CN219849642U - Reaction separator for improving product purity and yield - Google Patents
Reaction separator for improving product purity and yield Download PDFInfo
- Publication number
- CN219849642U CN219849642U CN202321354093.9U CN202321354093U CN219849642U CN 219849642 U CN219849642 U CN 219849642U CN 202321354093 U CN202321354093 U CN 202321354093U CN 219849642 U CN219849642 U CN 219849642U
- Authority
- CN
- China
- Prior art keywords
- reaction
- horizontal container
- diaphragm
- outlet
- waste gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 81
- 238000000926 separation method Methods 0.000 claims abstract description 42
- 238000005192 partition Methods 0.000 claims abstract description 28
- 239000007788 liquid Substances 0.000 claims description 33
- 239000002994 raw material Substances 0.000 claims description 28
- 239000002912 waste gas Substances 0.000 claims description 25
- 239000007921 spray Substances 0.000 claims description 14
- 239000007789 gas Substances 0.000 claims description 7
- 238000005507 spraying Methods 0.000 claims description 3
- 230000007547 defect Effects 0.000 abstract description 4
- 238000000034 method Methods 0.000 description 8
- 230000008569 process Effects 0.000 description 6
- 238000012423 maintenance Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000001311 chemical methods and process Methods 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Abstract
The utility model relates to a reaction separator for improving the purity and yield of products, which comprises a horizontal container, a circulating pump, a jet pump, an anti-blocking nozzle, an inclined guide plate and a baffle plate; the partition plate comprises a longitudinal partition plate and a transverse partition plate; the utility model overcomes the defects of short reaction and separation flow and insufficient time of the existing reaction separator, utilizes the partition plate to reasonably divide the internal space of the reaction separator, increases the volumes of a reaction section and a separation section, and effectively prolongs the reaction and separation time on the premise of unchanged volume of the reaction separator, thereby improving the yield and purity of the product.
Description
Technical Field
The utility model relates to the technical field of chemical equipment, in particular to a reaction separator for improving the purity and yield of a product.
Background
Chemical equipment exists depending on chemical technology and serves the chemical technological process. In the traditional chemical process flow, the reaction equipment and the separation equipment are required to be arranged separately, the process flow is long, the occupied area is large, the operation is complex, the investment is high, and the maintenance cost is high. Along with the improvement of chemical process flow, a reaction separator integrating reaction and separation functions is provided. The 'a horizontal reaction separator integrating reaction and separation functions' disclosed in Chinese patent application with the application publication number of CN 110947343A comprises a horizontal container, a circulating pump, a jet pump, an anti-blocking nozzle, an inclined guide plate, a partition plate and a jet pipe, wherein the inclined guide plate and the partition plate are arranged in the horizontal container and are divided into a reaction section and a separation section; the inlet of the circulating pump is connected with the horizontal container, the outlet of the circulating pump is connected with the jet pump, the jet pump and the jet pipe, the jet pipe stretches into the horizontal container, and a plurality of anti-blocking spray heads are uniformly distributed at the end part of the jet pipe. The beneficial effects are as follows: the method overcomes the defect that the reaction equipment and the separation equipment are independently arranged in the existing chemical process flow, shortens the process flow, reduces the occupied area, reduces the equipment, reduces the investment, simplifies the operation and reduces the maintenance cost.
However, with the practical application of the reaction separator in production, people gradually find that the reaction and separation are insufficient, the purity and yield of the product are affected, and the main reason is that the residence time of the raw materials in the reaction section and the separation section is insufficient, and the reaction separator cannot be lengthened infinitely due to the influence of factors such as sites, equipment manufacturing and the like. Therefore, there is a need to develop a reaction separator capable of effectively improving the purity and yield of the product.
Disclosure of Invention
The utility model provides a reaction separator for improving the purity and the yield of products, which overcomes the defects of short reaction and separation flow and insufficient time existing in the prior reaction separator, utilizes a baffle plate to reasonably divide the internal space of the reaction separator, increases the volumes of a reaction section and a separation section, and effectively prolongs the reaction and separation time on the premise of unchanged volume of the reaction separator, thereby improving the yield and the purity of the products.
In order to achieve the above purpose, the utility model is realized by adopting the following technical scheme:
a reaction separator for improving the purity and yield of products comprises a horizontal container, a circulating pump, a jet pump, an anti-blocking nozzle, an inclined guide plate and a baffle plate; the horizontal container is provided with a raw material inlet, a circulating liquid outlet, a light component outlet, a heavy component outlet and a waste gas outlet; the partition plate comprises a longitudinal partition plate and a transverse partition plate; the waste gas outlet is arranged at one end of the top of the horizontal container, the longitudinal partition plate is vertically arranged in the middle of the horizontal container, one end and two sides of the longitudinal partition plate are fixedly connected with the inner wall of the horizontal container, and a gap is reserved between one end of the corresponding waste gas outlet and the inner wall of the horizontal container; the internal space of the horizontal container at two sides of the longitudinal partition plate is respectively a reaction section and a separation section; wherein, the reaction section is provided with a raw material inlet at one end far away from the bottom of the waste gas outlet, and a plurality of groups of anti-blocking spray heads are longitudinally arranged in the reaction section; the liquid inlet end of each group of anti-blocking spray heads is connected with a circulating liquid outlet through a circulating liquid pipeline, a circulating pump and a jet pump are arranged on the circulating liquid pipeline, and the jet pump is provided with a raw material gas inlet; a plurality of groups of inclined guide plates are longitudinally arranged in the separation section, a diaphragm is arranged at one end of the separation section, which is far away from the waste gas outlet, the diaphragm is vertically arranged, one end of the diaphragm is connected with the longitudinal diaphragm, the other end of the diaphragm is connected with the inner wall of the horizontal container, an upper notch is reserved between the top of the diaphragm and the top of the horizontal container, and a lower notch is reserved between the bottom of the diaphragm and the bottom of the horizontal container; the upper part of one end of the horizontal container far away from the waste gas outlet is provided with a light component outlet, and the bottom is provided with a heavy component outlet.
Further, the spraying direction of the anti-blocking spray head is the same as the flowing direction of the liquid raw material.
Further, a plurality of groups of inclined guide plates are arranged at equal intervals.
Compared with the prior art, the utility model has the beneficial effects that:
1) The defects of short reaction and separation flow and insufficient time existing in the existing reaction separator are overcome, the internal space of the reaction separator is reasonably divided by the partition plate, the volumes of the reaction section and the separation section are increased, and the reaction and separation time is effectively prolonged on the premise of unchanged volume and raw material processing capacity of the reaction separator, so that the yield and purity of products are improved;
2) The reaction separator integrates the reaction and separation functions, has short process flow, simple operation, external vulnerable equipment and convenient maintenance;
3) The reaction separator is favorable for full reaction of raw materials, separation of light and heavy components and higher product purity and yield;
4) The reaction separator is a horizontal container, the arrangement of the reaction section and the separation section is compact and reasonable, the reaction process and the separation process are carried out simultaneously, and the light and heavy components are separated only by using density difference gravity, so that the operation cost is lower.
Drawings
FIG. 1 is a top view of a reaction separator according to the present utility model.
Fig. 2 is a left side view of fig. 1.
FIG. 3 is a schematic view of the distribution of baffles in a reaction separator according to the present utility model.
In the figure: 1. horizontal vessel 2, raw material inlet 3, waste gas outlet 4, light component outlet 5, heavy component outlet 6, longitudinal partition 7, anti-blocking spray head 8, inclined guide plate 9, diaphragm 10, circulating pump 11, jet pump 12, upper notch 13, lower notch I, reaction section II and separation section
Detailed Description
The following is a further description of embodiments of the utility model, taken in conjunction with the accompanying drawings:
as shown in fig. 1 to 3, the reaction separator for improving the purity and the yield of the product comprises a horizontal container 1, a circulating pump 10, a jet pump 11, an anti-blocking nozzle 7, an inclined guide plate 8 and a partition plate; the horizontal container 1 is provided with a raw material inlet 2, a circulating liquid outlet, a light component outlet 4, a heavy component outlet 5 and an exhaust gas outlet 3; the partition plate comprises a longitudinal partition plate 6 and a transverse partition plate 9; the waste gas outlet 3 is arranged at one end of the top of the horizontal container 1, the longitudinal baffle plate 6 is vertically arranged in the middle of the horizontal container 1, one end and two sides of the longitudinal baffle plate 6 are fixedly connected with the inner wall of the horizontal container 1, and a gap is reserved between one end of the corresponding waste gas outlet 3 and the inner wall of the horizontal container 1; the internal space of the horizontal container 1 at two sides of the longitudinal partition plate 6 is respectively provided with a reaction section I and a separation section II; wherein, the reaction section I is provided with a raw material inlet 2 at one end far away from the bottom of the waste gas outlet 3, and a plurality of groups of anti-blocking spray heads 7 are longitudinally arranged in the reaction section I; the liquid inlet end of each group of anti-blocking spray heads 7 is connected with a circulating liquid outlet through a circulating liquid pipeline, a circulating pump 10 and a jet pump 11 are arranged on the circulating liquid pipeline, and the jet pump 11 is provided with a raw material gas inlet; a plurality of groups of inclined guide plates 8 are longitudinally arranged in the separation section II, a diaphragm plate 9 is arranged at one end of the separation section II far away from the waste gas outlet 3, the diaphragm plate 9 is vertically arranged, one end of the diaphragm plate 9 is connected with the longitudinal diaphragm plate 6, the other end of the diaphragm plate is connected with the inner wall of the horizontal container 1, an upper notch 12 is reserved between the top of the diaphragm plate 9 and the top of the horizontal container 1, and a lower notch 13 is reserved between the bottom of the diaphragm plate 9 and the bottom of the horizontal container 1; the horizontal container 1 is provided with a light component outlet 4 at the upper part of one end far away from the waste gas outlet 3, and a heavy component outlet 5 at the bottom.
Further, the spraying direction of the anti-blocking spray head 7 is the same as the flowing direction of the liquid raw material.
Further, the plurality of groups of inclined guide plates 8 are arranged at equal intervals.
The reaction separator for improving the purity and the yield of the product has the following working processes:
1) The liquid raw material enters a reaction section I of the horizontal container 1 from a raw material inlet 2, part of the liquid raw material flows out from a circulating liquid outlet, is pressurized by a circulating pump 10, enters a jet pump 11 to be fully mixed with raw material gas, and is then sprayed into the reaction section I through an anti-blocking nozzle 7 to complete gas-liquid reaction; the waste gas generated by the gas-liquid reaction is discharged from a waste gas outlet 3;
2) The gas-liquid mixture formed after the gas-liquid reaction flows into the separation section II through a notch at the end part of the longitudinal partition plate 6; under the action of the inclined guide plate 8, the light components in the gas-liquid mixture rise in an accelerating way and the heavy components fall in an accelerating way, so that the separation of the light components and the heavy components is completed;
3) The separated light components enter the other side of the diaphragm 9 through an upper notch 12 above the diaphragm 9 and flow out through a light component outlet 4; the heavy component enters the other side of the diaphragm 9 through a lower notch 13 below the diaphragm 9 and flows out through the heavy component outlet 5.
The reaction separator for improving the purity and the yield of the product integrates the reaction and separation functions, the body of the reaction separator is a horizontal container 1, the reaction separator is divided into a reaction section I and a separation section II by a longitudinal partition plate 6, and the lengths of the reaction section I and the separation section II are close to the length of the horizontal container 1. The material flow directions in the reaction section I and the separation section II are opposite. Compared with the conventional reaction separator, the reaction separator has larger space between the reaction section I and the separation section II, long flow path of raw materials and long residence time, is favorable for full reaction of the raw materials and separation of light and heavy components, and therefore, the product purity and the yield are higher, and the process requirements can be completely met. In addition, the utility model has the advantages of external vulnerable equipment and convenient maintenance.
The anti-blocking spray heads 7 in the reaction section I can be divided into a plurality of groups to be arranged, so that the raw materials are mixed more uniformly, and laminar flow is avoided.
The inclined baffles 8 of the separation section ii may be arranged in several groups and equally spaced apart. The upper and lower ends of the diaphragm 9 are respectively provided with an upper notch 12 and a lower notch 13, and the separated light component and heavy component respectively flow to the other side of the diaphragm 9 through the upper notch 12 and the lower notch 13 and flow out through corresponding outlets.
The following examples are given by way of illustration of detailed embodiments and specific procedures based on the technical scheme of the present utility model, but the scope of the present utility model is not limited to the following examples.
[ example ]
In the embodiment, the reaction separator for improving the purity and the yield of the product comprises a horizontal container 1, a circulating pump 10, a jet pump 11, an anti-blocking nozzle 7, an inclined guide plate 8, a longitudinal baffle plate 6 and a transverse baffle plate 9; the horizontal container 1 is provided with a raw material inlet 2, a circulating liquid outlet, a light component outlet 4, a heavy component outlet 5 and an exhaust gas outlet 3; the waste gas outlet 3 is arranged at one end of the top of the horizontal container 1, the longitudinal baffle 6 is vertically arranged in the middle of the horizontal container 1, one end and two sides of the longitudinal baffle 6 are fixedly connected with the inner wall of the horizontal container 1, and a gap is reserved between one end of the corresponding waste gas outlet 3 and the inner wall of the horizontal container 1.
The internal space of the horizontal container 1 at two sides of the longitudinal partition plate 6 is respectively provided with a reaction section I and a separation section II; wherein the reaction section I is provided with a raw material inlet 2 at one end of the bottom part far away from the waste gas outlet 3. In the embodiment, 3 groups of anti-blocking spray heads 7 are longitudinally arranged in the reaction section I; the liquid inlet ends of each group of anti-blocking spray heads 7 are connected with a circulating liquid outlet through a circulating liquid pipeline, a circulating pump 10 and a jet pump 11 are arranged on the circulating liquid pipeline, and the jet pump 11 is provided with a raw material gas inlet.
In this embodiment, the number of the nozzles in the 3 groups of anti-blocking nozzles 7 is different, and along the flow direction of the liquid raw material, the number of the nozzles in the 3 groups of anti-blocking nozzles is 7, 5 and 3, respectively, and the injection direction of the nozzles is the same as the flow direction of the liquid raw material.
In this embodiment, 3 groups of inclined guide plates are longitudinally arranged in the separation section II, each group of inclined guide plates consists of 2 guide plates, and each group of inclined guide plates are equidistantly and alternately arranged and are parallel to the 2 guide plates.
The separation section II is provided with a diaphragm plate 9 at one end far away from the waste gas outlet, the diaphragm plate 9 is vertically arranged, one end of the diaphragm plate 9 is connected with the longitudinal diaphragm plate 6, the other end of the diaphragm plate is connected with the inner wall of the horizontal container 1, an upper notch 12 is reserved between the top of the diaphragm plate 9 and the top of the horizontal container 1, and a lower notch 13 is reserved between the bottom of the diaphragm plate 9 and the bottom of the horizontal container 1; the horizontal container 1 is provided with a light component outlet 4 at the upper part of one end far away from the waste gas outlet 3, and a heavy component outlet 5 at the bottom.
The foregoing is only a preferred embodiment of the present utility model, but the scope of the present utility model is not limited thereto, and any person skilled in the art, who is within the scope of the present utility model, should make equivalent substitutions or modifications according to the technical scheme of the present utility model and the inventive concept thereof, and should be covered by the scope of the present utility model.
Claims (3)
1. A reaction separator for improving the purity and yield of products comprises a horizontal container, a circulating pump, a jet pump, an anti-blocking nozzle, an inclined guide plate and a baffle plate; the horizontal container is provided with a raw material inlet, a circulating liquid outlet, a light component outlet, a heavy component outlet and a waste gas outlet; the partition board is characterized by comprising a longitudinal partition board and a transverse partition board; the waste gas outlet is arranged at one end of the top of the horizontal container, the longitudinal partition plate is vertically arranged in the middle of the horizontal container, one end and two sides of the longitudinal partition plate are fixedly connected with the inner wall of the horizontal container, and a gap is reserved between one end of the corresponding waste gas outlet and the inner wall of the horizontal container; the internal space of the horizontal container at two sides of the longitudinal partition plate is respectively a reaction section and a separation section; wherein, the reaction section is provided with a raw material inlet at one end far away from the bottom of the waste gas outlet, and a plurality of groups of anti-blocking spray heads are longitudinally arranged in the reaction section; the liquid inlet end of each group of anti-blocking spray heads is connected with a circulating liquid outlet through a circulating liquid pipeline, a circulating pump and a jet pump are arranged on the circulating liquid pipeline, and the jet pump is provided with a raw material gas inlet; a plurality of groups of inclined guide plates are longitudinally arranged in the separation section, a diaphragm is arranged at one end of the separation section, which is far away from the waste gas outlet, the diaphragm is vertically arranged, one end of the diaphragm is connected with the longitudinal diaphragm, the other end of the diaphragm is connected with the inner wall of the horizontal container, an upper notch is reserved between the top of the diaphragm and the top of the horizontal container, and a lower notch is reserved between the bottom of the diaphragm and the bottom of the horizontal container; the upper part of one end of the horizontal container far away from the waste gas outlet is provided with a light component outlet, and the bottom is provided with a heavy component outlet.
2. The reaction separator for improving the purity and the yield of products according to claim 1, wherein the spraying direction of the anti-blocking spray head is the same as the flowing direction of the liquid raw material.
3. The reaction separator of claim 1, wherein the plurality of inclined baffles are disposed at equal intervals.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321354093.9U CN219849642U (en) | 2023-05-30 | 2023-05-30 | Reaction separator for improving product purity and yield |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321354093.9U CN219849642U (en) | 2023-05-30 | 2023-05-30 | Reaction separator for improving product purity and yield |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219849642U true CN219849642U (en) | 2023-10-20 |
Family
ID=88316559
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321354093.9U Active CN219849642U (en) | 2023-05-30 | 2023-05-30 | Reaction separator for improving product purity and yield |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219849642U (en) |
-
2023
- 2023-05-30 CN CN202321354093.9U patent/CN219849642U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN219849642U (en) | Reaction separator for improving product purity and yield | |
| CN112473613A (en) | Atomizing gas-liquid two-phase reaction device | |
| CN116586024A (en) | Reaction separator for improving product purity and yield and working method thereof | |
| CN101984099B (en) | On-line degassing device for aluminium melt | |
| CN219849641U (en) | Do benefit to reaction separator of light and heavy components separation | |
| CN218812136U (en) | Gas-liquid separator for water electrolysis hydrogen production | |
| CN206081788U (en) | High -efficient backwash filter and have device's multiple -layer filtering ware | |
| CN110694450A (en) | Water spraying waste gas purification device for biomass power generation purification treatment equipment | |
| GB2031747A (en) | Gas-liquid dissolving tank | |
| CN116617996A (en) | Reaction separator beneficial to separation of light components and heavy components and working method thereof | |
| CN206168433U (en) | Ethoxy - apparatus for producing | |
| CN218871825U (en) | Gas-liquid mixing device | |
| CN209885771U (en) | Partition plate type vinyl ether product reactor | |
| CN211754834U (en) | Horizontal reaction separator integrating reaction and separation functions | |
| CN102600788B (en) | Multi-stage spray reaction tower | |
| CN112474087A (en) | Liquid distributor, multistage efficient distributor and washing liquid spraying method | |
| CN110975770A (en) | Decomposition process and device of phenate in coal tar processing process | |
| CN210410000U (en) | Washing tower with uniform airflow distribution | |
| CN207169653U (en) | A kind of inlet diffuser | |
| CN219964497U (en) | Horizontal spray tower | |
| CN110947343A (en) | Horizontal reaction separator integrating reaction and separation functions | |
| CN209952514U (en) | Wood-based plate tail gas cleanup unit | |
| CN115161659B (en) | Circulating gas injection type alkaline water electrolysis gas-liquid separation system and working method thereof | |
| SU1586738A1 (en) | Installation for producing phosphoric acid | |
| CN220176829U (en) | Adjust tuning tower of nitrite ratio |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |