CN219808042U - Electrostatic spinning device - Google Patents
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Abstract
Description
技术领域Technical field
本实用新型涉及静电纺丝技术领域,尤其是指一种静电纺丝装置。The utility model relates to the technical field of electrospinning, in particular to an electrostatic spinning device.
背景技术Background technique
静电纺丝技术是一种应用广泛的纳米纤维制备方法,聚合物溶液或熔体在强电场力的作用下喷射纺丝,制备出的纤维具有直径小、比表面积大和孔隙率高等特点,具有多功能性和广阔的应用背景,受到广泛的关注。但单一的静电纺膜难以满足某个领域对于膜各个方面的需求,故需对静电纺膜进行改性,现常见的改性方法包括混纺,浸涂和热压。现浸涂和热压法制备改性纤维膜,需要人为的将纤维膜取下来放进浸涂溶液中进行浸涂,或者将纺好的纤维膜放入热压辊之间,在人为操作过程很容易破坏静电纺膜,整个过程需人工看守及时取膜热压等,具有生产效率低的缺陷。此外,传统的储液槽仅靠边缘喷丝,喷出的聚合物细流较少,难以实现批量制备静电纺膜。Electrospinning technology is a widely used method for preparing nanofibers. A polymer solution or melt is spray-spun under the action of a strong electric field. The fibers produced have the characteristics of small diameter, large specific surface area and high porosity. They have many properties. Functional and broad application background, it has received widespread attention. However, it is difficult for a single electrospun membrane to meet the needs of all aspects of membranes in a certain field, so the electrospun membrane needs to be modified. Common modification methods include blending, dip coating and hot pressing. The modified fiber membrane is prepared by dipping and hot pressing. It is necessary to manually remove the fiber membrane and put it into the dip coating solution for dip coating, or to put the spun fiber membrane between the hot pressing rollers. During the manual operation process It is easy to damage the electrospun membrane, and the entire process requires manual supervision to remove the membrane and heat press it in time, which has the disadvantage of low production efficiency. In addition, the traditional liquid storage tank only relies on edge spinning, and the small flow of polymer ejected is small, making it difficult to prepare electrospun membranes in batches.
实用新型内容Utility model content
本实用新型所要解决的技术问题在于克服现有技术中存在的不足,提供一种静电纺丝装置,其实现了智能化制备静电纺纳米纤维,极大地提高了静电纺丝的效率,同时也节约了人工成本。The technical problem to be solved by this utility model is to overcome the deficiencies in the existing technology and provide an electrospinning device, which realizes the intelligent preparation of electrospun nanofibers, greatly improves the efficiency of electrospinning, and also saves money. labor costs.
按照本实用新型提供的技术方案,所述静电纺丝装置包括储液器,所述储液器上设有纺丝喷出口;浸液槽,用于放置浸涂溶液;自转滚筒,所述自转滚筒与第一驱动装置相连;运动控制装置,与所述自转滚筒相连,用于控制所述自转滚筒沿设定轨迹运动;刮板,所述刮板与所述浸液槽旋转连接,所述刮板与第二驱动装置相连,所述第二驱动装置控制刮板刮取所述自转滚筒上的纺丝。According to the technical solution provided by the present utility model, the electrospinning device includes a liquid reservoir, which is provided with a spinning nozzle; a liquid immersion tank for placing the dipping solution; and a rotating drum. The drum is connected to the first driving device; a motion control device is connected to the rotation drum and is used to control the movement of the rotation drum along the set trajectory; the scraper is rotatably connected to the immersion tank, and the scraper is rotatably connected to the immersion tank. The scraper is connected to a second driving device, and the second driving device controls the scraper to scrape the spinning fiber on the rotating drum.
在本实用新型的一个实施例中,所述运动控制装置包括控制器、两个转盘以及连接杆,所述两个转盘分别通过连接杆连接在所述自转滚筒两端,所述两个转盘通过所述控制器驱动旋转。In one embodiment of the present invention, the motion control device includes a controller, two turntables and a connecting rod. The two turntables are connected to both ends of the rotation drum through connecting rods. The two turntables pass through The controller drives the rotation.
在本实用新型的一个实施例中,所述连接杆包括第一连接杆以及第二连接杆,所述第一连接杆一端连接在所述转盘上,另一端与所述第二连接杆连接,所述第二连接杆沿所述自转滚筒的轴线穿设所述自转滚筒,所述第一连接杆为伸缩杆。In one embodiment of the present invention, the connecting rod includes a first connecting rod and a second connecting rod. One end of the first connecting rod is connected to the turntable, and the other end is connected to the second connecting rod. The second connecting rod passes through the rotating drum along the axis of the rotating drum, and the first connecting rod is a telescopic rod.
在本实用新型的一个实施例中,所述自转滚筒包括第一滚筒以及第二滚筒,所述第一滚筒以及第二滚筒均位于所述两个转盘之间,并与两个转盘连接。In one embodiment of the present invention, the rotating drum includes a first drum and a second drum. The first drum and the second drum are both located between the two turntables and connected to the two turntables.
在本实用新型的一个实施例中,还包括气流通道,所述气流通道环绕所述储液器下端。In one embodiment of the present invention, an air flow channel is further included, and the air flow channel surrounds the lower end of the liquid reservoir.
在本实用新型的一个实施例中,所述浸液槽槽口边缘连接有传送带,所述传送带与所述刮板相对应,所述传送带远离所述浸液槽的一端设有热压辊。In one embodiment of the present invention, a conveyor belt is connected to the edge of the slot of the immersion tank, and the conveyor belt corresponds to the scraper. A hot pressing roller is provided at one end of the conveyor belt away from the immersion tank.
在本实用新型的一个实施例中,所述热压辊包括第一热压辊以及第二热压辊,所述第一热压辊以及第二热压辊分别位于所述传送带的正反两面。In one embodiment of the present invention, the heat pressure roller includes a first heat pressure roller and a second heat pressure roller, and the first heat pressure roller and the second heat pressure roller are respectively located on the front and back sides of the conveyor belt. .
在本实用新型的一个实施例中,所述刮板的长度与所述自转滚筒的轴线长度相一致。In one embodiment of the present invention, the length of the scraper is consistent with the length of the axis of the rotating drum.
在本实用新型的一个实施例中,所述储液器的内径沿储液口指向纺丝喷出口方向逐渐减小。In one embodiment of the present invention, the inner diameter of the liquid reservoir gradually decreases along the direction from the liquid storage port to the spinning nozzle.
在本实用新型的一个实施例中,所述刮板一侧通过转轴连接在所述浸液槽的槽口边缘。In one embodiment of the present invention, one side of the scraper is connected to the edge of the slot of the liquid immersion tank through a rotating shaft.
本实用新型的上述技术方案相比现有技术具有以下优点:The above technical solution of the present invention has the following advantages compared with the existing technology:
本实用新型所述的静电纺丝装置设有自转滚筒,储液器的纺丝喷出口喷出纺丝后,纺丝落至自转滚筒上,自转滚筒被运动控制装置驱动在浸液槽和储液器之间往复运动,实现自动浸涂,本实用新型静电纺丝装置还设有传动带和热压辊,刮板将自动滚筒上的纺丝刮至传送带上,然后由热压辊热压实现自动热压,纺丝过程中不需要关闭电源再手动的取出纤维膜进行浸涂或热压,实现了智能化制备静电纺纳米纤维,极大地提高了静电纺丝的效率,同时也节约了人工成本,使得纺丝更加智能化、便捷化。The electrospinning device described in the utility model is equipped with a rotating drum. After the spinning nozzle of the liquid reservoir ejects the spinning yarn, the spinning yarn falls on the rotating drum. The rotating drum is driven by the motion control device between the immersion tank and the storage tank. The reciprocating movement between the liquid containers realizes automatic dipping. The electrospinning device of this utility model is also equipped with a transmission belt and a hot pressing roller. The scraper scrapes the spinning fiber on the automatic roller to the conveyor belt, and then the hot pressing roller performs hot pressing. Automatic hot pressing. During the spinning process, there is no need to turn off the power and manually take out the fiber membrane for dip coating or hot pressing. This realizes the intelligent preparation of electrospun nanofibers, greatly improves the efficiency of electrospinning, and also saves labor. cost, making spinning more intelligent and convenient.
附图说明Description of the drawings
为了使本实用新型的内容更容易被清楚的理解,下面根据本实用新型的具体实施例并结合附图,对本实用新型作进一步详细的说明。In order to make the content of the present utility model easier to understand clearly, the utility model will be further described in detail below based on specific embodiments of the utility model and in conjunction with the accompanying drawings.
图1是本实用新型静电纺丝装置去除热压装置后的结构示意图;Figure 1 is a schematic structural diagram of the electrospinning device of the present invention without the hot pressing device;
图2是本实用新型浸液槽与热压装置的连接示意图。Figure 2 is a schematic diagram of the connection between the liquid immersion tank and the hot pressing device of the present invention.
说明书附图标记说明:1-储液器;2-气流通道;3-转盘;4-自转滚筒;5-控制器;6-连接杆;7-浸液槽;8-刮板;9-高压电源;10-转轴;11-传送带;12-热压辊;13-热压开关。Explanation of reference symbols in the manual: 1-liquid reservoir; 2-air flow channel; 3-turntable; 4-rotating drum; 5-controller; 6-connecting rod; 7-immersion tank; 8-scraper; 9-high pressure Power supply; 10-rotating shaft; 11-conveyor belt; 12-heat pressing roller; 13-heat pressing switch.
具体实施方式Detailed ways
下面结合附图和具体实施例对本实用新型作进一步说明,以使本领域的技术人员可以更好地理解本实用新型并能予以实施,但所举实施例不作为对本实用新型的限定。The present utility model will be further described below in conjunction with the accompanying drawings and specific embodiments, so that those skilled in the art can better understand the present utility model and implement it, but the embodiments are not intended to limit the present utility model.
参照图1所示,为了提高了静电纺丝的效率,节约人工成本,本实用新型包括储液器1,所述储液器1上设有纺丝喷出口;浸液槽7,用于放置浸涂溶液;自转滚筒4,所述自转滚筒4与第一驱动装置相连;运动控制装置,与所述自转滚筒4相连,用于控制所述自转滚筒4沿设定轨迹运动;刮板8,所述刮板8与所述浸液槽7旋转连接,所述刮板8与第二驱动装置相连,所述第二驱动装置控制刮板8刮取所述自转滚筒4上的纺丝。Referring to Figure 1, in order to improve the efficiency of electrospinning and save labor costs, the utility model includes a liquid reservoir 1, which is provided with a spinning nozzle; a liquid immersion tank 7 for placing Dip coating solution; rotation drum 4, the rotation drum 4 is connected to the first driving device; a motion control device, connected to the rotation drum 4, is used to control the movement of the rotation drum 4 along the set trajectory; scraper 8, The scraper 8 is rotatably connected to the immersion tank 7 , and the scraper 8 is connected to a second driving device. The second driving device controls the scraper 8 to scrape the spinning yarn on the rotating drum 4 .
具体地,在静电纺丝的过程中,首先在储液器1中选择性地倒入一定量的纺丝液,所述储液器1的内径沿储液口指向纺丝喷出口方向逐渐减小,然后打开高压电源9进行纺丝,盛有纺丝液的储液器1边缘会纺出连续不断的丝,自转滚筒4在纺丝过程中先在纺丝喷出口下接受纺丝,接收到期望厚度的时候自转滚筒4由运动控制装置转到浸液槽7内,以进行浸涂处理。所述刮板8一侧通过转轴10连接在所述浸液槽7的槽口,浸涂后,刮板8通过转轴10向上旋转,以与自转滚筒4相抵,所述刮板8的长度与所述自转滚筒4的轴线长度相一致,通过自转滚筒4的自转将纤维膜从自转滚筒4表面刮下,实现自动浸涂。Specifically, during the electrospinning process, a certain amount of spinning liquid is first selectively poured into the liquid reservoir 1, and the inner diameter of the liquid reservoir 1 gradually decreases along the liquid storage port toward the spinning nozzle. small, then turn on the high-voltage power supply 9 for spinning, the edge of the liquid reservoir 1 containing the spinning liquid will spin out continuous silk, the rotating drum 4 first receives the spinning under the spinning nozzle during the spinning process, and then receives When the desired thickness is reached, the rotating drum 4 is transferred to the immersion tank 7 by the motion control device to perform the dip coating process. One side of the scraper 8 is connected to the notch of the immersion tank 7 through the rotating shaft 10. After dipping, the scraper 8 rotates upward through the rotating shaft 10 to offset the rotating drum 4. The length of the scraper 8 is equal to The axis lengths of the rotating drums 4 are consistent, and the fiber film is scraped off the surface of the rotating drum 4 through the rotation of the rotating drum 4, thereby realizing automatic dip coating.
具体实施时,第一驱动装置用于驱动自转滚筒4自转,当自转滚筒4运动至设定轨迹的第一区域时,所述自转滚筒接收所述储液器1喷出的纺丝,当所述自转滚筒4运动至设定轨迹的第二区域时,所述自转滚筒将其上的纺丝传输至所述浸液槽7内,当所述自转滚筒4运动至设定位置时,控制所述刮板8运动,刮取所述自转滚筒4上的纺丝。During specific implementation, the first driving device is used to drive the autorotating drum 4 to rotate. When the autorotating drum 4 moves to the first area of the set trajectory, the autorotating drum receives the spinning yarn ejected from the liquid reservoir 1. When the autorotating drum 4 moves to the first area of the set trajectory, When the autorotating drum 4 moves to the second area of the set trajectory, the autorotating drum transfers the spinning fiber to the immersion tank 7. When the autorotating drum 4 moves to the set position, all the spinning drums are controlled. The scraper 8 moves to scrape the spinning yarn on the rotating drum 4.
进一步地,所述运动控制装置包括控制器5、两个转盘3以及连接杆6,所述两个转盘3分别通过连接杆6连接在所述自转滚筒4两端,所述两个转盘3通过所述控制器5驱动旋转。Further, the motion control device includes a controller 5, two turntables 3 and a connecting rod 6. The two turntables 3 are connected to both ends of the rotation drum 4 through the connecting rods 6. The two turntables 3 pass through The controller 5 drives the rotation.
具体地,控制器5驱动两个转盘3旋转,两个转盘3的旋转方向与旋转速度相一致,自转滚筒4连接在两个转盘3之间,随转盘3的自转而做圆周运动,所述自转滚筒4设定轨迹的第一区域与所述储液器1的纺丝喷出口相对应,所述自转滚筒4设定轨迹的第二区域与所述浸液槽7相对应,以实现所需的自动浸涂。Specifically, the controller 5 drives the two turntables 3 to rotate, and the rotation direction of the two turntables 3 is consistent with the rotation speed. The rotation drum 4 is connected between the two turntables 3 and makes a circular motion with the rotation of the turntables 3. The first area of the set trajectory of the rotary drum 4 corresponds to the spinning nozzle of the liquid reservoir 1, and the second area of the set trajectory of the autorotating drum 4 corresponds to the immersion tank 7 to achieve the desired results. Automatic dipping required.
进一步地,所述连接杆6包括第一连接杆6以及第二连接杆6,所述第一连接杆6一端连接在所述转盘3上,另一端与所述第二连接杆6连接,所述第二连接杆6沿所述自转滚筒4的轴线穿设所述自转滚筒4,所述第一连接杆6为伸缩杆。Further, the connecting rod 6 includes a first connecting rod 6 and a second connecting rod 6. One end of the first connecting rod 6 is connected to the turntable 3, and the other end is connected to the second connecting rod 6. The second connecting rod 6 passes through the rotating drum 4 along the axis of the rotating drum 4, and the first connecting rod 6 is a telescopic rod.
具体地,位于自转滚筒4两侧的转盘3上均设有第一连接杆6,两个转盘3的第一连接杆6通过第二连接杆6连接,第二连接杆6上穿设有自转滚筒4,当浸涂完成后,刮板8旋转与自转滚筒4相抵,将纺丝刮落,可通过调节可伸缩的第一连接杆6使自转滚筒4延伸出浸液槽7槽口外的位置,使纺丝刮落至所需的位置。Specifically, the turntables 3 located on both sides of the rotating drum 4 are provided with first connecting rods 6. The first connecting rods 6 of the two turntables 3 are connected through the second connecting rods 6. The second connecting rods 6 are provided with self-rotating rods 6. Drum 4, when the dip coating is completed, the scraper 8 rotates against the rotating drum 4 to scrape off the spinning yarn. The rotating drum 4 can be extended out of the notch of the immersion tank 7 by adjusting the retractable first connecting rod 6. , so that the spinning fiber is scraped to the desired position.
进一步地,所述自转滚筒4包括第一滚筒以及第二滚筒,所述第一滚筒以及第二滚筒均位于所述两个转盘3之间,并与两个转盘3连接。Further, the rotating drum 4 includes a first drum and a second drum. The first drum and the second drum are both located between the two turntables 3 and connected to the two turntables 3 .
具体地,第一滚筒和第二滚筒可分别设置在自转滚筒4圆周运动轨道位于同一直线的两个顶点上,采用此种结构,可以在静电纺丝过程中,使一个滚筒在上方接收纺丝,同时另一个滚筒在下方完成浸涂,大大提高纺丝和浸涂的效率。当然,自转滚筒4的数量以及排布结构也可以时其他形式,具体可根据实际需要选择,具体以满足自动浸涂的目的为准。Specifically, the first roller and the second roller can be respectively arranged at the two vertices of the same straight line on the circular motion track of the rotating drum 4. With this structure, one roller can receive the spinning fiber from above during the electrospinning process. , while another roller completes dip coating below, greatly improving the efficiency of spinning and dip coating. Of course, the number and arrangement structure of the rotating drums 4 can also be in other forms, which can be selected according to actual needs and specifically to meet the purpose of automatic dip coating.
进一步地,还包括气流通道2,所述气流通道2环绕所述储液器1下端。Furthermore, it also includes an air flow channel 2 surrounding the lower end of the liquid reservoir 1 .
具体地,打开高压电源9进行纺丝,盛有纺丝液的储液器1边缘会纺出连续不断的丝,往气流通道2中输入热气流,热气流不断从外界输入经过气流通道2在纺丝喷出口处产生一定的压强,以促进喷丝。在喷丝的过程中,不断输送热气流到纺丝喷出口处,使得喷丝口处压强增大,相比于普通静电纺丝装置喷出的丝更加细密,促进纺丝过程的进行,提高纺丝效率。Specifically, when the high-voltage power supply 9 is turned on for spinning, continuous yarn will be spun from the edge of the liquid reservoir 1 containing the spinning solution, and hot air flow is input into the air flow channel 2. The hot air flow is continuously input from the outside through the air flow channel 2. A certain pressure is generated at the spinning nozzle to promote spinning. During the spinning process, the hot air flow is continuously transported to the spinning nozzle, which increases the pressure at the spinning nozzle. Compared with the ordinary electrospinning device, the filaments ejected are finer, which promotes the spinning process and improves the spinning process. Spinning efficiency.
进一步地,所述浸液槽7槽口边缘连接有传送带11,所述传送带11与所述刮板8相对应,所述传送带11远离所述浸液槽7的一端设有热压辊12。Further, a conveyor belt 11 is connected to the edge of the liquid immersion tank 7 , and the conveyor belt 11 corresponds to the scraper 8 . A hot pressing roller 12 is provided at one end of the conveyor belt 11 away from the liquid immersion tank 7 .
所述热压辊12包括第一热压辊12以及第二热压辊12,所述第一热压辊12以及第二热压辊12分别位于所述传送带11的正反两面。The heat press roller 12 includes a first heat press roller 12 and a second heat press roller 12 . The first heat press roller 12 and the second heat press roller 12 are respectively located on the front and back sides of the conveyor belt 11 .
具体地,打开热压开关13,从自动滚筒上刮下的纤维膜经过传动带运送到热压辊12之间进行热压。Specifically, the heat pressing switch 13 is turned on, and the fiber film scraped off from the automatic roller is transported to between the heat pressing rollers 12 through the transmission belt for heat pressing.
本实用新型设有自动浸涂和自动热压装置,纺丝过程中不需要关闭电源再手动的取出纤维膜进行浸涂或热压,实现了智能化制备静电纺纳米纤维,极大地提高了静电纺丝的效率,同时也节约了人工成本。存在某些薄膜不需要浸涂或热压,那么此时浸液槽7里不装有液体或热压辊12不施加压力,即可实现对静电纺薄膜进行选择性控制处理。The utility model is equipped with automatic dipping and automatic hot pressing devices. During the spinning process, there is no need to turn off the power and manually take out the fiber membrane for dip coating or hot pressing. This realizes the intelligent preparation of electrospun nanofibers and greatly improves the electrostatic efficiency. The efficiency of spinning also saves labor costs. There are some films that do not require dip coating or hot pressing. If there is no liquid in the immersion tank 7 or no pressure is applied by the hot pressing roller 12, the electrospun film can be selectively controlled and processed.
显然,上述实施例仅仅是为清楚地说明所作的举例,并非对实施方式的限定。对于所属领域的普通技术人员来说,在上述说明的基础上还可以做出其它不同形式变化或变动。这里无需也无法对所有的实施方式予以穷举。而由此所引申出的显而易见的变化或变动仍处于本实用新型创造的保护范围之中。Obviously, the above-mentioned embodiments are only examples for clear explanation and are not intended to limit the implementation. For those of ordinary skill in the art, other changes or modifications may be made based on the above description. An exhaustive list of all implementations is neither necessary nor possible. The obvious changes or changes derived therefrom are still within the protection scope of the invention.
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