 is a structural sectional view of the outer case 1 in the present utility model;

FIG. 3 is an enlarged view of the structure A of FIG. 2 in accordance with the present utility model;

FIG. 4 is a cross-sectional view of the discharge casing of the present utility model;

FIG. 5 is a schematic view of the structure of the connecting parts such as the housing cover and the telescopic tube in the utility model;

in the figure:

1. an outer housing; 2. a pretreatment mechanism; 3. a heat treatment mechanism; 4. a discharging mechanism; 5. a discharge housing; 6. a filter plate;

7. a pushing component; 71. an L bracket; 72. a housing cover; 73. an exhaust hole; 74. a telescopic baffle; 75. a telescopic tube; 76. a moving rod; 77. a multi-stage push rod; 78. an air pump; 79. a connecting pipe; 711. a baffle plate; 712. a fastening bolt; 713. a chute; 714. a sealing gasket;

8. an extraction assembly; 81. a liquid storage tank; 82. a water pump; 83. a delivery tube; 84. and (5) tilting the block.

Detailed Description

The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.

Example 1

As shown in fig. 1:

the utility model provides a crystal treatment purification device, includes shell body 1 and fixed mounting at the inside pretreatment mechanism 2 of shell body 1 and fixed mounting at the inside heat treatment mechanism 3 that is located pretreatment mechanism 2 below of shell body 1, and shell body 1 is inside to be close to heat treatment mechanism 3 one side fixed mounting has discharge mechanism 4, and shell body 1 lower surface is fixed with, and discharge casing 5 is inside to be provided with filter 6.

In this embodiment: existing device { public (announcement) number }: CN218596578U discloses a crystal treatment and purification device for black phosphorus crystals after preparation, in which a shell, a pretreatment device and a heat treatment device proposed in the present document are disclosed, and an outer shell 1, a pretreatment mechanism 2 and a heat treatment mechanism 3 in the present document adopt the same technical means in the prior art, which are not described in detail herein, and the present subject utility model is further improved, and the details refer to the following disclosure technology; in order to solve the technical problem in the prior art, as disclosed in the background art, although the design avoids the risk that black phosphorus is corroded by acid liquor, and simultaneously avoids the problem that alkali liquor and black phosphorus generate phosphine toxic gas, the utility model realizes the green safe and stable black phosphorus purification purpose, but when the acetone solution is discharged, as crystals are always positioned above the material blocking inclined net, the material blocking inclined net is blocked by the crystals, the acetone solution discharging speed is reduced, thereby reducing the using effect of the device, the problem is obviously a problem which exists in reality and is difficult to solve in combination with the use, and therefore, in order to solve the technical problem, the utility model adds the pushing component 7 and the extracting component 8 on the file, and the power equipment involved in the product is powered by an external power supply.

Further, the method comprises the following steps:

as shown in fig. 1-5:

the pushing assembly 7 is further mounted on the discharging shell 5, the pushing assembly 7 comprises a shell cover 72 arranged on the upper surface of the filter plate 6, a multi-stage push rod 77 arranged outside the discharging shell 5 and a moving rod 76 fixed at the output end of the multi-stage push rod 77, and a telescopic baffle 74 is fixed between the discharging shell 5 and the shell cover 72.

In this embodiment: when the crystal treatment purifying device is used, firstly, crystal materials enter the pretreatment mechanism 2 through a feed inlet (not shown in the figure), inert gas is filled into the pretreatment mechanism 2 through an air inlet (not shown in the figure), the crystal materials are ball-milled through the pretreatment mechanism 2 in the inert gas process to obtain the smoothness of the crystal surfaces, then the crystal materials are discharged to the heat treatment mechanism 3 for heat treatment, after the heat treatment is finished, a crystal material disc is discharged to the bottom of the outer shell 1 through the discharge mechanism 4, then acetone solution (not shown in the figure) is discharged through a discharge pipe (not shown in the figure) to soak the crystal materials, after the soaking is finished, when the acetone solution is required to be discharged, a multistage push rod 77 is started firstly, then a moving rod 76 is driven to move, a shell cover 72 is driven to move on a filter plate 6 through the moving rod 76, the shell cover 72 is driven to stretch or shrink, a plurality of groups of liquid permeation holes (not shown in the figure) are formed in the surface of the telescopic baffle 74, and meanwhile, the acetone solution can be discharged from the liquid permeation holes through the shell cover 6, the filter plate 6 can be effectively controlled to be always in contact with the filter plate 6, and the actual contact speed of the filter plate is improved, and the contact speed of the crystal is effectively improved.

It should be noted that: the discharging mechanism 4 is composed of an electric push rod (not shown in the figure) and an L-shaped baffle plate (not shown in the figure), and the electric push rod drives the L-shaped baffle plate to move so as to perform material blocking or discharging operation on the crystal material.

It should be noted that: the shell cover 72 is of a triangular structure design, when the shell cover 72 moves, the crystal material extruded along with the crystal material moves upwards through the inclined surface of the shell cover 72, so that the crystal is separated from the filter plate 6, the blocking of the crystal to the filter plate 6 is reduced, and the liquid draining speed of the acetone solution is improved.

It should be noted that: the telescopic baffle plate 74 is fixed on one side of the shell cover 72 opposite to the inclined surface, the telescopic baffle plate 74 is formed by combining small-to-large butting shells, the telescopic baffle plate 74 can be stretched or stretched, a plurality of groups of liquid seepage holes are formed in the surface of the telescopic baffle plate 74, and along with the stretching or shrinking movement of the telescopic baffle plate 74, the liquid seepage holes on the telescopic baffle plate 74 are staggered with crystals, so that acetone solution is conveniently discharged.

In an alternative embodiment, an L bracket 71 is fixed to the outer surface of the discharge casing 5 near the side of the moving rod 76, the multi-stage push rod 77 is fixed to the surface of the L bracket 71, one end of the moving rod 76 far from the multi-stage push rod 77 is fixed to the surface of the casing cover 72, a sliding hole is formed in the surface of the discharge casing 5 near the side of the moving rod 76, and the moving rod 76 and the discharge casing 5 are slidably connected through the sliding hole.

In this embodiment: the multi-stage push rod 77 is fixed through the L bracket 71, and the multi-stage push rod 77 further drives the moving rod 76 to perform telescopic movement, so that the moving rod 76 slides in a sliding hole formed in the discharging shell 5.

In an alternative embodiment, the lower surface of the housing cover 72 is provided with a plurality of groups of exhaust holes 73, one side of the surface of the discharge housing 5, which is close to the L bracket 71, is fixed with an air pump 78, the output end of the air pump 78 is fixed with a connecting pipe 79, one end, away from the air pump 78, of the connecting pipe 79 penetrates through the outside of the discharge housing 5 and extends to the inside of the discharge housing 5, and is fixedly connected with a telescopic pipe 75 in the discharge housing 5, and one end, away from the connecting pipe 79, of the telescopic pipe 75 is fixed on the surface of the housing cover 72.

In this embodiment: the air generated by starting the air pump 78 is discharged into the telescopic pipe 75 through the connecting pipe 79, is discharged into the shell cover 72 through the telescopic pipe 75, is discharged through the exhaust hole 73 on the shell cover 72, and is discharged with larger air flow, the generated impact force washes away the residue remained on a part of the surface in the filtering hole of the filtering plate 6, so that the discharging speed of the acetone solution is improved.

In an alternative embodiment, a chute 713 is formed in one side, close to the filter plate 6, of the interior of the discharge casing 5, the filter plate 6 is slidably connected with the discharge casing 5 through the chute 713, a baffle plate 711 is arranged on one side, close to the chute 713, of the surface of the discharge casing 5, two groups of fastening bolts 712 are in symmetrical arrangement in threaded connection with the baffle plate 711, the baffle plate 711 is connected with the discharge casing 5 through the fastening bolts 712, and a sealing gasket 714 is bonded on one side, close to the discharge casing 5, of the surface of the baffle plate 711.

In this embodiment: because the filter plate 6 is soaked by the acetone solution for a long time, when the filter plate 6 needs to be replaced due to corrosion, the fastening bolt 712 is rotated at first, the fastening bolt 712 is screwed out of the discharge shell 5, then the baffle plate 711 is taken down, the filter plate 6 is pulled, and the filter plate 6 slides in the chute 713 formed in the discharge shell 5, so that the filter plate 6 is taken out of the discharge shell 5, the filter plate 6 is convenient to replace, the practicability of the device is improved, the sealing performance between the baffle plate 711 and the discharge shell 5 is increased through the sealing gasket 714, and the leakage of liquid from the chute 713 is avoided.

Further, the method comprises the steps of;

this crystal processing purification device still includes the extraction subassembly 8 of installing in shell body 1 one side, extraction subassembly 8 is including fixing the liquid reserve tank 81 that is close to heat treatment mechanism 3 one side at shell body 1 surface and fixing the suction pump 82 at liquid reserve tank 81 upper surface, the input of suction pump 82 is fixed with conveyer pipe 83, the output of suction pump 82 passes through the input and fixes the upper surface at liquid reserve tank 81, pass through fluid-discharge tube fixed connection between liquid reserve tank 81 and the shell body 1, the one end that suction pump 82 was kept away from to conveyer pipe 83 is fixed in the surface of row's material casing 5, the one side that row's material casing 5 is inside to be close to conveyer pipe 83 is fixed with sloping block 84.

In this embodiment: when the acetone solution is discharged through the filter plate 6, the water suction pump 82 is started subsequently, and then the discharged acetone solution is pumped out through the conveying pipe 83 and discharged into the liquid storage tank 81, in the process, the inclined block 84 is of an inclined structure, so that discharged liquid can be gathered at the conveying pipe 83, the acetone solution can be conveniently pumped out, when the acetone solution is required to be discharged, the acetone solution is discharged into the outer shell 1 through the liquid discharge pipe of the liquid storage tank 81, the discharged acetone solution is automatically pumped into the liquid storage tank 81 through the operation, the cyclic utilization is facilitated, meanwhile, people are not required to collect the discharged acetone solution, and the labor intensity of workers is relieved.

It should be noted that: the lower surface of the discharging shell 5 is designed into a plugging structure.

It should be understood that: the input pipe between the water pump 82 and the liquid storage tank 81 is located at the bottom of the water pump 82, so that materials can be saved better.

The working principle and the using flow of the utility model are as follows: in use, the crystal processing purifying device firstly enters the pretreatment mechanism 2 through a feed port (not shown), inert gas is filled through an air inlet (not shown), the crystal material is ball-milled through the pretreatment mechanism 2 in the process of inert gas to obtain the smoothness of the crystal surface, then is discharged into the heat treatment mechanism 3 for heat treatment, after the heat treatment is finished, the crystal material disc is discharged to the bottom of the outer shell 1 through the discharge mechanism 4, then is discharged into acetone solution (not shown) through a discharge pipe (not shown) to soak the crystal material, after the soaking is finished, when the acetone solution is required to be discharged, the multistage push rod 77 is started firstly, the moving rod 76 is driven to move, the moving rod 76 slides in the sliding hole formed in the discharging shell 5 and drives the shell cover 72 to move on the filter plate 6, the shell cover 72 is driven to extend or retract in the moving process, a plurality of groups of seepage holes (not shown in the figure) are formed on the surface of the telescopic baffle 74, acetone solution is discharged from the seepage holes at the same time, crystals can be effectively controlled to always contact with the filter plate 6 in the reciprocating process of the filter plate 6 through the shell cover 72, the blocking of the crystals on the filter plate 6 is reduced, the liquid discharging speed of the acetone solution is improved, the using effect of the device is improved, the actual using requirement is met, meanwhile, gas generated by the air pump 78 is started to be discharged into the telescopic pipe 75 through the connecting pipe 79, discharged into the shell cover 72 through the telescopic pipe 75, and discharged larger airflow is discharged through the exhaust hole 73 on the shell cover 72, the impact force that produces washes the broken slag that a part of filter 6 filter downthehole surface was remained, the improvement acetone solution discharge rate, because filter 6 is soaked by the acetone solution for a long time, when needs change because of corroding, at first rotate fastening bolt 712, make fastening bolt 712 follow discharge casing 5 in unscrew, later take off baffle 711, pull filter 6, make filter 6 slide in spout 713 that discharge casing 5 offered, thereby take out filter 6 follow discharge casing 5 in, be convenient for make filter 6 change, the practicality of device has been improved, when the acetone solution is discharged through filter 6, later start suction pump 82, and then take out the acetone solution of discharge through conveyer pipe 83, and discharge the liquid storage box 81 is inside, in this process, tilting block 84 is the slope structure, can make the liquid collection of discharge in conveyer pipe 83 department, be convenient for take out the acetone solution, when needs to discharge the acetone solution, through the drain pipe of liquid storage box 81 is discharged to shell 1 inside, through this operation, automatic suction to the liquid storage box 81 is convenient for use for circulate and take out the acetone solution, the intensity of collecting the people who discharges acetone solution, the intensity of workers is convenient for the recycling.

Finally, it should be noted that: the foregoing description is only a preferred embodiment of the present utility model, and the present utility model is not limited thereto, but it is to be understood that modifications and equivalents of some of the technical features described in the foregoing embodiments may be made by those skilled in the art, although the present utility model has been described in detail with reference to the foregoing embodiments. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present utility model should be included in the protection scope of the present utility model.

Claims (7)

1. The utility model provides a crystal treatment purification device, includes shell body (1) and fixed mounting be in pretreatment mechanism (2) and fixed mounting inside shell body (1) are in the inside heat treatment mechanism (3) that are located pretreatment mechanism (2) below of shell body (1), the inside being close to of shell body (1) discharge mechanism (4) are installed to heat treatment mechanism (3) one side fixed mounting, surface mounting has discharge casing (5) under shell body (1), discharge casing (5) are inside to be provided with filter (6), its characterized in that: a pushing component (7) is also arranged on the discharging shell (5);

the pushing assembly (7) comprises a shell cover (72) arranged on the upper surface of the filter plate (6), a multi-stage push rod (77) arranged outside the discharging shell (5) and a moving rod (76) fixed at the output end of the multi-stage push rod (77), and a telescopic baffle plate (74) is fixed between the discharging shell (5) and the shell cover (72).

2. The crystal processing purifying apparatus according to claim 1, wherein: the utility model discloses a material discharging shell, including material discharging shell (5), movable rod (76), multistage push rod (77), shell cover (72) and slide hole, material discharging shell (5) surface is close to movable rod (76) one side is fixed with L support (71), multistage push rod (77) are fixed the surface of L support (71), movable rod (76) are kept away from the one end of multistage push rod (77) is fixed the surface of shell cover (72), the slide hole has been seted up on the surface of material discharging shell (5) near movable rod (76) one side, movable rod (76) with material discharging shell (5) are through this slide hole sliding connection.

3. The crystal processing purifying apparatus according to claim 2, wherein: the lower surface of casing cover (72) has seted up a plurality of exhaust hole (73), the surface of arranging material casing (5) is close to one side of L support (71) is fixed with air pump (78), the output of air pump (78) is fixed with connecting pipe (79), connecting pipe (79) are kept away from the one end of air pump (78) runs through arrange material casing (5) outside, and extend to arrange material casing (5) inside, and with the flexible pipe (75) fixed connection of arranging material casing (5) inside, flexible pipe (75) are kept away from the one end of connecting pipe (79) is fixed the surface of casing cover (72).

4. A crystal processing purifying apparatus according to claim 3, wherein: the utility model discloses a filter, including row material casing (5), filter, baffle plate (711), baffle plate (712) are provided with in row material casing (5) inside one side that is close to filter (6) has seted up spout (713), filter (6) with row material casing (5) are passed through spout (713) sliding connection, row material casing (5) surface is close to spout (713) one side is provided with baffle plate (711), baffle plate (711) inside threaded connection has two sets of fastening bolt (712) that are symmetrical arrangement, baffle plate (711) with row material casing (5) are passed through fastening bolt (712) are connected.

5. The crystal processing purifying apparatus according to claim 4, wherein: a sealing gasket (714) is adhered to one side, close to the discharging shell (5), of the surface of the baffle plate (711).

6. The crystal processing purifying apparatus according to claim 5, wherein: still including installing extraction subassembly (8) of shell body (1) one side, extraction subassembly (8) are including fixing shell body (1) surface is close to liquid reserve tank (81) of heat treatment mechanism (3) one side and fix suction pump (82) of liquid reserve tank (81) upper surface, the input of suction pump (82) is fixed with conveyer pipe (83), the output of suction pump (82) is fixed at the upper surface of liquid reserve tank (81) through the input pipe, liquid reserve tank (81) with pass through fluid-discharge tube fixed connection between shell body (1).

7. The crystal processing purifying apparatus according to claim 6, wherein: one end of the conveying pipe (83) far away from the water suction pump (82) is fixed on the surface of the discharging shell (5), and an inclined block (84) is fixed on one side, close to the conveying pipe (83), of the inside of the discharging shell (5).