CN219915372U - Detection device for content of impurities in titanium tetrachloride oil - Google Patents

Abstract

The utility model provides a detection device for the impurity content of titanium tetrachloride oil, which comprises an infrared spectrometer body and a cover hinged with the infrared spectrometer body, wherein a strip-shaped slideway is arranged on the side surface of the infrared spectrometer body in the infrared irradiation direction, a slide rail matched with the infrared spectrometer is arranged on the slideway, a strip-shaped sample detection pool is arranged on the top surface of the slide rail, a plurality of partition plates are uniformly arranged in the sample detection pool at intervals, a plurality of single and sealed sample detection cavities can be formed by the partition plates, the sample detection pool is covered by a cover plate, a liquid inlet pipe is arranged on the cover plate and is respectively communicated with the sample detection cavities, a propeller is connected to one side of the liquid inlet pipe, an electric telescopic rod is arranged on the infrared spectrometer on one side of the slideway, and the free end of the rod body of the electric telescopic rod is connected with the slide rail by a connecting block; the device can realize that titanium tetrachloride is kept apart with the air, avoids air pollution, can carry out continuous detection simultaneously, has improved work efficiency.

Description

Detection device for content of impurities in titanium tetrachloride oil

Technical Field

The utility model belongs to the technical field of detection equipment, and particularly relates to a detection device for the impurity content of titanium tetrachloride oil.

Background

Titanium tetrachloride, or titanium (IV) chloride, is an inorganic compound of the formula TiCl4, which contains various organic components, and infrared spectrometers are currently used for detecting the components.

The titanium tetrachloride has the characteristics of easy volatilization, water dissolution, toxicity and the like, so the titanium tetrachloride is mostly detected in a closed environment, the traditional detection device still needs manual operation, the harm to experimental staff is large, the infrared spectrometer for detecting the titanium tetrachloride is detected at present in a single time, the organic matter content in the titanium tetrachloride cannot be completely displayed by single detection, and further the secondary detection work can be carried out after the titanium tetrachloride is sequentially detected and is required to be cleaned and dried, so the mode has long working time and extremely influences the working efficiency.

Disclosure of Invention

The utility model provides the device for detecting the content of the oil impurities in the titanium tetrachloride, which can realize the isolation of the titanium tetrachloride and the air, avoid the air pollution, simultaneously can continuously detect, and improves the working efficiency, and the specific scheme is as follows:

the utility model provides a detection device for titanium tetrachloride oil impurity content, includes infrared spectrometer body and the lid of articulated connection thereof, be equipped with rectangular type slide on the side of infrared irradiation direction of infrared spectrometer body, and be crisscross form with the infrared irradiation direction, be equipped with rather than assorted slide rail on the slide, the slide rail top surface is equipped with a rectangular type sample detection pond along its length direction, evenly be equipped with a plurality of baffles along its length direction interval in the sample detection pond, a plurality of baffles can form a plurality of single and sealed sample detection chamber, the sample detection pond is closed by a apron lid, be equipped with the feed liquor pipe on the apron, the feed liquor pipe is linked together with a plurality of sample detection chamber respectively, be connected with one on one side of the apron and can advance the titanium tetrachloride feed liquor pipe and get into the propeller in a plurality of sample detection chamber, be equipped with electric telescopic handle on the infrared spectrometer of slide rail one side, and electric telescopic handle body free end links to each other with the slide rail by a connecting block.

Further, a strip-shaped clamping groove is formed in the sliding rail along the length direction of the sliding rail, a clamping block capable of sliding in the clamping groove is arranged in the clamping groove, and the sample detection tank is connected to the top of the clamping block.

Further, limiting blocks are respectively connected to two opposite sides of the clamping block.

Furthermore, the inside of the sample detection pond is uniformly provided with U-shaped placing grooves at intervals along the length direction, and a plurality of partition boards are respectively arranged in a plurality of placing grooves.

Still further, a plurality of baffle tops all connect perpendicularly on the apron bottom surface.

The beneficial effects of the utility model are as follows:

according to the detection device for the content of the titanium tetrachloride oil impurities, the slide way, the slide rail, the sample detection cavities separated by the partition boards and the electric telescopic rod connected with the slide rail are arranged, when the detection is finished, the electric telescopic rod works to push the slide rail, so that the next sample detection cavity is used for detection, and the following sample detection cavities are pushed in the same way, so that the titanium tetrachloride can be continuously detected, the detection continuity is improved, the detection efficiency is improved, meanwhile, the titanium tetrachloride enters the sample detection cavities through the propeller, and the titanium tetrachloride cannot contact with air until the detection is finished, and the pollution of the titanium tetrachloride to the air due to contact with the air is avoided.

Drawings

Fig. 1 is a schematic structural view of the present utility model.

Fig. 2 is a schematic view of a partial structure of the present utility model.

Fig. 3 and 4 are partial exploded views of the present utility model.

FIG. 5 is a schematic diagram of a sample detection cell according to the present utility model.

FIG. 6 is a schematic illustration of the connection of the inlet tube and the propeller of the present utility model.

Fig. 7 is a schematic diagram of a cover plate structure of the present utility model.

Wherein: the infrared spectrometer comprises an infrared spectrometer body 1, a slide way 2, a slide rail 3, a sample detection pool 4, a sample detection cavity 41, a placing groove 42, a cover 5, a partition plate 6, a cover plate 7, a liquid inlet pipe 8, a propeller 9, an electric telescopic rod 10, a connecting block 11, a clamping groove 12, a clamping block 13 and a limiting block 14.

Detailed Description

The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments.

Referring to fig. 1-7, a detecting device for the impurity content of titanium tetrachloride oil comprises an infrared spectrometer body 1 and a cover 5 hinged with the infrared spectrometer body 1, wherein the infrared spectrometer body 1 is in the prior art, a strip-shaped slide way 2 is arranged on the side surface of the infrared irradiation direction of the infrared spectrometer body 1, the distance between the infrared spectrometer body and the slide way 2 is set according to actual requirements, the infrared irradiation direction is staggered, a slide rail 3 matched with the slide rail 2 is arranged on the slide rail 2, the length of the slide rail 3 is set according to the travel of a sample detection tank 4, the top surface of the slide rail 3 is provided with a strip-shaped sample detection tank 4 along the length direction, the sample detection tank 4 is in a strip-shaped flat shape, a plurality of partition boards 6 are uniformly arranged in the sample detection tank 4 along the length direction at intervals, the partition boards 6 are perpendicular to the bottom surface of the sample detection tank 4, a plurality of the partition boards 6 can form a plurality of single and sealed sample detection cavities 41, the capacity of the sample detection cavity 41 is set according to the actual detection requirement, the sample detection tank 4 is covered by a cover plate 7, a step is circumferentially arranged at the top of the sample detection tank 4, an annular clamp suitable for covering the step is arranged on the bottom surface of the cover plate 7, a liquid inlet pipe 8 is arranged on the cover plate 7, the liquid inlet pipe 8 is respectively communicated with a plurality of sample detection cavities 41, a pusher 9 capable of pushing titanium tetrachloride into the liquid inlet pipe 8 and into a plurality of sample detection cavities 41 is connected on one side of the cover plate 7, the pusher 9 is detachably connected with the liquid inlet pipe 8, the liquid inlet pipe 8 is detachably connected with the cover plate 7, the pusher 9 can be a syringe similar to a syringe, an electric telescopic rod 10 is arranged on the infrared spectrometer body 1 on one side of the slide rail 2, the free end of the rod body of the electric telescopic rod 10 is connected with the slide rail 3 by a connecting block 11, the connecting block 11 is detachably connected with the free end part of the electric telescopic rod 10 and the sliding rail 3.

The slide rail 3 is provided with a strip-shaped clamping groove 12 along the length direction, a clamping block 13 capable of sliding in the clamping groove 12 is arranged in the clamping groove 12, the sample detection tank 4 is connected to the top of the clamping block 13, the clamping groove 12 and the clamping block 13 capable of being arranged in the clamping groove are arranged, so that after titanium tetrachloride detection is finished, the sample detection tank 4 can be directly taken out from the clamping groove 12, and the operation space is increased no matter the sample detection tank 4 is cleaned or samples are added for next detection.

Two opposite sides of the clamping block 13 are respectively connected with a limiting block 14, the two clamping blocks 13 are respectively stuck to the top surface of the clamping groove 12, and the arrangement of the two limiting blocks 14 increases the stability of the sample detection pool 4 when the electric telescopic rod 10 pushes the sliding rail 3 to advance.

The inside of the sample detection pond 4 is provided with U-shaped placing grooves 42 at equal intervals along the length direction, a plurality of baffle plates 6 are respectively arranged in the placing grooves 42, and when titanium tetrachloride is detected, the baffle plates 6 can be taken out from the placing grooves 42, so that the space of the sample detection pond 4 is enlarged for cleaning.

The tops of the plurality of clapboards 6 are vertically connected to the bottom surface of the cover plate 7, when titanium tetrachloride is detected, the cover plate 7 is only required to be taken out, and then the plurality of clapboards 6 can be taken out together, so that the space of the sample detection pool 4 is enlarged, the cleaning is convenient, the plurality of clapboards 6 are also convenient to take out in the plurality of placing grooves 42 one by one, the time is saved, and the working efficiency is further improved.

When the device is used, titanium tetrachloride is filled into the propeller 9 in advance according to the capacity of the plurality of sample detection cavities 41 and the amount of the titanium tetrachloride to be detected, then the clamping block 13 at the lower side of the sample detection pond 4 is pushed into the clamping groove 12, then the titanium tetrachloride in the propeller 9 is pushed into the liquid inlet pipe 8, then the titanium tetrachloride is pushed into each sample detection cavity 41, the cover 5 is covered, finally the infrared spectrometer body 1 is opened for detection, after detection, the sample detection pond 4 is taken out from the clamping groove 12 for cleaning the sample detection pond 4, and after detection, the data of the content of the oil impurities in the titanium tetrachloride can be obtained through the obtained map.

It will be evident to those skilled in the art that the utility model is not limited to the details of the foregoing illustrative embodiments, and that the present utility model may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the utility model being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.

Furthermore, it should be understood that although the present disclosure describes embodiments, not every embodiment is provided with a separate embodiment, and that this description is provided for clarity only, and that the disclosure is not limited to the embodiments described in detail below, and that the embodiments described in the examples may be combined as appropriate to form other embodiments that will be apparent to those skilled in the art.

Claims (5)

1. A detection device for titanium tetrachloride oil impurity content, its characterized in that: including infrared spectrometer body (1) and rather than hinged lid (5) of connection, be equipped with rectangular type slide (2) on the side of infrared irradiation direction of infrared spectrometer body (1), and be crisscross form with the infrared irradiation direction, be equipped with on slide (2) rather than assorted slide rail (3), slide rail (3) top surface is equipped with rectangular type sample detection pond (4) along its length direction, be equipped with a plurality of baffles (6) along its length direction even interval in sample detection pond (4), a plurality of baffles (6) can form a plurality of singles and sealed sample detection chamber (41), sample detection pond (4) are closed by a apron (7) lid, be equipped with feed liquor pipe (8) on apron (7), feed liquor pipe (8) are linked together with a plurality of sample detection chamber (41) respectively, be connected with one on one side of apron (7) can advance feed liquor pipe (8) and advance into a plurality of sample detection chamber (41) propeller (9), be equipped with on infrared spectrometer body (1) of slide (2) one side and be equipped with electric rod body (10) and flexible end (10) and flexible link to each other by slide rail (11).

2. The detection device for the impurity content of titanium tetrachloride oil according to claim 1, wherein: the slide rail (3) is provided with a strip-shaped clamping groove (12) along the length direction, a clamping block (13) capable of sliding in the clamping groove (12) is arranged in the clamping groove, and the sample detection tank (4) is connected to the top of the clamping block (13).

3. The detection apparatus for the impurity content of titanium tetrachloride oil according to claim 2, wherein: limiting blocks (14) are respectively connected to two opposite sides of the clamping block (13).

4. The detection device for the impurity content of titanium tetrachloride oil according to claim 1, wherein: the inside of the sample detection pool (4) is uniformly provided with U-shaped placing grooves (42) at intervals along the length direction, and a plurality of partition boards (6) are respectively arranged in the placing grooves (42).

5. The detection device for the impurity content of titanium tetrachloride oil according to claim 4, wherein: the tops of the plurality of baffle plates (6) are vertically connected to the bottom surface of the cover plate (7).