CN219745663U - Azodiisobutyronitrile oxidation centrifugal spraying and leaching device - Google Patents
Azodiisobutyronitrile oxidation centrifugal spraying and leaching device Download PDFInfo
- Publication number
- CN219745663U CN219745663U CN202321015308.4U CN202321015308U CN219745663U CN 219745663 U CN219745663 U CN 219745663U CN 202321015308 U CN202321015308 U CN 202321015308U CN 219745663 U CN219745663 U CN 219745663U
- Authority
- CN
- China
- Prior art keywords
- case
- connecting pipe
- azodiisobutyronitrile
- oxidation
- mounting panel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 title claims abstract description 60
- 238000002386 leaching Methods 0.000 title claims abstract description 15
- 230000003647 oxidation Effects 0.000 title claims abstract description 14
- 238000007254 oxidation reaction Methods 0.000 title claims abstract description 14
- 238000005507 spraying Methods 0.000 title abstract description 7
- 238000004080 punching Methods 0.000 claims abstract description 19
- 238000005119 centrifugation Methods 0.000 claims abstract description 3
- 239000007921 spray Substances 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 abstract description 22
- 239000007788 liquid Substances 0.000 abstract description 5
- 238000005406 washing Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000001035 drying Methods 0.000 abstract 1
- 238000007599 discharging Methods 0.000 description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000018044 dehydration Effects 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 230000004308 accommodation Effects 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 241001330002 Bambuseae Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003505 polymerization initiator Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- Centrifugal Separators (AREA)
Abstract
The utility model relates to the technical field of azodiisobutyronitrile production and discloses an azodiisobutyronitrile oxidation centrifugal spraying and leaching device which comprises a base, wherein the top of the base is provided with a containing box, the inside of the containing box is provided with a punching and cleaning box, the top of the punching and cleaning box is communicated with a second connecting pipe, and the top of the second connecting pipe penetrates into the first mounting plate and is in rotary connection with the first mounting plate through a bearing. This azobisisobutyronitrile oxidation centrifugation spouts leaching device holds the washing liquid through the setting of holding the case, and the setting through punching a hole washs the case and realize holding the washing to azobisisobutyronitrile, and the setting through the second connecting pipe is to absorb and washs the case and carry out fixed connection, realizes the drive arrangement to the drive that washs the case that punches a hole when leading-in to the inside washs the case that punches a hole of azobisisobutyronitrile to realize wasing centrifugal spin-drying to azobisisobutyronitrile.
Description
Technical Field
The utility model relates to the technical field of azodiisobutyronitrile production, in particular to an azodiisobutyronitrile oxidation centrifugal spraying and leaching device.
Background
Azobisisobutyronitrile (AIBN), which is an organic compound having a chemical formula of C8H12N4, is white crystalline powder, is insoluble in water, is soluble in various organic solvents such as ethanol, diethyl ether, toluene, methanol, etc., is mainly used as a foaming agent for rubber, plastic, etc., and a polymerization initiator, and can also be used for organic synthesis.
The utility model provides an azo-bis-isobutyronitrile need wash it when producing and spray and carry out centrifugal dehydration to it, as the device of an automated production azo-bis-isobutyronitrile that patent number is CN214765435U discloses, and it is through including the cauldron body and kerve, the kerve inner bottom surface is equipped with the cauldron body through the landing leg mount, and the internal internally mounted of cauldron has the stirring rake to cauldron body top surface central point puts fixed mounting and has driving motor, the stirring rake top surface runs through cauldron body top surface and is connected with driving motor output, cauldron body one side is erect the intake pipe, and the intake pipe surface link up and be connected with the shunt tubes to the shunt tubes runs through the cauldron body and is connected with the cauldron body link up, the ring canal has been erect to the inside top of the cauldron body, and the ring canal bottom surface link up and be connected with the inlet tube, horizontal fixed mounting has the mounting panel between the landing leg, and the vertical fixed mounting of mounting panel top surface has first cylinder to the piston rod top surface fixedly connected with of first cylinder, it has the filter screen to go up the central point put fixedly to install the filter screen, and be for the structure of inversion section of thick bamboo to run through cauldron body top surface and insert into the cauldron body bottom surface, the inside filter screen, the filter screen inside is connected with the filter screen, can not realize the realization when using the plug is realized in the plug, but can's the realization is difficult to use in the plug, and the realization is used to the plug.
In order to solve the problems, the improvement is provided, and an azodiisobutyronitrile oxidation centrifugal spraying and leaching device is provided.
Disclosure of Invention
The utility model aims to provide an azodiisobutyronitrile oxidation centrifugal spraying and leaching device, which aims to solve the problems in the background technology.
In order to achieve the above purpose, the present utility model provides the following technical solutions:
the utility model provides an azodiisobutyronitrile oxidation centrifugation spouts leaching device, includes the base, the top of base is provided with the accommodation box, the inside of accommodation box is provided with the washing case that punches a hole, the top intercommunication of washing case that punches a hole has the second connecting pipe, the top of second connecting pipe runs through to the inside of first mounting panel and rotates through the bearing between being connected with first mounting panel, the top of washing case that punches a hole is provided with first mounting panel, the top of first mounting panel is provided with drive arrangement, the top of first mounting panel and the top that is located drive arrangement are provided with the second mounting panel, the top fixed mounting of second mounting panel has the holding dish;
the driving device comprises a motor arranged at the top of the first mounting plate, a first gear fixedly arranged at the outer side of the second connecting pipe and a second gear fixedly arranged on an output shaft of the motor, and the second gear is meshed with the first gear.
As still further aspects of the utility model: the top fixed mounting of base has four first bracing pieces, the top of first bracing piece and the bottom fixed connection of first mounting panel, the outside of holding the case and the inboard fixed connection of first bracing piece.
As still further aspects of the utility model: the bottom intercommunication that washs the case punches a hole has first connecting pipe, first connecting pipe runs through the holding case and extends to the bottom that holds the case, the outside cover of first connecting pipe is equipped with mechanical seal, mechanical seal's outside and holding case fixed connection.
As still further aspects of the utility model: the bottom fixed mounting of first connecting pipe has rotary joint, rotary joint's bottom intercommunication has row material pipe, row material pipe's end extends to the left side of base left.
As still further aspects of the utility model: four second support rods are fixedly arranged at the top of the first mounting plate, and the top of each second support rod is fixedly connected with the bottom of the second mounting plate.
As still further aspects of the utility model: the bottom of holding the dish is connected with the hose, the bottom of hose runs through to the inside of second connecting pipe, the inside fixed mounting of hose has the motorised valve.
As still further aspects of the utility model: the bottom of base fixed mounting has four supporting seats, the bottom intercommunication on holding case right side has the drain pipe.
Compared with the prior art, the utility model has the beneficial effects that:
1. according to the utility model, the cleaning liquid is contained through the arrangement of the containing box, the azobisisobutyronitrile is contained and cleaned through the arrangement of the punching and cleaning box, the punching and cleaning box is fixedly connected through the second connecting pipe, the azobisisobutyronitrile is led into the inside of the punching and cleaning box, and meanwhile, the driving of the punching and cleaning box by the driving device is realized, so that the azobisisobutyronitrile is cleaned and centrifugally dried.
2. According to the utility model, the first mounting plate and the accommodating box are mounted through the arrangement of the first supporting rod, the stability of the accommodating box is improved, the centrifugally dried azodiisobutyronitrile is discharged through the cooperation between the first connecting pipe and the discharging pipe, the connection between the discharging pipe and the first connecting pipe is realized through the arrangement of the rotary joint, the rotation of the first connecting pipe relative to the discharging pipe is realized, the second mounting plate is supported through the arrangement of the second supporting rod, the driving device is convenient to mount, the azodiisobutyronitrile in the accommodating vessel is led into the punching cleaning box through the arrangement of the hose, and the cleaning liquid is discharged through the arrangement of the drain pipe.
Drawings
FIG. 1 is a schematic structural view of an azodiisobutyronitrile oxidative centrifugal spray rinsing device;
FIG. 2 is a schematic diagram of the front structure of an azodiisobutyronitrile oxidative centrifugal spray device;
FIG. 3 is a schematic view of the structure of an isometric section of an azodiisobutyronitrile oxidative centrifugal spray device;
fig. 4 is an enlarged schematic view of the structure of the azodiisobutyronitrile oxidized centrifugal spray device at a position a in fig. 3.
In the figure: 1. a base; 2. a first support bar; 3. a housing box; 4. punching a cleaning box; 5. a first mounting plate; 6. a second support bar; 7. a second mounting plate; 8. a holding vessel; 9. a drain pipe; 10. a discharge pipe; 11. a rotary joint; 12. a first connection pipe; 13. a hose; 14. a second connection pipe; 15. a driving device; 151. a motor; 152. a first gear; 153. a second gear; 16. a support base; 17. and (5) mechanical sealing.
Detailed Description
Referring to fig. 1-4, an azodiisobutyronitrile oxidizing centrifugal spraying and leaching device comprises a base 1, wherein a containing box 3 is arranged at the top of the base 1, a punching and cleaning box 4 is arranged in the containing box 3, a second connecting pipe 14 is communicated with the top of the punching and cleaning box 4, the top of the second connecting pipe 14 penetrates into the first mounting plate 5 and is rotationally connected with the first mounting plate 5 through a bearing, the top of the punching and cleaning box 4 is provided with the first mounting plate 5, a driving device 15 is arranged at the top of the first mounting plate 5, a second mounting plate 7 is arranged at the top of the first mounting plate 5 and above the driving device 15, and a containing dish 8 is fixedly arranged at the top of the second mounting plate 7;
the driving device 15 includes a motor 151 mounted on the top of the first mounting plate 5, a first gear 152 fixedly mounted on the outer side of the second connection pipe 14, and a second gear 153 fixedly mounted on the output shaft of the motor 151, and the second gear 153 is meshed with the first gear 152.
Specifically, four first support rods 2 are fixedly arranged at the top of the base 1, the top of each first support rod 2 is fixedly connected with the bottom of the first mounting plate 5, and the outer side of the containing box 3 is fixedly connected with the inner side of each first support rod 2.
Through above-mentioned technical scheme, realize installing first mounting panel 5 and holding case 3 through the setting of first bracing piece 2, increase the stability of holding case 3.
Specifically, the bottom intercommunication of punching cleaning case 4 has first connecting pipe 12, and first connecting pipe 12 runs through and holds case 3 and extends to the bottom that holds case 3, and the outside cover of first connecting pipe 12 is equipped with mechanical seal 17, and mechanical seal 17's the outside and hold case 3 fixed connection.
Through the above technical scheme, the azobisisobutyronitrile which is centrifugally dried is discharged through the cooperation between the first connecting pipe 12 and the discharging pipe 10.
Specifically, a rotary joint 11 is fixedly installed at the bottom of the first connecting pipe 12, a discharge pipe 10 is communicated with the bottom of the rotary joint 11, and the tail end of the discharge pipe 10 extends leftwards to the left side of the base 1.
Through the above technical solution, the connection between the discharge pipe 10 and the first connecting pipe 12 is realized through the arrangement of the rotary joint 11, and the rotation of the first connecting pipe 12 relative to the discharge pipe 10 is realized.
Specifically, four second support rods 6 are fixedly arranged at the top of the first mounting plate 5, and the top of each second support rod 6 is fixedly connected with the bottom of each second mounting plate 7.
Through above-mentioned technical scheme, realize supporting second mounting panel 7 through the setting of second bracing piece 6, conveniently install drive arrangement 15.
Specifically, the bottom of holding dish 8 communicates there is hose 13, and the bottom of hose 13 runs through to the inside of second connecting pipe 14, and the inside fixed mounting of hose 13 has the motorised valve.
Through the technical scheme, the azo-bis-isobutyronitrile in the holding vessel 8 is guided into the punching cleaning box 4 through the arrangement of the hose 13.
Specifically, four supporting seats 16 are fixedly arranged at the bottom of the base 1, and a drain pipe 9 is communicated with the bottom of the right side of the accommodating box 3.
Through the above technical scheme, the cleaning liquid is discharged through the arrangement of the drain pipe 9.
The working principle of the utility model is as follows: filling the cleaning liquid into the accommodating box 3, filling the azobisisobutyronitrile into the accommodating vessel 8, opening an electromagnetic valve in the hose 13, enabling the azobisisobutyronitrile in the accommodating vessel 8 to enter the punching cleaning box 4 through the hose 13 and the second connecting pipe 14 and be mixed with the solution in the accommodating box 3, driving the second gear 153 to rotate through the motor 151, driving the first gear 152 and the second connecting pipe 14 to rotate so as to enable the punching cleaning box 4 to rotate, realizing cleaning the azobisisobutyronitrile in the accommodating box 3, discharging the solution in the accommodating box 3 through the drain pipe 9 after cleaning, driving the second gear 153 and the first gear 152 to rotate through the motor 151, realizing centrifugal dehydration of the azobisisobutyronitrile through the rotation of the second connecting pipe 14 and the punching cleaning box 4, and discharging the azobisisobutyronitrile through the first connecting pipe 12 and the discharge pipe 10 after dehydration.
The foregoing description is only a preferred embodiment of the present utility model, but the scope of the present utility model is not limited thereto, and any person skilled in the art, who is within the scope of the present utility model, should make equivalent substitutions or modifications according to the technical solution of the present utility model and the inventive concept thereof, and should be covered by the scope of the present utility model.
Claims (7)
1. The utility model provides an azodiisobutyronitrile oxidation centrifugation spouts leaching material device, includes base (1), its characterized in that: the top of base (1) is provided with holds case (3), the inside of holding case (3) is provided with and punches a hole and washs case (4), the top intercommunication of punching a hole and washs case (4) has second connecting pipe (14), the top of second connecting pipe (14) runs through to the inside of first mounting panel (5) and is connected through the bearing rotation between with first mounting panel (5), the top of punching a hole and washs case (4) is provided with first mounting panel (5), the top of first mounting panel (5) is provided with drive arrangement (15), the top of first mounting panel (5) just is located the top of drive arrangement (15) and is provided with second mounting panel (7), the top fixed mounting of second mounting panel (7) has holding dish (8);
the driving device (15) comprises a motor (151) arranged at the top of the first mounting plate (5), a first gear (152) fixedly arranged at the outer side of the second connecting pipe (14) and a second gear (153) fixedly arranged on an output shaft of the motor (151), and the second gear (153) is meshed with the first gear (152).
2. The azodiisobutyronitrile oxidation centrifugal spray leaching device according to claim 1, wherein: the top fixed mounting of base (1) has four first bracing piece (2), the top of first bracing piece (2) is connected with the bottom fixed of first mounting panel (5), the outside of holding case (3) is connected with the inboard fixed of first bracing piece (2).
3. The azodiisobutyronitrile oxidation centrifugal spray leaching device according to claim 1, wherein: the bottom intercommunication that washs case (4) punches a hole has first connecting pipe (12), first connecting pipe (12) run through and hold case (3) and extend to the bottom that holds case (3), the outside cover of first connecting pipe (12) is equipped with mechanical seal (17), the outside of mechanical seal (17) and hold case (3) fixed connection.
4. A azobisisobutyronitrile oxidizing centrifugal spray rinsing device according to claim 3, characterized in that: the bottom of first connecting pipe (12) fixed mounting has rotary joint (11), the bottom intercommunication of rotary joint (11) has row material pipe (10), the end of row material pipe (10) extends to the left side of base (1) left.
5. The azodiisobutyronitrile oxidation centrifugal spray leaching device according to claim 1, wherein: four second supporting rods (6) are fixedly arranged at the top of the first mounting plate (5), and the top of each second supporting rod (6) is fixedly connected with the bottom of the second mounting plate (7).
6. The azodiisobutyronitrile oxidation centrifugal spray leaching device according to claim 1, wherein: the bottom of holding dish (8) is linked together there is hose (13), the inside to second connecting pipe (14) is run through to the bottom of hose (13), the inside fixed mounting of hose (13) has the motorised valve.
7. The azodiisobutyronitrile oxidation centrifugal spray leaching device according to claim 1, wherein: the bottom of base (1) fixed mounting has four supporting seats (16), the bottom intercommunication on holding case (3) right side has drain pipe (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321015308.4U CN219745663U (en) | 2023-04-28 | 2023-04-28 | Azodiisobutyronitrile oxidation centrifugal spraying and leaching device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321015308.4U CN219745663U (en) | 2023-04-28 | 2023-04-28 | Azodiisobutyronitrile oxidation centrifugal spraying and leaching device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219745663U true CN219745663U (en) | 2023-09-26 |
Family
ID=88072084
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321015308.4U Active CN219745663U (en) | 2023-04-28 | 2023-04-28 | Azodiisobutyronitrile oxidation centrifugal spraying and leaching device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219745663U (en) |
-
2023
- 2023-04-28 CN CN202321015308.4U patent/CN219745663U/en active Active
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| Date | Code | Title | Description |
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| GR01 | Patent grant | ||
| GR01 | Patent grant |