CN219722107U - Regenerated alkali liquor recycling device in dioxygen pentacyclic production - Google Patents
Regenerated alkali liquor recycling device in dioxygen pentacyclic production Download PDFInfo
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- CN219722107U CN219722107U CN202321356585.1U CN202321356585U CN219722107U CN 219722107 U CN219722107 U CN 219722107U CN 202321356585 U CN202321356585 U CN 202321356585U CN 219722107 U CN219722107 U CN 219722107U
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- recycling device
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- 239000003513 alkali Substances 0.000 title claims abstract description 54
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 33
- 238000004064 recycling Methods 0.000 title claims abstract description 32
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 229910001882 dioxygen Inorganic materials 0.000 title claims abstract description 21
- 238000003756 stirring Methods 0.000 claims abstract description 41
- 230000007246 mechanism Effects 0.000 claims abstract description 36
- 238000001914 filtration Methods 0.000 claims abstract description 21
- 239000007788 liquid Substances 0.000 claims description 25
- WNXJIVFYUVYPPR-UHFFFAOYSA-N 1,3-dioxolane Chemical compound C1COCO1 WNXJIVFYUVYPPR-UHFFFAOYSA-N 0.000 claims description 11
- 125000004122 cyclic group Chemical group 0.000 claims description 8
- 238000007790 scraping Methods 0.000 claims description 6
- 230000008929 regeneration Effects 0.000 claims description 3
- 238000011069 regeneration method Methods 0.000 claims description 3
- 238000004891 communication Methods 0.000 claims description 2
- 239000012535 impurity Substances 0.000 abstract description 9
- 239000002699 waste material Substances 0.000 abstract description 9
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 12
- 239000008187 granular material Substances 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 238000007599 discharging Methods 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 244000309464 bull Species 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- BGJSXRVXTHVRSN-UHFFFAOYSA-N 1,3,5-trioxane Chemical group C1OCOCO1 BGJSXRVXTHVRSN-UHFFFAOYSA-N 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000012938 design process Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000005829 trimerization reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model provides a regenerated alkali liquor recycling device in the production of a dioxygen pentacyclic, which comprises a bottom plate, wherein the top of the bottom plate is respectively provided with a stirring mechanism and a filtering mechanism, the stirring mechanism comprises a stirring box and a motor, the top of the bottom plate is fixedly connected with the stirring box, the top of the stirring box is fixedly connected with the motor, the filtering mechanism comprises a filter cartridge and a clamping block, the top of the bottom plate is fixedly connected with the filter cartridge, and the inner wall of the filter cartridge is fixedly connected with the clamping block. The regenerated alkali liquor recycling device in the dioxane production solves the problems that at present, when alkali liquor is recycled, waste alkali liquor and alkali blocks cannot be fully stirred and mixed, and granular impurities in the alkali liquor cannot be filtered, so that the subsequent recycling of the alkali liquor is affected, and alkali liquor resource waste is caused.
Description
Technical Field
The utility model relates to the field of dioxygen pentacyclic production, in particular to a recycling device for regenerated alkali liquor in dioxygen pentacyclic production.
Background
The dioxygen pentacyclic is an excellent organic solvent, the application is wide, mainly used as solvent of oil and fat, extractant, electrolytic solvent of lithium battery, in order to improve the displacement effect of the trimerization synthesis reactor, optimize the original design process, change the periodic liquid discharge of the synthesis reactor into continuous liquid discharge, banned sulfuric acid neutralizing tank, this technological transformation has promoted yield and quality of trioxymethylene greatly, but all alkali lyes regenerated in each unit are sent to the waste lye storage tank of tank area up to this point, treated regularly by the unit with qualification, have increased the alkali lye treatment cost.
At present, when recycling alkali liquor, waste alkali liquor and alkali blocks cannot be fully stirred and mixed, and granular impurities in the alkali liquor cannot be filtered, so that the follow-up recycling of the alkali liquor is affected, and alkali liquor resource waste is caused.
Therefore, it is necessary to provide a new regenerated alkali liquor recycling device in the production of the dioxygen pentacyclic to solve the technical problems.
Disclosure of Invention
In order to solve the technical problems, the utility model provides a recycling device for regenerated alkali liquor in the production of a dioxygen pentacyclic with stirring and filtering functions.
The utility model provides a regenerated alkali liquor recycling device in dioxygen pentacyclic production, which comprises a bottom plate, wherein the top of the bottom plate is respectively provided with a stirring mechanism and a filtering mechanism, the stirring mechanism comprises a stirring box and a motor, the top of the bottom plate is fixedly connected with the stirring box, the top of the stirring box is fixedly connected with the motor, the filtering mechanism comprises a filter cartridge and a clamping block, the top of the bottom plate is fixedly connected with the filter cartridge, and the inner wall of the filter cartridge is fixedly connected with the clamping block.
In order to achieve the effect of uniformly stirring alkali liquor, the utility model provides a regenerated alkali liquor recycling device in the production of a dioxygen pentacyclic, and preferably, the stirring mechanism further comprises a rotating rod, a fixed sleeve, a stirring rod and a scraping plate, wherein the output end of the motor is fixedly connected with the rotating rod, the bottom of the rotating rod is rotationally connected with the bottom of the inner cavity of the stirring box, and the outer side of the rotating rod is fixedly connected with the fixed sleeve.
In order to achieve the effect of scraping the residue on the inner wall of the stirring tank, the regenerated alkali liquor recycling device in the production of the dioxolane is provided by the utility model, preferably, the outer side of the fixed sleeve is fixedly connected with a stirring rod, and one end of the stirring rod is fixedly connected with a scraping plate.
In order to achieve the effect of filtering alkali liquor, the utility model provides a regenerated alkali liquor recycling device in the production of a dioxygen pentacyclic ring, and preferably, the filtering mechanism further comprises a first filter plate, a thread bush, a threaded rod, a connecting rod, a limiting ring and a handle, wherein the outer side of the clamping block is clamped with the first filter plate, and the top of the first filter plate is fixedly connected with the thread bush.
In order to achieve the effect of being convenient for disassembling and cleaning the first filter plate, the utility model provides the regenerated alkali liquor recycling device in the production of the dioxygen pentacyclic, preferably, the inner wall of the threaded sleeve is in threaded connection with a threaded rod, and the top of the threaded rod is fixedly connected with a connecting rod.
In order to achieve the effect of limiting the connecting rod, the regenerated alkali liquor recycling device in the production of the dioxygen pentacyclic compound is provided by the utility model, preferably, the outer side of the connecting rod is fixedly connected with a limiting ring, the outer side of the limiting ring is in sliding connection with the inner wall of the filter cartridge, and the top of the connecting rod is fixedly connected with a handle.
In order to achieve the effect of extracting the stirred alkali liquor, the regenerated alkali liquor recycling device in the production of the dioxolane is provided by the utility model, preferably, the top of the bottom plate is fixedly connected with a supporting plate, the top of the supporting plate is fixedly connected with a liquid extracting pump, one end of the liquid extracting pump is communicated with the outer side of the stirring box, and the other end of the liquid extracting pump is provided with a connecting pipe.
In order to achieve the effect of further filtering alkali liquor, the regenerated alkali liquor recycling device in the production of the dioxygen pentacyclic compound is provided by the utility model, preferably, the inner wall of the connecting pipe is in threaded connection with a liquid outlet pipe, one end of the liquid outlet pipe is communicated with the outer side of the filter cartridge, and the inner wall of the liquid outlet pipe is provided with a second filter plate.
In order to achieve the effect of recycling alkali liquor, the utility model provides a regenerated alkali liquor recycling device in the production of a dioxygen pentacyclic, preferably, a feed inlet is arranged on the outer side of a stirring tank, a cylinder cover is arranged on the top of a filter cylinder, a discharge pipe is arranged on the outer side of the filter cylinder, and a valve is arranged on the outer side of the discharge pipe.
Compared with the prior art, the utility model has the beneficial effects that:
this regeneration alkali lye cyclic utilization device in dioxygen pentacyclic production through setting up rabbling mechanism, reaches the effect that stirs the mixture to the lye, through setting up drawing liquid pump and second filter, reaches and carries out filterable effect to the lye medium-sized granule impurity, through setting up filtering mechanism, reaches and carries out filterable effect to the lye medium-sized granule impurity, improved lye cyclic utilization's quality, solved at present when cyclic utilization to the lye, can't carry out intensive mixing to waste lye and lye, and can't carry out filtration to the granule impurity in the lye, influence follow-up cyclic utilization to the lye, the problem of lye resource waste has been caused.
Drawings
FIG. 1 is a schematic diagram of a recycling apparatus for regenerated lye in the production of dioxolane according to a preferred embodiment of the present utility model;
FIG. 2 is a schematic diagram of a filtering mechanism according to the present utility model;
FIG. 3 is a schematic view of a first filter plate according to the present utility model;
FIG. 4 is a schematic structural view of the stirring mechanism in the present utility model;
fig. 5 is a schematic structural view of a support plate according to the present utility model.
Reference numerals in the drawings: 1. a bottom plate; 2. a stirring mechanism; 21. a stirring tank; 22. a motor; 23. a rotating rod; 24. a fixed sleeve; 25. a stirring rod; 26. a scraper; 3. a filtering mechanism; 31. a filter cartridge; 32. a clamping block; 33. a first filter plate; 34. a thread sleeve; 35. a threaded rod; 36. a connecting rod; 37. a limiting ring; 38. a handle; 4. a support plate; 5. a liquid pump; 6. a connecting pipe; 7. a liquid outlet pipe; 8. a second filter plate; 9. a feed inlet; 10. a cylinder cover; 11. a discharge pipe; 12. and (3) a valve.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to fall within the scope of the utility model. It is to be understood that the drawings are designed solely for the purposes of illustration and not as a definition of the limits of the utility model. The connection relationships shown in the drawings are for convenience of clarity of description only and are not limiting on the manner of connection.
It is noted that when one component is considered to be "connected" to another component, it may be directly connected to the other component, or intervening components may also be present. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this utility model belongs. It should also be noted that the terms "mounted," "connected," and "connected" are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected, unless otherwise specifically defined and limited; either mechanically or electrically, or by communication between two components. The specific meaning of the above terms in the present utility model will be understood in specific cases by those of ordinary skill in the art. The terminology used herein in the description of the utility model is for the purpose of describing particular embodiments only and is not intended to be limiting of the utility model.
Referring to fig. 1, fig. 2, fig. 3, fig. 4 and fig. 5 in combination, fig. 1 is a schematic structural diagram of a preferred embodiment of a recycling device for regenerated alkaline solution in a dioxane production provided by the present utility model; FIG. 2 is a schematic diagram of a filtering mechanism according to the present utility model; FIG. 3 is a schematic view of a first filter plate according to the present utility model; FIG. 4 is a schematic structural view of the stirring mechanism in the present utility model; fig. 5 is a schematic structural view of a support plate according to the present utility model. Regeneration alkali lye cyclic utilization device in the production of dioxygen five rings, including bottom plate 1, the top of bottom plate 1 is provided with rabbling mechanism 2 and filtering mechanism 3 respectively, and rabbling mechanism 2 includes agitator tank 21 and motor 22, and the top fixedly connected with agitator tank 21 of bottom plate 1, the top fixedly connected with motor 22 of agitator tank 21, filtering mechanism 3 include cartridge filter 31 and fixture block 32, the top fixedly connected with cartridge filter 31 of bottom plate 1, the inner wall fixedly connected with fixture block 32 of cartridge filter 31.
In the specific implementation process, as shown in fig. 1 and 4, the stirring mechanism 2 further comprises a rotating rod 23, a fixed sleeve 24, a stirring rod 25 and a scraping plate 26, the output end of the motor 22 is fixedly connected with the rotating rod 23, the bottom of the rotating rod 23 is rotationally connected with the bottom of the inner cavity of the stirring box 21, and the outer side of the rotating rod 23 is fixedly connected with the fixed sleeve 24.
The outside fixedly connected with puddler 25 of fixed cover 24, the one end fixedly connected with scraper blade 26 of puddler 25.
The outside of agitator tank 21 is provided with feed inlet 9, and the top of cartridge filter 31 is provided with cover 10, and the outside of cartridge filter 31 is provided with discharging pipe 11, and the outside of discharging pipe 11 is provided with valve 12.
It should be noted that: when the device is used, through setting up rabbling mechanism 2, pour waste lye and the alkali block in the production of dioxygen pentacyclic into agitator tank 21 inside through feed inlet 9, starter motor 22 drives bull stick 23 and rotates, drives puddler 25 through fixed cover 24 and rotates, carries out intensive mixing to lye and alkali block, scrapes the remaining material of agitator tank 21 inner wall through scraper blade 26, reduces the wasting of resources.
Referring to fig. 1, 2, 3 and 5, the filtering mechanism 3 further includes a first filter plate 33, a threaded sleeve 34, a threaded rod 35, a connecting rod 36, a limiting ring 37 and a handle 38, the outer side of the clamping block 32 is clamped with the first filter plate 33, and the top of the first filter plate 33 is fixedly connected with the threaded sleeve 34.
The inner wall threaded connection of thread bush 34 has threaded rod 35, and the top fixedly connected with connecting rod 36 of threaded rod 35.
The outside fixedly connected with spacing ring 37 of connecting rod 36, the outside of spacing ring 37 and the inner wall sliding connection of cartridge filter 31, the top fixedly connected with handle 38 of connecting rod 36.
The top fixedly connected with backup pad 4 of bottom plate 1, the top fixedly connected with drawing liquid pump 5 of backup pad 4, the one end and the outside intercommunication of agitator tank 21 of drawing liquid pump 5, the other end of drawing liquid pump 5 is provided with connecting pipe 6.
The inner wall threaded connection of connecting pipe 6 has drain pipe 7, and the one end of drain pipe 7 communicates with the outside of cartridge filter 31, and the inner wall of drain pipe 7 is provided with second filter 8.
It should be noted that: after the alkali liquor stirring is finished, the liquid suction pump 5 is started to pump alkali liquor in the stirring tank 21, the alkali liquor is conveyed to the inside of the filter cartridge 31 through the connecting pipe 6 and the liquid outlet pipe 7, large particle impurities in the alkali liquor are filtered through the second filter plate 8, the connecting pipe 6 is in threaded connection with the liquid outlet pipe 7, the second filter plate 8 can be conveniently detached and cleaned, after the alkali liquor enters the filter cartridge 31, small particle impurities in the alkali liquor are filtered through the first filter plate 33, after the alkali liquor is filtered, the valve 12 is opened, the alkali liquor is discharged and collected through the discharging pipe 11, the alkali liquor is conveniently recycled, the stirring mechanism 2 and the filtering mechanism 3 are matched for use, the alkali liquor recycling quality is improved, after the alkali liquor treatment is finished, the cylinder cover 10 is opened, the handle 38 is pulled to drive the connecting rod 36 and the limiting ring 37 to rise, the first filter plate 33 is separated from the clamping block 32, the first filter plate 33 is rotated, and the first filter plate 33 is removed for replacement and cleaning.
The working principle of the regenerated alkali liquor recycling device in the production of the dioxygen pentacyclic is as follows:
when the device is used, through setting up rabbling mechanism 2, waste lye and the alkali block in the production of dioxygen five rings are poured into the agitator tank 21 through feed inlet 9 inside, starter motor 22 drives bull stick 23 and rotates, drive puddler 25 through fixed cover 24 and rotate, fully stir and mix lye and alkali block, scrape the remaining material of agitator tank 21 inner wall through scraper blade 26, reduce the wasting of resources, after the lye stirring is accomplished, start the drawing liquid pump 5 and take out the lye of agitator tank 21 inside, carry lye to cartridge filter 31 inside through connecting pipe 6 and drain pipe 7, filter the large granule impurity in the lye through second filter 8, connecting pipe 6 and drain pipe 7 threaded connection, can be convenient for dismantle the washing to second filter 8, after the lye gets into cartridge filter 31 inside, filter through first filter 33 and filter the small granule impurity in the lye, open valve 12, conveniently discharge and collect lye through the drain pipe 11, the cyclic utilization of lye, use through rabbling mechanism 2 and filter mechanism 3 cooperation, the quality of cyclic utilization has been improved, after the processing is accomplished, open lid 10, drive the filter 33 and take out the filter 33 and rotate the first filter 33, take out the first filter 33 and take out the filter 33 and rotate the cover 33, take out the filter through the first filter.
The foregoing description is only illustrative of the present utility model and is not intended to limit the scope of the utility model, and all equivalent structures or equivalent processes or direct or indirect application in other related technical fields are included in the scope of the present utility model.
Claims (9)
1. Regeneration alkali lye cyclic utilization device in the production of dioxygen five rings, a serial communication port, including bottom plate (1), the top of bottom plate (1) is provided with rabbling mechanism (2) and filter mechanism (3) respectively, rabbling mechanism (2) are including agitator tank (21) and motor (22), the top fixedly connected with agitator tank (21) of bottom plate (1), the top fixedly connected with motor (22) of agitator tank (21), filter mechanism (3) are including cartridge filter (31) and fixture block (32), the top fixedly connected with cartridge filter (31) of bottom plate (1), the inner wall fixedly connected with fixture block (32) of cartridge filter (31).
2. The recycling device for regenerated alkaline liquor in the production of the dioxolane according to claim 1, wherein the stirring mechanism (2) further comprises a rotating rod (23), a fixing sleeve (24), a stirring rod (25) and a scraping plate (26), the output end of the motor (22) is fixedly connected with the rotating rod (23), the bottom of the rotating rod (23) is rotationally connected with the bottom of the inner cavity of the stirring box (21), and the outer side of the rotating rod (23) is fixedly connected with the fixing sleeve (24).
3. The recycling device for regenerated alkaline liquor in the production of the dioxolane according to claim 2, wherein a stirring rod (25) is fixedly connected to the outer side of the fixing sleeve (24), and a scraping plate (26) is fixedly connected to one end of the stirring rod (25).
4. The recycling device for regenerated alkaline liquor in the production of the dioxolane according to claim 1, wherein the filtering mechanism (3) further comprises a first filtering plate (33), a threaded sleeve (34), a threaded rod (35), a connecting rod (36), a limiting ring (37) and a handle (38), the first filtering plate (33) is clamped on the outer side of the clamping block (32), and the threaded sleeve (34) is fixedly connected to the top of the first filtering plate (33).
5. The recycling device for regenerated lye in the production of the dioxolane according to claim 4, wherein the inner wall of the thread sleeve (34) is in threaded connection with a threaded rod (35), and the top of the threaded rod (35) is fixedly connected with a connecting rod (36).
6. The recycling device for regenerated alkaline liquor in the production of the dioxolane according to claim 4, wherein a limiting ring (37) is fixedly connected to the outer side of the connecting rod (36), the outer side of the limiting ring (37) is slidably connected with the inner wall of the filter cartridge (31), and a handle (38) is fixedly connected to the top of the connecting rod (36).
7. The recycling device for regenerated alkaline liquor in the production of the dioxolane according to claim 1, wherein the top of the bottom plate (1) is fixedly connected with a supporting plate (4), the top of the supporting plate (4) is fixedly connected with a liquid drawing pump (5), one end of the liquid drawing pump (5) is communicated with the outer side of the stirring box (21), and the other end of the liquid drawing pump (5) is provided with a connecting pipe (6).
8. The recycling device for regenerated alkaline liquid in the production of the dioxolane according to claim 7 is characterized in that a liquid outlet pipe (7) is connected to the inner wall of the connecting pipe (6) in a threaded mode, one end of the liquid outlet pipe (7) is communicated with the outer side of the filter cartridge (31), and a second filter plate (8) is arranged on the inner wall of the liquid outlet pipe (7).
9. The recycling device for regenerated alkaline liquor in the production of the dioxolane according to claim 1, wherein a feed inlet (9) is arranged on the outer side of the stirring box (21), a cylinder cover (10) is arranged at the top of the filter cylinder (31), a discharge pipe (11) is arranged on the outer side of the filter cylinder (31), and a valve (12) is arranged on the outer side of the discharge pipe (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321356585.1U CN219722107U (en) | 2023-05-27 | 2023-05-27 | Regenerated alkali liquor recycling device in dioxygen pentacyclic production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321356585.1U CN219722107U (en) | 2023-05-27 | 2023-05-27 | Regenerated alkali liquor recycling device in dioxygen pentacyclic production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219722107U true CN219722107U (en) | 2023-09-22 |
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ID=88032528
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321356585.1U Active CN219722107U (en) | 2023-05-27 | 2023-05-27 | Regenerated alkali liquor recycling device in dioxygen pentacyclic production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219722107U (en) |
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2023
- 2023-05-27 CN CN202321356585.1U patent/CN219722107U/en active Active
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