CN219922942U - Continuous reaction device for preparing phenyl trimethoxy silane - Google Patents
Continuous reaction device for preparing phenyl trimethoxy silane Download PDFInfo
- Publication number
- CN219922942U CN219922942U CN202321068845.5U CN202321068845U CN219922942U CN 219922942 U CN219922942 U CN 219922942U CN 202321068845 U CN202321068845 U CN 202321068845U CN 219922942 U CN219922942 U CN 219922942U
- Authority
- CN
- China
- Prior art keywords
- trimethoxy silane
- driving motor
- phenyl trimethoxy
- reaction chamber
- continuous reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 76
- ZNOCGWVLWPVKAO-UHFFFAOYSA-N trimethoxy(phenyl)silane Chemical compound CO[Si](OC)(OC)C1=CC=CC=C1 ZNOCGWVLWPVKAO-UHFFFAOYSA-N 0.000 title claims abstract description 60
- 238000002360 preparation method Methods 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 238000007790 scraping Methods 0.000 claims description 21
- 239000002994 raw material Substances 0.000 abstract description 26
- 238000000034 method Methods 0.000 abstract description 5
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 150000003961 organosilicon compounds Chemical class 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Abstract
The utility model discloses a continuous reaction device for preparing phenyl trimethoxy silane, which comprises an operation box, wherein one end of the operation box is provided with a feed inlet, a speed limiting mechanism is arranged in the feed inlet, and one end of the speed limiting mechanism is connected with a reaction chamber; in this a continuous reaction unit for preparation of phenyl trimethoxy silane, when phenyl trimethoxy silane preparation, under the use of second driving motor, the threaded rod begins to rotate for the outside threaded connection's of threaded rod removal cover is removed to the adapter sleeve, and then will adjust the pole angle and slowly adjust to 90 degrees, increase the interval between each other of scraper blade, and then laminate the scraper blade at the inner wall of reaction chamber inner bag, and then in rotatory in-process, fully stir the inside phenyl trimethoxy silane raw materials of reaction chamber, and accelerate the reaction of phenyl trimethoxy silane raw materials, until the phenyl trimethoxy silane raw materials takes place the reaction, then get into in the next reaction chamber of group, carry out continuous reaction.
Description
Technical Field
The utility model relates to the technical field related to phenyl trimethoxy silane, in particular to a continuous reaction device for preparing phenyl trimethoxy silane.
Background
Phenyltrimethoxysilane, also known as trimethoxyphenylsilane; the mono-phenyl trimethoxy silane is insoluble in water, has a melting point of-25 ℃ and a boiling point of 233 ℃ and has a density of 1.062G/ML at 25 ℃ and is mainly used as a raw material for preparing high molecular organosilicon compounds,
however, the above-mentioned prior art solution has a drawback that the existing continuous reaction apparatus for preparing phenyltrimethoxysilane is inconvenient to adjust according to different stages of phenyltrimethoxysilane, resulting in poor phenyltrimethoxysilane preparation effect, so we propose a continuous reaction apparatus for preparing phenyltrimethoxysilane, so as to solve the above-mentioned problems.
Disclosure of Invention
The utility model aims to provide a continuous reaction device for preparing phenyl trimethoxy silane, when the phenyl trimethoxy silane is prepared, the phenyl trimethoxy silane enters corresponding reaction chambers under specific conditions according to the characteristics of the phenyl trimethoxy silane raw materials so as to react, meanwhile, under the use of a second driving motor, a threaded rod starts to rotate, a movable sleeve in threaded connection with the outer part of the threaded rod moves towards a connecting sleeve, the angle of an adjusting rod is slowly adjusted to 90 degrees, the distance between scraping plates is increased, the scraping plates are attached to the inner wall of a reaction chamber, the phenyl trimethoxy silane raw materials in the reaction chamber are fully stirred in the rotating process, the reaction of the phenyl trimethoxy silane raw materials is accelerated until the phenyl trimethoxy silane raw materials react, then the phenyl trimethoxy silane raw materials enter the next group of reaction chambers to continuously react, and in addition, under the arrangement that the scraping plates are attached to the inner wall of the reaction chamber, the phenyl trimethoxy silane raw materials can be scratched, so that cost loss is avoided.
In order to achieve the above purpose, the present utility model provides the following technical solutions: a continuous reaction unit for preparation of phenyl trimethoxy silane, includes the operation box, the feed inlet has been seted up to operation box one end, the inside speed-limiting mechanism that is provided with of feed inlet, speed-limiting mechanism one end is connected with the reaction chamber, the inside rabbling mechanism that is provided with of reaction chamber, the reaction chamber lower extreme is connected with unloading subassembly.
Preferably, the speed limiting mechanism comprises a first driving motor, a gear, a connecting frame, a sliding rail, a moving block, an opening plate and a moving groove, wherein the first driving motor is arranged on one side of a feeding hole, the gear is arranged at the output end of the first driving motor, one end of the gear is connected with the connecting frame, the sliding rail is arranged on the surface of the connecting frame, the moving block is arranged in the sliding rail in a matched mode, the opening plate is arranged at one end of the moving block, the upper end of the moving block is arranged on the surface of the moving groove, and the moving groove is arranged at the upper end of the connecting frame.
Preferably, six groups of opening and closing plates are arranged on the surface of the connecting frame, and the outer diameter sizes of the six groups of opening and closing plates are matched with the inner diameter sizes of the feed inlets.
Preferably, the reaction chambers are provided with three groups inside the operation box, and the temperatures inside the three groups of reaction chambers are different.
Preferably, the stirring mechanism comprises a second driving motor, a connecting plate, a connecting sleeve, a threaded rod, a movable sleeve, an adjusting rod, a scraping plate, a limiting block and a limiting groove, wherein the second driving motor is arranged on one side of an operation box, the connecting plate is arranged on one side of the second driving motor, the connecting sleeve is welded on one end of the connecting plate, the threaded rod penetrates through the connecting plate and the connecting sleeve, the threaded rod is arranged at the output end of the second driving motor, the movable sleeve is connected with the movable sleeve through the movable sleeve, one end of the movable sleeve is movably connected with the scraping plate through the adjusting rod, one end of the scraping plate is connected with the limiting block, the limiting block is arranged inside the limiting groove, and the limiting groove is formed in the surface of the connecting plate.
Preferably, the movable sleeve and the connecting sleeve form a movable structure through a threaded rod, and the inner diameter size of the movable sleeve is matched with the outer diameter size of the connecting sleeve.
Preferably, the scraping plate forms a rotating structure through the adjusting rod and the moving sleeve, the adjusting rod and the scraping plate are arranged on the surface of the moving sleeve from four groups, and meanwhile, the surface of the scraping plate is distributed in an arc shape.
Compared with the prior art, the utility model has the beneficial effects that:
1. this a continuous reaction unit for preparation of phenyl trimethoxy silane, through the setting of reaction chamber and rabbling mechanism, when phenyl trimethoxy silane preparation, get into corresponding reaction chamber under the characteristic according to phenyl trimethoxy silane raw materials under specific circumstances, thereby take place the reaction, simultaneously under the use of second driving motor, the threaded rod begins to rotate, make the removal cover of threaded rod outside threaded connection remove to the adapter sleeve, and then adjust gradually adjusting the regulation pole angle to 90 degrees, increase the interval between each other of scraper blade, and then laminate the scraper blade at the inner wall of reaction chamber, and then in rotatory in-process, fully stir the inside phenyl trimethoxy silane raw materials of reaction chamber, and accelerate the reaction of phenyl trimethoxy silane raw materials, until phenyl trimethoxy silane raw materials takes place the reaction, then get into next group reaction chamber, carry out continuous reaction, in addition under the setting of scraper blade laminating at the inner wall of reaction chamber inner wall, can cut and rub the phenyl trimethoxy silane raw materials, avoid leaving over, cause the cost loss.
Drawings
FIG. 1 is a schematic elevational view of the present utility model;
FIG. 2 is a schematic diagram of the speed limiting mechanism of the present utility model;
FIG. 3 is a schematic view of the stirring mechanism of the present utility model;
FIG. 4 is a schematic side view of the stirring mechanism of the present utility model.
In the figure: 1. an operation box; 2. a feed inlet; 3. a speed limiting mechanism; 301. a first driving motor; 302. a gear; 303. a connecting frame; 304. a slide rail; 305. a moving block; 306. an opening plate; 307. a moving groove; 4. a reaction chamber; 5. a stirring mechanism; 501. a second driving motor; 502. a connecting plate; 503. connecting sleeves; 504. a threaded rod; 505. a moving sleeve; 506. an adjusting rod; 507. a scraper; 508. a limiting block; 509. a limit groove; 6. and (5) blanking components.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1-4, the present utility model provides a technical solution: a continuous reaction device for preparing phenyl trimethoxysilane comprises an operation box 1, wherein a feed port 2 is formed in one end of the operation box 1, a speed limiting mechanism 3 is arranged in the feed port 2, the speed limiting mechanism 3 comprises a first driving motor 301, a gear 302, a connecting frame 303, a sliding rail 304, a moving block 305, an opening and closing plate 306 and a moving groove 307, the first driving motor 301 is arranged on one side of the feed port 2, the gear 302 is installed at the output end of the first driving motor 301, one end of the gear 302 is connected with the connecting frame 303, a sliding rail 304 is formed in the surface of the connecting frame 303, the moving block 305 is internally matched with the moving block 305, the opening and closing plate 306 is installed at one end of the moving block 305, the upper end of the moving block 305 is arranged on the surface of the moving groove 307, the moving groove 307 is formed in the upper end of the connecting frame 303, and corresponding phenyl trimethoxysilane is poured into a reaction chamber 4 from the feed port 2 according to the preparation requirement of phenyl trimethoxysilane, so that the gear 302 is rotated through the use of the first driving motor 301, the connecting frame 303 is meshed with one end of the gear 302, the connecting frame 303 is rotated, the moving block 305 connected with one end of the connecting frame 306 is further, the moving block 305 is connected with the sliding rail 303 at one end of the connecting frame, the connecting frame 306 is connected with the bottom of the connecting frame 2, the opening and closing plate 306 is slowly matched with the six-opening and closing plate 306, the inner diameter of the surface of the six-opening and closing plate 2, and closing plate is gradually arranged, and the size of the raw materials are gradually reduced, and the inside the opening and closing plate 2 is gradually;
the speed limiting mechanism 3 is characterized in that one end of the speed limiting mechanism 3 is connected with the reaction chamber 4, three groups of reaction chambers 4 are arranged in the operation box 1, the temperatures inside the three groups of reaction chambers 4 are different, the stirring mechanism 5 is arranged in the reaction chamber 4, the stirring mechanism 5 comprises a second driving motor 501, a connecting plate 502, a connecting sleeve 503, a threaded rod 504, a movable sleeve 505, an adjusting rod 506, a scraping plate 507, a limiting block 508 and a limiting groove 509, the second driving motor 501 is arranged on one side of the operation box 1, the connecting plate 502 is arranged on one side of the second driving motor 501, the connecting sleeve 503 is welded at one end of the connecting plate 502, a threaded rod 504 penetrates through the connecting plate 502 and the connecting sleeve 503, the threaded rod 504 is arranged at the output end of the second driving motor 501, a limiting block 508 is connected to one end of the scraping plate 507 through the adjusting rod 506, the limiting block 508 is arranged in the limiting groove 509, the limiting groove 509 is formed in the surface of the connecting plate 502, the movable sleeve 505 forms a movable structure through the 504 and the connecting sleeve 503, the inner diameter of the movable sleeve 505 is matched with the outer diameter of the connecting sleeve 503, the scraping plate 507 forms a rotary structure through the adjusting rod 506 and the movable sleeve 505, the movable sleeve 507 and the scraping plate 506 and the scraping plate 507 are arranged on the surface of the movable sleeve 505, and the movable sleeve 505 is distributed under the four-shaped surface of the reaction chamber 6, and the arc-shaped components are arranged at the surface of the lower surface of the reaction chamber 4, and the reaction chamber is connected with the lower end components;
when phenyltrimethoxysilane is prepared, the phenyltrimethoxysilane enters the corresponding reaction chamber 4 under specific conditions according to the characteristics of the phenyltrimethoxysilane raw materials, so that the reaction occurs, meanwhile, under the use of the second driving motor 501, the threaded rod 504 starts to rotate, so that the movable sleeve 505 in threaded connection with the threaded rod 504 moves towards the connecting sleeve 503, the angle of the adjusting rod 506 is gradually adjusted to 90 degrees, the distance between the scrapers 507 is increased, the scrapers 507 are attached to the inner wall of the reaction chamber 4, the phenyltrimethoxysilane raw materials in the reaction chamber 4 are fully stirred in the rotating process, the reaction of the phenyltrimethoxysilane raw materials is accelerated until the phenyltrimethoxysilane raw materials react, then the phenyltrimethoxysilane raw materials enter the next group of reaction chambers 4, the continuous reaction is performed, and in addition, the phenyltrimethoxysilane raw materials can be scraped and rubbed under the condition that the scrapers 507 are attached to the inner wall of the reaction chamber 4, so that cost loss is avoided.
Working principle: for such a continuous reaction device for preparing phenyl trimethoxy silane, firstly, according to the requirement of preparing phenyl trimethoxy silane, corresponding phenyl trimethoxy silane is poured into a reaction chamber 4 from a feed inlet 2, therefore, under the use of a first driving motor 301, a gear 302 is rotated, thereby a connecting frame 303 which is connected with one end of the gear 302 in a meshed manner is rotated, further a moving block 305 which is connected with one end of a starting plate 306 is moved inside a sliding rail 304 which is arranged at the bottom of the connecting frame 303, thereby the bottom of the feed inlet 2 is opened and closed, further the phenyl trimethoxy silane raw material is slowly put in, excessive put-in is avoided, then under the use of a second driving motor 501, a threaded rod 504 starts to rotate, a moving sleeve 505 which is connected with the threaded rod 504 by external threads moves towards a connecting sleeve 503, then the angle of an adjusting rod 506 is slowly adjusted to 90 degrees, the distance between the scraping plates 507 is increased, further the scraping plates 507 are attached to the inner wall of the inner liner of the reaction chamber 4, and the phenyl trimethoxy silane raw material is fully stirred in the rotating process, and the reaction of the phenyl trimethoxy silane raw material is accelerated until the phenyl trimethoxy silane is continuously rubbed into the inner wall of the reaction chamber 4, and finally, the reaction chamber is continuously lost, and the phenyl trimethoxy silane raw material is continuously prepared in the reaction chamber 4, and the reaction chamber is avoided.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. A continuous reaction unit for preparation of phenyl trimethoxy silane, includes operation box (1), its characterized in that: feed inlet (2) have been seted up to control box (1) one end, feed inlet (2) inside is provided with speed limiting mechanism (3), speed limiting mechanism (3) one end is connected with reaction chamber (4), inside rabbling mechanism (5) that are provided with of reaction chamber (4), reaction chamber (4) lower extreme is connected with unloading subassembly (6).
2. A continuous reaction apparatus for the preparation of phenyltrimethoxysilane as claimed in claim 1, wherein: the speed limiting mechanism (3) comprises a first driving motor (301), a gear (302), a connecting frame (303), a sliding rail (304), a moving block (305), an opening and closing plate (306) and a moving groove (307), wherein the first driving motor (301) is arranged on one side of a feeding hole (2), the gear (302) is installed at the output end of the first driving motor (301), one end of the gear (302) is connected with the connecting frame (303), the sliding rail (304) is arranged on the surface of the connecting frame (303), the moving block (305) is arranged in the sliding rail (304) in a matched mode, the opening and closing plate (306) is arranged at one end of the moving block (305), the upper end of the moving block (305) is arranged on the surface of the moving groove (307), and the moving groove (307) is arranged at the upper end of the connecting frame (303).
3. A continuous reaction apparatus for the preparation of phenyltrimethoxysilane as claimed in claim 2, wherein: six groups of opening and closing plates (306) are arranged on the surface of the connecting frame (303), and the outer diameter size of the six groups of opening and closing plates (306) is matched with the inner diameter size of the feed inlet (2).
4. A continuous reaction apparatus for the preparation of phenyltrimethoxysilane as claimed in claim 1, wherein: three groups of reaction chambers (4) are arranged in the operation box (1), and the temperatures in the three groups of reaction chambers (4) are different.
5. A continuous reaction apparatus for the preparation of phenyltrimethoxysilane as claimed in claim 1, wherein: the stirring mechanism (5) comprises a second driving motor (501), a connecting plate (502), a connecting sleeve (503), a threaded rod (504), a movable sleeve (505), an adjusting rod (506), a scraping plate (507), a limiting block (508) and a limiting groove (509), wherein the second driving motor (501) is arranged on one side of an operation box (1), the connecting plate (502) is arranged on one side of the second driving motor (501), the connecting sleeve (503) is welded at one end of the connecting plate (502), the threaded rod (504) is penetrated inside the connecting sleeve (503), the threaded rod (504) is arranged at the output end of the second driving motor (501), the movable sleeve (505) is connected with the movable sleeve (505) through the adjusting rod (506), the limiting block (508) is connected with one end of the scraping plate (507), and the limiting block (508) is arranged inside the limiting groove (509) and is arranged on the surface of the connecting plate (502).
6. The continuous reaction apparatus for preparing phenyltrimethoxysilane according to claim 5, wherein: the movable sleeve (505) and the connecting sleeve (503) form a movable structure through a threaded rod (504), and the inner diameter size of the movable sleeve (505) is matched with the outer diameter size of the connecting sleeve (503).
7. The continuous reaction apparatus for preparing phenyltrimethoxysilane according to claim 5, wherein: the scraping plates (507) form a rotating structure through the adjusting rods (506) and the moving sleeves (505), the surfaces of the adjusting rods (506) and the scraping plates (507) are provided with self-four groups on the surfaces of the moving sleeves (505), and meanwhile, the surfaces of the scraping plates (507) are distributed in an arc shape.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321068845.5U CN219922942U (en) | 2023-05-06 | 2023-05-06 | Continuous reaction device for preparing phenyl trimethoxy silane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321068845.5U CN219922942U (en) | 2023-05-06 | 2023-05-06 | Continuous reaction device for preparing phenyl trimethoxy silane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219922942U true CN219922942U (en) | 2023-10-31 |
Family
ID=88494054
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321068845.5U Active CN219922942U (en) | 2023-05-06 | 2023-05-06 | Continuous reaction device for preparing phenyl trimethoxy silane |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219922942U (en) |
-
2023
- 2023-05-06 CN CN202321068845.5U patent/CN219922942U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN111841423B (en) | Temperature-adjustable graphene processing equipment and use method | |
| CN212021282U (en) | A melting material modification blending device for production of liquid traditional chinese medicine wrapping bag | |
| CN219922942U (en) | Continuous reaction device for preparing phenyl trimethoxy silane | |
| CN210021926U (en) | Mixing and stirring device for lithium battery materials | |
| CN114147853B (en) | Thermal insulation mortar preparation system | |
| CN210171346U (en) | Refractory material mixing device | |
| CN216137073U (en) | Preparation facilities for gel thermal insulation coating convenient to operation | |
| CN216378110U (en) | Making wine is convenient for multi-functional fermentation cylinder that removes | |
| CN219583241U (en) | Concrete mixer with good mixing effect for construction | |
| CN221843731U (en) | Chocolate hot stirring device | |
| CN215610980U (en) | V-shaped mixer for producing soft magnetic ferrite material | |
| CN213901764U (en) | Raw materials drying equipment is used in graphite felt production | |
| CN219727004U (en) | Auxiliary structure for feed opening of injection molding machine | |
| CN219002743U (en) | Rake type stirring equipment controlled by torque | |
| CN219441364U (en) | Industrial coating agitator tank of high-efficient stirring | |
| CN219186906U (en) | Composite heat-insulating material production device | |
| CN220634347U (en) | Novel dissolving tank | |
| CN221753139U (en) | Mixing equipment for waterproof coating preparation | |
| CN221336498U (en) | Sand storage barrel for clay sand casting | |
| CN221376255U (en) | Semi-coke drying automatic discharging device | |
| CN220219207U (en) | Stirring device of extrusion type sheet machine | |
| CN213885854U (en) | A mediation cauldron for bonding wax production | |
| CN215359087U (en) | Brick making machine for cement brick production | |
| CN219463288U (en) | Stirring device for GRG gypsum powder | |
| CN218422531U (en) | Paint mixing equipment for preparing water-based epoxy zinc-rich primer |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |