CN219891178U - Chromatographic column for purifying and separating sanguisorbin - Google Patents
Chromatographic column for purifying and separating sanguisorbin Download PDFInfo
- Publication number
- CN219891178U CN219891178U CN202321066160.7U CN202321066160U CN219891178U CN 219891178 U CN219891178 U CN 219891178U CN 202321066160 U CN202321066160 U CN 202321066160U CN 219891178 U CN219891178 U CN 219891178U
- Authority
- CN
- China
- Prior art keywords
- fixedly connected
- plate
- chromatographic column
- fixed
- fixed ring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229930190125 Sanguisorbin Natural products 0.000 title claims abstract description 18
- 238000013375 chromatographic separation Methods 0.000 claims abstract description 17
- 238000000746 purification Methods 0.000 claims description 11
- 238000000926 separation method Methods 0.000 claims description 11
- 239000007787 solid Substances 0.000 claims description 9
- 238000009434 installation Methods 0.000 claims description 4
- 235000008282 Sanguisorba officinalis Nutrition 0.000 description 4
- 235000008291 Poterium sanguisorba Nutrition 0.000 description 3
- 244000173853 Sanguisorba officinalis Species 0.000 description 3
- 239000000203 mixture Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000010355 oscillation Effects 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 235000004789 Rosa xanthina Nutrition 0.000 description 1
- 241000220222 Rosaceae Species 0.000 description 1
- 241000581682 Sanguisorba Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
Landscapes
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
The utility model relates to the technical field of chromatographic columns and discloses a chromatographic column for purifying and separating sanguisorbin II, which comprises a bottom plate, wherein a fixing plate is fixedly connected to the rear side of the top end of the bottom plate, the fixing plate is connected with a pushing plate through a threaded rod, the pushing plate is connected with pushing blocks through fixing grooves, the pushing blocks are respectively arranged on two sides of a blanking section, a chromatographic separation section is arranged at the bottom end of the blanking section, a fixing ring II is fixedly connected to the outer side of the top end of the blanking section, a fixing ring I is arranged at the top end of the fixing ring II, a bolt II is connected to the fixing ring I through a sleeve, the fixing block II is rotationally connected with the fixing block II through a connecting rod and a supporting rod, and a limiting plate is fixedly connected to the outer side of one end of the sleeve. In the utility model, the sleeve is extended into the first fixed ring and the second fixed ring, and the chromatographic separation section and the blanking section are connected by utilizing the cooperation of the combined supporting rod, the connecting rod and the limiting plate.
Description
Technical Field
The utility model relates to the technical field of chromatographic columns, in particular to a chromatographic column for secondary purification and separation of sanguisorbin.
Background
The garden burnet is perennial herb plant of the genus garden burnet of the family Rosaceae, thirty to one hundred twenty cm in height, upright stem and arris, and the garden burnet is a common traditional Chinese herbal medicine, has cold nature, bitter taste and no toxicity; the Chinese medicinal composition has the effects of cooling blood, stopping bleeding, clearing heat and detoxicating, cultivating and nourishing yin, detumescence and healing sore, and the like, and simultaneously needs to use a chromatographic column when purifying and separating the Chinese medicinal composition.
The chromatographic column consists of a column tube, a press cap, a sealing ring, a filter disc, a joint, a screw and the like, the chromatographic column is often required to be cleaned after the second sanguisorbin is purified and separated by the chromatographic column, so that the next use is prevented from being influenced, and meanwhile, the chromatographic column is required to be fully mixed and reacted in the chromatographic column in the purification and separation process.
Disclosure of Invention
The utility model aims to solve the defects in the prior art, and provides a chromatographic column for purifying and separating sanguisorbin.
In order to achieve the above purpose, the present utility model adopts the following technical scheme: the utility model provides a chromatographic column is used in purification of two separation of sanguisorbin, includes the bottom plate, bottom plate top rear side fixedly connected with fixed plate, the inside threaded connection in fixed plate top has the threaded rod, the threaded rod other end rotates and is connected with the push pedal, the equal fixedly connected with fixed slot in push pedal both sides, the equal sliding connection in fixed slot has the ejector pad, the ejector pad sets up respectively in unloading section both sides, unloading section bottom is provided with the chromatographic separation section, unloading section top outside fixedly connected with solid fixed ring two, gu fixed ring two tops are provided with solid fixed ring one, gu fixed ring one both ends all run through there is the sleeve, the equal threaded connection in sleeve inside has the bolt two, the equal rotation of bolt two removal is connected with gu fixed block two, two one side four corners of fixed block all rotate and are connected with the connecting rod, the equal rotation of connecting rod other end is connected with the bracing piece, the bracing piece other end all rotates and is connected in fixed block one end four corners, sleeve one end outside fixedly connected with limiting plate.
As a further description of the above technical solution:
the utility model discloses a motor, including bottom plate, mounting panel, slider, screw bolt, reciprocating screw rod, motor drive end, the spout has been seted up on the bottom plate top, the inside sliding connection of spout has the slider, the slider top rotates and is connected with the backup pad, the backup pad is connected with the mounting panel through electric putter, equal fixedly connected with installation piece in mounting panel one side both ends, the inside equal threaded connection of installation piece has bolt one, one side that bolt one is close to each other all rotates and is connected with the clamp splice, the inside threaded connection of slider has reciprocating screw rod, bottom plate one side fixedly connected with motor, motor drive end runs through spout lateral wall fixedly connected with reciprocating screw rod.
As a further description of the above technical solution:
one side of the limiting plate is provided with a first fixed block, and the first fixed block is rotationally connected to one end, far away from the limiting plate, of the sleeve.
As a further description of the above technical solution:
the electric putter fixed connection is in bracing piece top one side, electric putter drive end fixedly connected with mounting panel.
As a further description of the above technical solution:
one end of the sleeve, which is far away from the first fixed ring, penetrates through two ends of the fixed ring respectively, and the first fixed ring is fixedly connected to the outer side of the bottom end of the blanking section.
As a further description of the above technical solution:
the locating device is characterized in that locating rods are fixedly connected to two ends of one side of the push plate, which is close to the threaded rod, the other ends of the locating rods are slidably connected inside locating holes, and the locating holes are respectively formed in two ends of one side of the fixed plate, which is close to the push plate.
As a further description of the above technical solution:
springs are fixedly connected to four corners of the inner bottom wall of the fixed groove, and the other ends of the springs are respectively and fixedly connected to four corners of one side, away from each other, of the pushing block.
The utility model has the following beneficial effects:
1. in the utility model, when the chromatographic separation section and the blanking section are required to be cleaned, the sleeve is taken out from the first fixing ring and the second fixing ring and cleaned, then the sleeve extends into the first fixing ring and the second fixing ring, and the chromatographic separation section and the blanking section are connected by utilizing the cooperation of the combined supporting rod, the connecting rod and the limiting plate.
2. According to the chromatographic separation device, the chromatographic separation section is fixed by utilizing the cooperation of the clamping block and the first bolt, the motor is operated to enable the reciprocating screw rod to rotate, the sliding block is pushed to move by utilizing the rotation of the reciprocating screw rod, and the sliding block and the supporting plate are matched to enable the sliding block to oscillate.
Drawings
FIG. 1 is a front perspective view of a chromatographic column for purifying and separating sanguisorbin II;
FIG. 2 is a front perspective view of a bottom plate of a chromatographic column for purifying and separating sanguisorbin II;
FIG. 3 is a top perspective view of a fixing plate of a chromatographic column for purifying and separating sanguisorbin II;
fig. 4 is a schematic perspective view of a sleeve of a chromatographic column for purifying and separating sanguisorbin.
Legend description:
1. a bottom plate; 2. a chromatographic separation section; 3. a blanking section; 4. a fixing plate; 5. a slide block; 6. a motor; 7. a chute; 8. a reciprocating screw rod; 9. a first bolt; 10. an electric push rod; 11. a support plate; 12. a mounting block; 13. clamping blocks; 14. a threaded rod; 15. positioning holes; 16. a positioning rod; 17. a pushing block; 18. a fixing groove; 19. a spring; 20. a first fixed ring; 21. a second fixing ring; 22. a support rod; 23. a sleeve; 24. a second bolt; 25. a limiting plate; 26. a first fixed block; 27. a connecting rod; 28. a second fixed block; 29. a push plate; 30. and (3) mounting a plate.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Referring to fig. 1-4, one embodiment provided by the present utility model is: the utility model provides a chromatographic column for purification and separation of sanguisorba saponin two, comprising a base plate 1, bottom plate 1 top rear side fixedly connected with fixed plate 4, fixed plate 4 top inside threaded connection has threaded rod 14, threaded rod 14 other end rotation is connected with push pedal 29, the equal fixedly connected with fixed slot 18 in push pedal 29 both sides, the equal sliding connection in fixed slot 18 inside has push pedal 17, push pedal 17 sets up respectively in unloading section 3 both sides, unloading section 3 bottom is provided with chromatographic separation section 2, unloading section 3 top outside fixedly connected with solid fixed ring two 21, gu fixed ring two 21 top is provided with solid fixed ring one 20, utilize gu fixed ring one 20 and gu fixed ring two 21, sleeve 23, gu fixed ring two 24's cooperation is fixed unloading section 3 and chromatographic separation section 2, gu fixed ring one 20 both ends all run through and have sleeve 23, sleeve 23 inside equal threaded connection has bolt two 24, the equal sliding connection of bolt two 24 moves and has gu fixed block two 28, gu fixed block two 28 one side equal sliding connection in four corners connecting rod 27, the equal sliding connection in four corners 27 has bracing piece 22, bracing piece 22 other end all sliding connection in solid fixed block one end 26, gu fixed ring one end 23 outside solid fixed ring one end 25, gu fixed ring one end 25 need of moving and moving down fixed ring two ends 25, need of solid fixed ring two sides 25, when moving and two fixed ring 23 and two fixed ring 23 need of inner diameter sides 25, and two fixed ring 2 are stretched into to one end and two fixed ring 2, and one fixed ring 2 and one fixed ring is fixed ring 2 is fixed ring one end is fixed ring is fixed segment is fixed with 2 and fixed ring one side is fixed ring 2 and is fixed with 2, and is fixed ring 2 is fixed with one end is fixed ring 2, and is separated by two fixed ring and is 23 and is fixed and is moved after and is fixed segment is separated 2 and 23 and is separated.
The top end of the bottom plate 1 is provided with a chute 7, the inside of the chute 7 is slidingly connected with a slide block 5, the top end of the slide block 5 is rotationally connected with a supporting plate 11, the supporting plate 11 is connected with a mounting plate 30 through an electric push rod 10, one side of the mounting plate 30 is fixedly connected with a mounting block 12, the inside of the mounting block 12 is connected with a first bolt 9 in a threaded manner, one side of the first bolt 9, which is mutually close, is rotationally connected with a clamping block 13, the inside of the slide block 5 is connected with a reciprocating screw rod 8 in a threaded manner, one side of the bottom plate 1 is fixedly connected with a motor 6, the driving end of the motor 6 penetrates through the side wall of the chute 7 and is fixedly connected with the reciprocating screw rod 8, the reciprocating screw rod 8 is fixed by the cooperation of the pushing block 17 and the clamping block 13, the motor 6 can be operated after that, the reciprocating screw rod 8 is rotated by the reciprocating screw rod 8 is pushed to move by the rotation of the reciprocating screw rod 8, the sliding block 5 is oscillated by the cooperation of the sliding block 5 and the supporting plate 11, and the pushing plate 29 is moved to the fixed plate 4 when oscillation is not needed, one side of the limiting plate 25 is provided with a first fixed block 26, the first fixed block 26 is rotationally connected to one end of the sleeve 23 far away from the limiting plate 25, the chromatographic separation section 2 and the blanking section 3 are connected by utilizing the cooperation of the combined supporting rod 22, the connecting rod 27 and the limiting plate 25, the electric push rod 10 is fixedly connected to one side of the top end of the supporting rod 22, the driving end of the electric push rod 10 is fixedly connected with a mounting plate 30, the push plate 29 is pushed to move by the operation of the electric push rod 10, so that the clamping block 13 can fix the chromatographic separation section 2, one end of the sleeve 23 far away from the first fixed ring 20 penetrates through two ends of the second fixed ring 21 respectively, the first fixed ring 20 is fixedly connected to the outer side of the bottom end of the blanking section 3, the sleeve 23 stretches into the first fixed ring 20 and the second fixed ring 21, the second fixed ring 24 is rotated to enable the second fixed block 28 to approach the first fixed block 26, so that the supporting rod 22 is combined with the connecting rod 27, the chromatographic separation section 2 and the blanking section 3 are connected by utilizing the combined supporting rod 22, the connecting rod 27 and the limit plate 25, the two ends of one side of the push plate 29 close to the threaded rod 14 are fixedly connected with the positioning rods 16, the other ends of the positioning rods 16 are slidably connected in the positioning holes 15, the positioning holes 15 are respectively formed in the two ends of one side of the fixed plate 4 close to the push plate 29, when vibration is not needed, the threaded rod 14 can be rotated to enable the push plate 29 to move towards the fixed plate 4, the positioning rods 16 extend into the positioning holes 15, the push plate 29 is fixed, springs 19 are fixedly connected to four corners of the inner bottom wall of the fixed groove 18, the other ends of the springs 19 are fixedly connected to four corners of one side of the push block 17 away from each other, the push block 17 is pushed by the pushing force of the springs 19 to move towards the opposite directions, and the blanking section 3 is clamped and fixed.
Working principle: when the chromatographic separation section 2 and the blanking section 3 need to be cleaned, the sleeve 23 is taken out from the inside of the first fixed ring 20 and the second fixed ring 21 and cleaned, after cleaning, the sleeve 23 can be stretched into the inside of the first fixed ring 20 and the second fixed ring 21 again, the second fixed block 28 is close to the first fixed block 26 by rotating the second bolt 24, so that the support rod 22 and the connecting rod 27 are combined, the chromatographic separation section 2 and the blanking section 3 are connected by the combined support rod 22, the connecting rod 27 and the limit plate 25, the blanking section 3 and the chromatographic separation section 2 can be placed between the two push blocks 17 and the two clamping blocks 13 respectively in use, the push blocks 17 and the clamping blocks 13 are fixed by the cooperation, the reciprocating screw rod 8 is rotated by the motor 6, the sliding block 5 is pushed to move by the rotation of the reciprocating screw rod 8, the sliding block 5 and the supporting plate 11 are oscillated by the cooperation of the sliding block 5, the push plate 29 is moved towards the fixed plate 4 by the rotary 14 when the oscillation is not needed, and the positioning rod 16 is stretched into the positioning hole 15 to fix the push plate 29.
Finally, it should be noted that: the foregoing description is only illustrative of the preferred embodiments of the present utility model, and although the present utility model has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described, or equivalents may be substituted for elements thereof, and any modifications, equivalents, improvements or changes may be made without departing from the spirit and principles of the present utility model.
Claims (7)
1. The chromatographic column for the purification and separation of sanguisorbin comprises a bottom plate (1), and is characterized in that: bottom plate (1) top rear side fixedly connected with fixed plate (4), the inside threaded connection in fixed plate (4) top has threaded rod (14), threaded rod (14) other end rotates and is connected with push pedal (29), equal fixedly connected with fixed slot (18) in push pedal (29) both sides, equal sliding connection in fixed slot (18) inside has ejector pad (17), ejector pad (17) set up respectively in unloading section (3) both sides, unloading section (3) bottom is provided with chromatographic separation section (2), unloading section (3) top outside fixedly connected with solid fixed ring two (21), gu fixed ring two (21) top is provided with solid fixed ring one (20), gu fixed ring one (20) both ends all run through there is sleeve (23), equal threaded connection in sleeve (23) inside has bolt two (24), bolt two (24) remove and all rotate and be connected with fixed block two (28), fixed block two (28) four corners all rotate and are connected with connecting rod (27), connecting rod (27) other end all rotate and are connected with bracing piece (22), one end (25) is connected with bracing piece (22) in the outside fixed plate (25).
2. The chromatographic column for secondary purification and separation of sanguisorbin according to claim 1, wherein the chromatographic column comprises the following components: spout (7) have been seted up on bottom plate (1) top, inside sliding connection of spout (7) has slider (5), slider (5) top rotation is connected with backup pad (11), backup pad (11) are connected with mounting panel (30) through electric putter (10), equal fixedly connected with installation piece (12) in mounting panel (30) one side both ends, the inside equal threaded connection of installation piece (12) has bolt one (9), the equal rotation in one side that bolt one (9) is close to each other is connected with clamp splice (13), slider (5) inside threaded connection has reciprocating lead screw (8), bottom plate (1) one side fixedly connected with motor (6), motor (6) drive end runs through spout (7) lateral wall fixedly connected with reciprocating lead screw (8).
3. The chromatographic column for secondary purification and separation of sanguisorbin according to claim 1, wherein the chromatographic column comprises the following components: one side of the limiting plate (25) is provided with a first fixed block (26), and the first fixed block (26) is rotationally connected to one end, far away from the limiting plate (25), of the sleeve (23).
4. The chromatographic column for secondary purification and separation of sanguisorbin according to claim 2, wherein: the electric push rod (10) is fixedly connected to one side of the top end of the supporting rod (22), and the driving end of the electric push rod (10) is fixedly connected with the mounting plate (30).
5. The chromatographic column for secondary purification and separation of sanguisorbin according to claim 1, wherein the chromatographic column comprises the following components: one end of the sleeve (23) far away from the first fixed ring (20) penetrates through two ends of the second fixed ring (21) respectively, and the first fixed ring (20) is fixedly connected to the outer side of the bottom end of the blanking section (3).
6. The chromatographic column for secondary purification and separation of sanguisorbin according to claim 1, wherein the chromatographic column comprises the following components: the push plate (29) is close to the locating rod (16) fixedly connected with both ends of one side of the threaded rod (14), the other end of the locating rod (16) is slidably connected inside the locating hole (15), and the locating hole (15) is respectively formed in both ends of one side of the fixed plate (4) close to the push plate (29).
7. The chromatographic column for secondary purification and separation of sanguisorbin according to claim 1, wherein the chromatographic column comprises the following components: springs (19) are fixedly connected to four corners of the inner bottom wall of the fixing groove (18), and the other ends of the springs (19) are fixedly connected to four corners of one side, away from each other, of the pushing block (17) respectively.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202321066160.7U CN219891178U (en) | 2023-05-06 | 2023-05-06 | Chromatographic column for purifying and separating sanguisorbin |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202321066160.7U CN219891178U (en) | 2023-05-06 | 2023-05-06 | Chromatographic column for purifying and separating sanguisorbin |
Publications (1)
Publication Number | Publication Date |
---|---|
CN219891178U true CN219891178U (en) | 2023-10-24 |
Family
ID=88398076
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202321066160.7U Active CN219891178U (en) | 2023-05-06 | 2023-05-06 | Chromatographic column for purifying and separating sanguisorbin |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN219891178U (en) |
-
2023
- 2023-05-06 CN CN202321066160.7U patent/CN219891178U/en active Active
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101186572B (en) | Method for separating and purifying salvianolic acid from red sage root liquid extract by one step | |
CN105154478B (en) | A kind of method of high speed adverse current chromatogram and high performance liquid chromatography combination preparation high-purity hydroxytyrosol | |
CN102584918B (en) | Method for preparing high-purity baicalin | |
CN102702150B (en) | Preparation method and application of hydroxysafflor yellow A | |
CN102976909B (en) | Method for extracting and purifying 6-gingerol from ginger | |
CN101260131A (en) | Method for extracting iridoid active site and monomer from eucommia bark | |
CN219891178U (en) | Chromatographic column for purifying and separating sanguisorbin | |
CN112472727B (en) | Method for co-producing ginkgo leaf extract, terpene lactone and shikimic acid | |
CN208823982U (en) | A kind of Multi-channel solid phase extraction equipment | |
CN1762428A (en) | Method for extracting efficient component from mulberry leaf | |
CN107098942A (en) | A kind of method of kaempferia galamga glycosides in Subcritical Water Extraction radish leaves | |
CN108970175A (en) | Intelligent Chinese Traditional Medicine effective component extraction element | |
CN1171857C (en) | Process for enriching and purifying capsaicin with macroporous adsorption resin | |
CN209969732U (en) | A cutting auxiliary device that is arranged in titanium alloy blank pipe course of working | |
CN1193993C (en) | Chrysanthemum total flavone resin purification method | |
CN111300297A (en) | Be used for intelligent furniture production to use clamping device | |
CN111072736A (en) | A component rich in liquiritin and glycyrrhizic acid in Glycyrrhrizae radix extract and its preparation method | |
CN211986489U (en) | Blood filter device mount | |
CN109369382B (en) | A method for preparing ginkgolic acids | |
CN1295239C (en) | Process for extracting camptothecin | |
CN112480195A (en) | Novel method for enriching and purifying baicalin in scutellaria baicalensis by ZIF-8 | |
CN218695489U (en) | Large-scale metal target material welding device | |
CN212039400U (en) | Compressed air gas-liquid separation equipment | |
CN111909050A (en) | Enrichment and separation method of pepper polyene amide monomers and fragrance components | |
CN220922667U (en) | Prunella spike cutting device |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
GR01 | Patent grant | ||
GR01 | Patent grant |