CN219964195U - Liquid phase suction filtration equipment for recrystallization - Google Patents

Liquid phase suction filtration equipment for recrystallization Download PDF

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Publication number
CN219964195U
CN219964195U CN202321188994.5U CN202321188994U CN219964195U CN 219964195 U CN219964195 U CN 219964195U CN 202321188994 U CN202321188994 U CN 202321188994U CN 219964195 U CN219964195 U CN 219964195U
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suction filtration
pipe
liquid phase
storage tank
crystallization tank
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CN202321188994.5U
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单中喜
单筱惠
李海霞
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Pingyu Yimeikang Plant Technology Co ltd
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Pingyu Yimeikang Plant Technology Co ltd
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Abstract

The utility model discloses liquid phase suction filtration equipment for recrystallization, and relates to the technical field of quercetin recrystallization processing. The utility model comprises a crystallization tank, a liquid phase storage tank, a suction filtration pipe, an air extractor and a cooling component, wherein the crystallization tank and the liquid phase storage tank are arranged side by side, one end of the suction filtration pipe is communicated and fixed on the upper end face of the liquid phase storage tank, a suction filtration plate is fixed on the periphery of the end part of the suction filtration pipe positioned in the crystallization tank, a bucket-shaped filter screen frame is fixed at the bottom of the suction filtration plate, the air extractor is fixed on the upper end face of the liquid phase storage tank, and the cooling component is arranged in the crystallization tank above the suction filtration plate; the cooling assembly comprises a water inlet pipe, a water outlet pipe and three spiral coils fixed between the water inlet pipe and the water outlet pipe. The utility model solves the problems that the efficiency of the conventional suction filtration mode is too low, the suction filtration area is too small, and the solution cannot be completely crystallized and separated out due to insufficient temperature, so that the waste of the suction filtered liquid phase is caused by the arrangement of the suction filtration pipe, the liquid phase storage tank, the air extractor, the crystallization tank and the cooling component.

Description

Liquid phase suction filtration equipment for recrystallization
Technical Field
The utility model belongs to the technical field of quercetin recrystallization processing, and particularly relates to liquid phase suction filtration equipment for recrystallization.
Background
Recrystallization is a process in which a substance is dissolved in a solvent or melted and then recrystallized from the solution or melt. Recrystallization may allow purification of impure materials or separation of materials mixed together from one another. The solid material can be purified by recrystallization. Some metals or alloys may be recrystallized to refine the grain or to alter the crystallization of the crystal, thereby altering its properties.
In the recrystallization process, the solubility of the solid mixture in the solvent is closely related to temperature. Generally at elevated temperatures, the solubility increases. When the solution is saturated in a hot solvent, the solubility decreases upon cooling, and the solution becomes supersaturated to precipitate crystals. The solvent has different solubilities for the purified substance and impurities, so that the purified substance can be separated out. And the impurities are fully or mostly remained in the solution (if the solubility in the solvent is extremely small, the solution is prepared into a saturated solution and then filtered and removed), thereby achieving the aim of purification.
In the processing of quercetin, recrystallization is an indispensable step, and in the course of recrystallization, the following steps are generally included: (1) selecting a suitable solvent to prepare a hot saturated solution; (2) removing insoluble impurities; (3) cooling, crystallizing, filtering and removing; and (4) washing and drying to remove attachments and solvents. The following disadvantages still exist in the suction filtration process:
1. in the traditional recrystallization process, the temperature is mostly adopted to precipitate crystals in the solution, the liquid phase in the solution is pumped out after the crystals are precipitated, in the liquid pumping process, the internal solution is pumped out but the crystals are not pumped out in the pumping mode, so that the quality of the finally precipitated crystals is ensured, but the conventional pumping mode is far less efficient and is easy to block a filtering part, so that the pumping efficiency is greatly reduced, and the pumping area is usually smaller;
2. the suction filtration is to extract liquid phase and filter, but in the recrystallization process, the solution in the crystallization tank can be separated out to a certain degree, and the crystallization is realized completely depending on the cooling of the crystallization tank, so the temperature of the solution in the middle of the crystallization tank can be insufficient, the crystals can not be completely separated out, the solution still contains the required substances, and waste is caused, so the suction filtration operation can be performed after the crystallization is fully cooled.
Disclosure of Invention
The utility model aims to provide liquid phase suction filtration equipment for recrystallization, which solves the problems that the efficiency of a conventional suction filtration mode is low, the suction filtration area is small, and solution temperature is insufficient and complete crystallization precipitation is not realized, so that the suction filtered liquid phase is wasted by arranging a suction filtration pipe, a liquid phase storage tank, an air extractor, a crystallization tank and a cooling assembly.
In order to solve the technical problems, the utility model is realized by the following technical scheme:
the utility model relates to liquid phase suction filtration equipment for recrystallization, which comprises a crystallization tank, a liquid phase storage tank, a suction filtration pipe, an air extractor and a cooling component, wherein the crystallization tank and the liquid phase storage tank are arranged side by side;
the crystallization tank stores a certain amount of solution for recrystallization, which is not identical to the crystallization tank on the market, the liquid phase storage tank stores the residual solution after crystallization for use, and the suction filtration pipe as a transfer is used for pumping the residual solution after crystallization from the crystallization tank and conveying the residual solution to the liquid phase storage tank for storage; when the suction filtration pipe works, the bucket-shaped filter screen frame at the bottom of the suction filtration pipe can filter the crystallized solution to a certain extent, so that crystals are prevented from being discharged through the suction filtration pipe, air in the liquid-phase storage tank is pumped out by matching with the air pump to form negative pressure until the negative pressure is conducted into the suction filtration pipe, and the solution is filtered and pumped out through one end of the suction filtration pipe positioned in the crystallization tank until the solution enters the liquid-phase storage tank to finish storage;
the cooling assembly comprises a water inlet pipe, a water outlet pipe and three spiral coils fixed between the water inlet pipe and the water outlet pipe; the setting of cooling module for still have the required material of uncrystallization with the solution in the crystallization jar in the solution, cooling crystallization with the solution cooling in middle part region, the inlet tube lets in the cooling water, discharges from the outlet pipe after three spiral coil, accomplishes once circulation, cools down the solution fast, so reciprocating can.
Further, an exhaust pipe is fixed at the exhaust end of the air extractor, the other end of the exhaust pipe penetrates through the upper end face of the liquid-phase storage tank and is communicated with the inside of the liquid-phase storage tank, and an exhaust pipe is fixed at the exhaust end of the air extractor;
the air pump works to pump out the air in the liquid phase storage tank through the air pumping pipe and discharge the air from the air exhaust pipe, so that negative pressure is formed in the liquid phase storage tank, and suction filtration is facilitated.
Further, a liquid discharge pipe with a valve is fixedly penetrated at the bottom of the liquid phase storage tank, and the volume of the liquid phase storage tank is smaller than that of the crystallization tank;
when the solution in the liquid phase storage tank needs to be discharged, the liquid discharge pipe can be opened to discharge liquid, and the liquid phase storage tank is used as the solution in the storage crystallization tank, so that the volume equal to that of the crystallization tank is not required to be ensured, and the solution in the crystallization tank is not necessarily in a full state.
Further, one end of the suction filtration pipe positioned in the crystallization tank penetrates through the suction filtration plate and stretches into the bucket-type filter screen frame, but the end part of the suction filtration pipe is not contacted with the inner bottom surface of the bucket-type filter screen frame; when the suction filtration pipe performs suction filtration, the bottom end of the suction filtration pipe can extract the solution filtered by the bucket-type filter screen frame.
Further, the inner diameter of the filter plate and the maximum inner diameter of the bucket-shaped filter screen frame are smaller than the inner diameter of the crystallization tank; the normal crystallization use in the crystallization tank can not be influenced, the larger suction filtration area is ensured, the suction filtration plate and the bucket-type filter screen frame are arranged, the suction filtration area is larger than that of the traditional suction filtration head structure, and the loss and pollution in the reagent transferring process are reduced by suction filtration.
Further, the three spiral coils are sleeved on the outer side of the suction filtration pipe in the crystallization tank, the water inlet ends of the three spiral coils are communicated and fixed with the peripheral side of the water inlet pipe, and the water outlet ends of the three spiral coils are communicated and fixed with the peripheral side of the water outlet pipe;
after the cooling water is input from the water inlet pipe, the cooling water is led out from the water outlet pipe after passing through the three spiral coils, when passing through the three spiral coils, the cooling water can take away the heat of the solution in the crystallization tank, so that the cooling water can be rapidly cooled, crystallized and cooled, the spiral coils are designed to ensure that the cooling water is reserved in the solution for a longer time, the sufficient heat is taken away, and the cooling assembly can be used for circularly inputting the cooling water.
Further, the lowest end of the bucket-shaped filter screen frame is not contacted with the inner bottom surface of the crystallization tank; the crystallization effect is not affected.
The utility model has the following beneficial effects:
1. the utility model solves the problems of low efficiency and small suction filtration area of the conventional suction filtration mode by arranging the suction filtration pipe, the liquid phase storage tank and the air extractor; the suction filter plate and the bucket type filter screen frame are arranged, the suction filter area is larger than that of a traditional suction filter head structure, the maximum inner diameter of the suction filter plate and the bucket type filter screen frame is only slightly smaller than that of a crystallization tank, the suction filter plate and the bucket type filter screen frame are arranged at the lower part of an inner cavity of the crystallization tank, the suction filter plate and the bucket type filter screen frame can be fully contacted with solution, the solution is filtered and extracted in a large area, the filtering position is not blocked, and the rapid and efficient suction filtration processing is guaranteed.
2. The crystallization tank and the cooling assembly are arranged, so that the problem that the solution cannot be completely crystallized and separated out due to insufficient temperature, and the waste of the pumped and filtered liquid phase is solved; the cooling assembly is used for further separating out crystals of the solution in the crystallization tank, the fact that the uncrystallized required substances still exist in the solution is avoided, the solution in the middle area is cooled and crystallized, the water inlet pipe is filled with cooling water, the cooling water is discharged from the water outlet pipe after passing through the three spiral coils, one-time circulation is completed, the solution is cooled rapidly, and the fact that the uncrystallized substances in the solution are pumped away during suction filtration is avoided.
Drawings
FIG. 1 is a perspective view showing the structure of a liquid phase suction filtration apparatus for recrystallization;
FIG. 2 is a cross-sectional view;
FIG. 3 is a block diagram of a cooling module and a suction filter tube;
FIG. 4 is a semi-sectional view of a suction filter plate and a bucket screen frame;
fig. 5 is a block diagram of a cooling assembly.
Reference numerals:
1. a crystallization tank; 2. a liquid phase storage tank; 201. a liquid discharge pipe; 3. a suction filtration tube; 301. a filter plate is pumped; 302. a bucket-type filter screen frame; 4. an air extractor; 401. an exhaust pipe; 402. an exhaust pipe; 5. a cooling assembly; 501. a water inlet pipe; 502. a water outlet pipe; 503. spiral coil.
Detailed Description
The technical solutions in the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model.
Referring to fig. 1-5, the utility model discloses liquid phase suction filtration equipment for recrystallization, which comprises a crystallization tank 1, a liquid phase storage tank 2, a suction filtration pipe 3, an air extractor 4 and a cooling component 5, wherein the crystallization tank 1 and the liquid phase storage tank 2 are arranged side by side, one end of the suction filtration pipe 3 is penetrated and fixed on the upper end face of the liquid phase storage tank 2, the other end of the suction filtration pipe 3 stretches into the lower part of an inner cavity of the crystallization tank 1, a suction filtration plate 301 is fixed on the peripheral side of the end part of the suction filtration pipe 3 positioned in the crystallization tank 1, a bucket type filter screen frame 302 is fixed at the bottom of the suction filtration plate 301, the air extractor 4 is fixed on the upper end face of the liquid phase storage tank 2, and the cooling component 5 is arranged in the crystallization tank 1 above the suction filtration plate 301;
the crystallization tank 1 stores a certain solution for recrystallization of quercetin, which is identical to the crystallization tank 1 on the market, the liquid phase storage tank 2 stores the residual solution after crystallization for use, and the suction filtration pipe 3 as a transit pumps the residual solution after crystallization out of the crystallization tank 1 and conveys the residual solution into the liquid phase storage tank 2 for storage; when the suction filtration tube 3 works, the bucket-shaped filter screen frame 302 at the bottom of the suction filtration tube 3 can filter the crystallized solution to a certain extent, so that crystals of the crystallized solution are prevented from being discharged through the suction filtration tube 3, air in the liquid-phase storage tank 2 is pumped out by matching with the air pump 4 to form negative pressure until the negative pressure is conducted into the suction filtration tube 3, and the solution is filtered and pumped out through one end of the suction filtration tube 3 positioned in the crystallization tank 1 until the solution enters the liquid-phase storage tank 2 to finish storage;
the cooling module 5 comprises a water inlet pipe 501, a water outlet pipe 502 and three spiral coils 503 fixed between the water inlet pipe 501 and the water outlet pipe 502;
the cooling component 5 is used for further separating out and crystallizing the solution in the crystallization tank 1, avoiding the existence of uncrystallized required substances in the solution, cooling and crystallizing the solution in the middle area, introducing cooling water into the water inlet pipe 501, discharging the solution from the water outlet pipe 502 after passing through the three spiral coils 503, completing one-time circulation, rapidly cooling the solution, and so on.
As shown in fig. 1-2, an exhaust pipe 402 is fixed at the exhaust end of the air extractor 4, and the other end of the exhaust pipe 402 penetrates through the upper end surface of the liquid phase storage tank 2 and is communicated with the interior of the liquid phase storage tank 2, and an exhaust pipe 401 is fixed at the exhaust end of the air extractor 4; the air pump 4 works to pump the air in the liquid-phase storage tank 2 through the air pumping pipe 402 and discharge the air from the air exhaust pipe 401, so that negative pressure is formed in the liquid-phase storage tank 2, and suction filtration is facilitated;
the bottom of the liquid phase storage tank 2 is fixedly penetrated by a liquid discharge pipe 201 with a valve, and the volume of the liquid phase storage tank 2 is smaller than that of the crystallization tank 1;
when the solution in the liquid-phase tank 2 needs to be discharged, the liquid discharge pipe 201 can be opened to discharge the liquid, and the liquid-phase tank 2 is used as the solution in the storage crystallization tank 1, and the volume equivalent to that of the crystallization tank 1 does not need to be ensured, because the solution in the crystallization tank 1 is not necessarily in a full state.
1-4, one end of the suction filtration pipe 3 positioned in the crystallization tank 1 penetrates through the suction filtration plate 301 and stretches into the bucket type filter screen frame 302, but the end of the suction filtration pipe 3 is not contacted with the inner bottom surface of the bucket type filter screen frame 302; when the suction filtration tube 3 performs suction filtration, the bottom end of the suction filtration tube 3 extracts the solution filtered by the bucket-type filter screen frame 302;
the inner diameter of the filter plate 301 and the maximum inner diameter of the bucket-shaped filter screen frame 302 are smaller than the inner diameter of the crystallization tank 1; the normal crystallization use in the crystallization tank 1 is not affected, a larger suction filtration area is ensured, the suction filtration area of the suction filtration plate 301 and the bucket-type filter screen frame 302 is larger than that of the conventional suction filtration head structure, and the suction filtration reduces the loss and pollution in the reagent transferring process;
the lowest end of the bucket-shaped filter screen frame 302 is not contacted with the inner bottom surface of the crystallization tank 1; so that it does not affect the crystallization effect.
As shown in fig. 5, three spiral coils 503 are all sleeved outside the suction filtration tube 3 in the crystallization tank 1, the water inlet ends of the three spiral coils 503 are all communicated and fixed with the periphery of the water inlet tube 501, and the water outlet ends of the three spiral coils 503 are all communicated and fixed with the periphery of the water outlet tube 502; cooling water is input from the water inlet pipe 501, after being input, the cooling water is led out from the water outlet pipe 502 after passing through the three spiral coils 503, when passing through the three spiral coils 503, the cooling water can take away the heat of the solution in the crystallization tank 1, so that the cooling water can be rapidly cooled, crystallized and cooled, the design of the spiral coils 503 ensures that the cooling water stays in the solution for a longer time, the sufficient heat is taken away, and the cooling assembly 5 can circularly input the cooling water for use.
The specific working principle of the utility model is as follows: the crystallization tank 1 is internally provided with a certain solution for recrystallization of quercetin, then cooling water is input from a water inlet pipe 501, after the cooling water is input, the cooling water is led out from a water outlet pipe 502 after the cooling water passes through three spiral coils 503, when the cooling water passes through the three spiral coils 503, the cooling water can take away the heat of the solution in the crystallization tank 1, so that the cooling crystallization tank is cooled and cooled rapidly, the solution in the middle area is cooled and crystallized, the extracted liquid phase is prevented from containing crystallizable substances, then the air extractor 4 works, the air in the liquid phase storage tank 2 is extracted through an extraction pipe 402, the air is discharged from an exhaust pipe 401, so that negative pressure is formed in the liquid phase storage tank 2, and thus, when the suction filtration pipe 3 performs suction filtration, the solution filtered by a bucket type filter screen frame 302 is extracted, the crystallized solution is prevented from being discharged through the suction filtration pipe 3 until the liquid phase storage tank 2 is completely stored.
The foregoing is only a preferred embodiment of the present utility model, and the present utility model is not limited thereto, and any modification, equivalent replacement, and improvement of some of the technical features described in the foregoing embodiments are all within the scope of the present utility model.

Claims (7)

1. The utility model provides a liquid phase suction filtration equipment for recrystallization, includes crystallizer (1), liquid phase storage tank (2), suction filtration pipe (3), air extractor (4) and cooling module (5), its characterized in that: the crystallization tank (1) and the liquid-phase storage tank (2) are arranged side by side, one end of the suction filtration pipe (3) is communicated and fixed on the upper end face of the liquid-phase storage tank (2), the other end of the suction filtration pipe (3) stretches into the lower part of the inner cavity of the crystallization tank (1), a suction filtration plate (301) is fixed on the peripheral side of the end part of the suction filtration pipe (3) in the crystallization tank (1), a bucket-type filter screen frame (302) is fixed at the bottom of the suction filtration plate (301), an air extractor (4) is fixed on the upper end face of the liquid-phase storage tank (2), and a cooling assembly (5) is arranged in the crystallization tank (1) above the suction filtration plate (301);
the cooling assembly (5) comprises a water inlet pipe (501), a water outlet pipe (502) and three spiral coils (503) fixed between the water inlet pipe (501) and the water outlet pipe (502).
2. The liquid phase suction filtration apparatus for recrystallization according to claim 1, wherein: the exhaust end of the air extractor (4) is fixedly provided with an exhaust pipe (402), the other end of the exhaust pipe (402) penetrates through the upper end face of the liquid-phase storage tank (2) and is communicated with the inside of the liquid-phase storage tank (2), and the exhaust end of the air extractor (4) is fixedly provided with an exhaust pipe (401).
3. The liquid phase suction filtration apparatus for recrystallization according to claim 1, wherein: the bottom of the liquid phase storage tank (2) is communicated and fixed with a liquid discharge pipe (201) with a valve, and the volume of the liquid phase storage tank (2) is smaller than that of the crystallization tank (1).
4. The liquid phase suction filtration apparatus for recrystallization according to claim 1, wherein: one end of the suction filtration pipe (3) positioned in the crystallization tank (1) penetrates through the suction filtration plate (301) and stretches into the bucket-type filter screen frame (302), but the end of the suction filtration pipe (3) is not contacted with the inner bottom surface of the bucket-type filter screen frame (302).
5. The liquid phase suction filtration apparatus for recrystallization according to claim 1, wherein: the inner diameter of the filter pumping plate (301) and the maximum inner diameter of the bucket-type filter screen frame (302) are smaller than the inner diameter of the crystallization tank (1).
6. The liquid phase suction filtration apparatus for recrystallization according to claim 1, wherein: the three spiral coils (503) are all sleeved outside the suction filtration pipe (3) in the crystallization tank (1), the water inlet ends of the three spiral coils (503) are all communicated and fixed with the periphery of the water inlet pipe (501), and the water outlet ends of the three spiral coils (503) are all communicated and fixed with the periphery of the water outlet pipe (502).
7. The liquid phase suction filtration apparatus for recrystallization according to claim 1, wherein: the lowest end of the bucket-shaped filter screen frame (302) is not contacted with the inner bottom surface of the crystallization tank (1).
CN202321188994.5U 2023-05-16 2023-05-16 Liquid phase suction filtration equipment for recrystallization Active CN219964195U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202321188994.5U CN219964195U (en) 2023-05-16 2023-05-16 Liquid phase suction filtration equipment for recrystallization

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202321188994.5U CN219964195U (en) 2023-05-16 2023-05-16 Liquid phase suction filtration equipment for recrystallization

Publications (1)

Publication Number Publication Date
CN219964195U true CN219964195U (en) 2023-11-07

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ID=88590341

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202321188994.5U Active CN219964195U (en) 2023-05-16 2023-05-16 Liquid phase suction filtration equipment for recrystallization

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CN (1) CN219964195U (en)

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