CN219595887U - Multistage molecular distillation equipment - Google Patents

Multistage molecular distillation equipment Download PDF

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Publication number
CN219595887U
CN219595887U CN202320584201.5U CN202320584201U CN219595887U CN 219595887 U CN219595887 U CN 219595887U CN 202320584201 U CN202320584201 U CN 202320584201U CN 219595887 U CN219595887 U CN 219595887U
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wall
distillation
flask body
distillation flask
rotating rod
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CN202320584201.5U
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Chinese (zh)
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郑希林
徐梅菊
赵红颜
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Shandong Yuekang Pharmaceutical Co ltd
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Shandong Yuekang Pharmaceutical Co ltd
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Abstract

The utility model relates to the technical field of medicine preparation and discloses multistage molecular distillation equipment, which comprises three distillation flask bodies, wherein a heating mechanism is arranged in each distillation flask body, first fixing holes are formed in the top of each distillation flask body and the bottom end of the outer wall of each distillation flask body, a feeding pipe and a discharging pipe are respectively and fixedly connected to the inner wall of each first fixing hole, electromagnetic valves are arranged on each feeding pipe and each discharging pipe, the three distillation flask bodies are connected in series through connecting pipelines, one end of each connecting pipeline is arranged in each discharging pipe, the other end of each connecting pipeline is arranged on the inner wall of each feeding pipe, a liquid discharging mechanism for purifying is arranged at one end of each distillation flask body, a stirring mechanism for stirring distilled liquid is arranged in each distillation flask body, and a membrane breaking mechanism for breaking bubbles is arranged on each stirring mechanism. According to the utility model, through the stirring mechanism and the membrane breaking mechanism, the influence of the generation of bubbles on the distillation effect of liquid is avoided.

Description

Multistage molecular distillation equipment
Technical Field
The utility model relates to the technical field of medicine preparation, in particular to multistage molecular distillation equipment.
Background
Molecular distillation is a special liquid-liquid separation technology, and separation is realized by means of the difference of the motion average free path of molecules of different substances, so that the molecular distillation method has wide application in the industries of food, medicine, fine chemical industry and the like.
When the existing distillation equipment is used, bubbles are easily generated on the liquid surface when gas cannot be timely discharged in the liquid heating process, the bubbles cannot be timely broken by the existing equipment, and the gas at the distillation position is easily remained in the bubbles and cannot be discharged, so that the distillation effect is affected.
To this end, we propose a multistage molecular distillation apparatus.
Disclosure of Invention
The utility model mainly solves the technical problems existing in the prior art and provides multi-stage molecular distillation equipment.
In order to achieve the above purpose, the technical scheme is that the multistage molecular distillation device comprises three distillation flask bodies, wherein a heating mechanism is arranged in each distillation flask body, first fixing holes are formed in the top of each distillation flask body and the bottom end of the outer wall of each distillation flask body, a feeding pipe and a discharging pipe are respectively and fixedly connected to the inner wall of each first fixing hole, electromagnetic valves are arranged on each feeding pipe and each discharging pipe, the three distillation flask bodies are connected in series through a connecting pipeline, one end of each connecting pipeline is arranged in each discharging pipe, the other end of each connecting pipeline is arranged on the inner wall of each feeding pipe, a liquid draining mechanism for purifying is arranged at one end of each distillation flask body, a stirring mechanism for stirring distilled liquid is arranged in each distillation flask body, and a membrane breaking mechanism for breaking bubbles is arranged on each stirring mechanism.
Further, be provided with fluid-discharge tube and condensation box in the flowing back mechanism, the condensation box sets up in the inner wall of distillation flask body one side, and condensation box one end is provided with the second fixed orifices, and the second fixed orifices extends to distillation flask body outer wall, and fluid-discharge tube fixed connection is provided with the solenoid valve in the second fixed orifices inner wall on the fluid-discharge tube.
Further, a rotating shaft, a main stirring fan blade and an auxiliary stirring fan blade are arranged in the stirring mechanism.
Further, the axis of rotation passes through the motor to be rotated and is connected in the inner wall of distillation flask body bottom, and main stirring flabellum is the circumference and arranges at the axis of rotation outer wall, and main stirring flabellum internal rotation is connected with dwang one, and vice stirring flabellum is circumference and arranges at dwang one outer wall both ends.
Further, the through hole is formed in the inner wall of the bottom of the rotating shaft, the inner wall of the top of the rotating shaft is rotationally connected with the fixing rod, the bottom of the fixing rod penetrates through the through hole and is fixedly connected to the inner wall of the distillation flask body, and the outer wall of the fixing rod is fixedly connected with the first bevel gear.
Further, the main stirring fan blade is connected with a connecting rotating rod in a rotating way far away from the inner wall of one side of the rotating shaft, the connecting rotating rod extends to the inner wall of the rotating shaft, and a bevel gear II is arranged at one end, close to the fixed rod, of the connecting rotating rod and meshed with the outer wall of the bevel gear I.
Further, a second rotating rod and a membrane breaker are arranged in the membrane breaking mechanism, a plurality of linearly arranged rotating holes are formed in the outer wall of the main stirring fan blade, the second rotating rod is connected to the inner wall of the rotating hole in a rotating mode, and the membrane breaker is arranged at two ends of the second rotating rod.
Further, the outer wall of the connecting rotating rod is fixedly connected with a plurality of linearly arranged worms, the first rotating rod and the outer wall of the rotating rod are fixedly connected with worm wheels, and the worm wheels are meshed with the outer wall of the second rotating rod.
Further, the membrane breaker is conical, and a spiral thread groove is formed in the outer wall of the membrane breaker.
Advantageous effects
The utility model provides a multistage molecular distillation device. The beneficial effects are as follows:
(1) This multistage molecular distillation equipment, through rabbling mechanism and rupture of membranes mechanism that sets up, when need distill, this moment adds the raw materials in the distillation flask body through the inlet pipe, can distill through the heating mechanism in it, gasified gas can cool off in the condensate tank department and discharge through the fluid-discharge tube and purify, in distillation process, the main stirring flabellum that opens on the axis of rotation this moment can drive it on this internal raw materials stirring of distillation flask, improve its evaporation rate, and when its stirring, the dead lever is fixed knot constructs, thereby connect and rotate relatively between bull stick and the dead lever, then can drive the connection bull stick and rotate under the bevel gear second effect on the bull stick on the bevel gear on the dead lever, connect the bull stick rotation and can drive the dwang second on worm wheel through the discharging pipe on it and rotate, the dwang second rotates and can drive the rupture of membranes ware and rotate in step along with main stirring flabellum, then, the bubble that appears on the liquid level is broken through its and rotation, the bubble that avoids producing influences the distillation effect of liquid on the liquid level, and the bubble can not be influenced by the revolution effect on the side of the rotation groove, further can avoid the bubble to make progress the bubble on the side of the rotation, further can avoid the bubble to distill effect.
(2) This multistage molecular distillation equipment, through the rabbling mechanism that sets up, when main stirring flabellum rotates, the worm outside the connection bull stick on it drives the worm wheel and rotates, and the worm wheel rotates and can drive the dwang and together step by step rotates, and the revolute pair stirring flabellum on the dwang rotates, can stir liquid simultaneously in level and vertical two directions then, carries out the vortex to it, and liquid can be heated more evenly, improves its distillation efficiency.
Drawings
FIG. 1 is a front view of the present utility model;
FIG. 2 is a cross-sectional view of the present utility model;
FIG. 3 is an enlarged view of portion A of FIG. 2 in accordance with the present utility model;
fig. 4 is an enlarged view of portion B of fig. 2 in accordance with the present utility model.
Legend description: 1. a distillation flask body; 2. a connecting pipe; 3. a liquid discharge pipe; 4. a feed pipe; 5. a discharge pipe; 6. a condensing box; 7. a rotating shaft; 8. a main stirring blade; 9. rotating the first rod; 10. auxiliary stirring fan blades; 11. a fixed rod; 12. bevel gears I; 13. bevel gears II; 14. connecting a rotating rod; 15. a worm; 16. a second rotating rod; 17. a worm wheel; 18. a membrane breaker; 19. a thread groove.
Detailed Description
Embodiment one: the utility model provides a multistage molecular distillation equipment, as shown in fig. 1-2, including three distillation flask body 1, be provided with heating mechanism in the distillation flask body 1, first fixed orifices has all been seted up to distillation flask body 1 top and outer wall bottom, first fixed orifices inner wall fixedly connected with inlet pipe 4 and discharging pipe 5 respectively, all be provided with the solenoid valve on inlet pipe 4 and the discharging pipe 5, and three distillation flask body 1 establishes ties through connecting tube 2, connecting tube 2 one end is installed in discharging pipe 5, the connecting tube 2 other end is installed in inlet pipe 4 inner walls, distillation flask body 1 one end is provided with the flowing back mechanism that is used for the purification, and be provided with in the distillation flask body 1 and be used for the rabbling mechanism to the stirring of distillation liquid, be provided with on the rabbling mechanism and be used for the rupture of membranes mechanism to the bubble.
Be provided with fluid-discharge tube 3 and condensation tank 6 in the flowing back mechanism, condensation tank 6 sets up in the inner wall of distillation flask body 1 one side, and condensation tank 6 one end is provided with the second fixed orifices, and the second fixed orifices extends to distillation flask body 1 outer wall, and fluid-discharge tube 3 fixed connection is provided with the solenoid valve in second fixed orifices inner wall on the fluid-discharge tube 3.
The stirring mechanism is internally provided with a rotating shaft 7, a main stirring fan blade 8 and an auxiliary stirring fan blade 10.
As shown in fig. 3-4, the rotation shaft 7 is rotatably connected to the inner wall of the bottom of the distillation flask body 1 through a motor, the main stirring fan blades 8 are circumferentially arranged on the outer wall of the rotation shaft 7, the main stirring fan blades 8 are rotatably connected with a first rotation rod 9, and the auxiliary stirring fan blades 10 are circumferentially arranged at two ends of the outer wall of the first rotation rod 9.
The inner wall of the bottom of the rotating shaft 7 is provided with a through hole, the inner wall of the top of the rotating shaft 7 is rotationally connected with a fixing rod 11, the bottom of the fixing rod 11 penetrates through the through hole and is fixedly connected with the inner wall of the distillation flask body 1, and the outer wall of the fixing rod 11 is fixedly connected with a bevel gear I12.
The inner wall of one side of the main stirring fan blade 8 far away from the rotating shaft 7 is rotationally connected with a connecting rotating rod 14, the connecting rotating rod 14 extends to the inner wall of the rotating shaft 7, and one end, close to the fixed rod 11, of the connecting rotating rod 14 is provided with a bevel gear II 13, and the bevel gear II 13 is meshed with the outer wall of the bevel gear I12.
The membrane breaking mechanism is internally provided with a second rotating rod 16 and a membrane breaker 18, the outer wall of the main stirring fan blade 8 is provided with a plurality of rotating holes which are linearly arranged, the second rotating rod 16 is rotationally connected with the inner wall of the rotating hole, and the membrane breaker 18 is arranged at two ends of the second rotating rod 16.
The outer wall of the connecting rotating rod 14 is fixedly connected with a plurality of linearly arranged worms 15, the outer walls of the rotating rod I9 and the rotating rod II 16 are fixedly connected with worm gears 17, and the worm gears 17 are meshed with the outer walls of the rotating rod II 16.
The membrane breaker 18 is tapered, and the membrane breaker 18 is provided with a spiral thread groove 19 along its outer wall.
The working principle of the utility model is as follows: through rabbling mechanism and rupture of membranes mechanism that set up, when need distill, in adding the bottle body 1 through inlet pipe 4 with the raw materials this moment, can distill through its heating mechanism in, gasified gas can cool off in condensate tank 6 department and discharge through fluid-discharge tube 3 and purify, in distillation process, the motor on the axis of rotation 7 can drive main stirring flabellum 8 on it this moment and stir the raw materials in the bottle body 1, improve its evaporation rate, and when its stirring, dead lever 11 is fixed structure, thereby connect and rotate relatively between bull stick 14 and the dead lever 11, then can drive connection bull stick 14 and spin under the effect of bevel gear two 13 on connection bull stick 14 on the dead lever 11, connection bull stick 14 autorotation can drive the dwang 16 on worm wheel 17 and worm wheel 17 through discharging tube 5 on it, the dwang two 16 rotates and can drive the breaker 18 and rotate in step along with main stirring flabellum 8 and revolve around axis 7 simultaneously, then revolve and break the bubble on the liquid surface and produce the effect of breaking bubbles on the liquid through its revolution, and can avoid the bubble on the side of the distiller to produce the effect of bubble on the bubble can be better, can avoid the bubble on the side of the distiller is affected.
Through the rabbling mechanism who sets up, when main stirring flabellum 8 rotates, the outer worm 15 of connection bull stick 14 on it drives worm wheel 17 and rotates, and worm wheel 17 rotates and can drive dwang one 9 and rotate in step, and dwang one 9 rotates and drives the vice stirring flabellum 10 on it and rotate, can stir liquid simultaneously in level and vertical two directions, carries out the vortex to it, and liquid can be heated more evenly, improves its distillation efficiency.
The foregoing has shown and described the basic principles and main features of the present utility model and the advantages of the present utility model. It will be understood by those skilled in the art that the present utility model is not limited to the embodiments described above, and that the above embodiments and descriptions are merely illustrative of the principles of the present utility model, and various changes and modifications may be made without departing from the spirit and scope of the utility model, which is defined in the appended claims. The scope of the utility model is defined by the appended claims and equivalents thereof.

Claims (9)

1. Multistage molecular distillation equipment, including three distillation bottle body (1), be provided with heating mechanism, its characterized in that in distillation bottle body (1): the utility model provides a distillation flask body, including distillation flask body (1), connecting tube (2), feed pipe (4) and feed pipe (5), connecting tube (2) are installed to connecting tube (2) one end in feed pipe (5), connecting tube (2) other end is installed in feed pipe (4) inner wall, distillation flask body (1) one end is provided with the flowing back mechanism that is used for the purification, and is provided with in distillation flask body (1) and be used for the rabbling mechanism to distillation liquid stirring, is provided with on the rabbling mechanism and is used for the rupture of membranes mechanism to the bubble.
2. The multi-stage molecular distillation apparatus according to claim 1, wherein: be provided with fluid-discharge tube (3) and condensing case (6) in the flowing back mechanism, condensing case (6) set up in the inner wall of distillation flask body (1) one side, and condensing case (6) one end is provided with the second fixed orifices, and the second fixed orifices extends to distillation flask body (1) outer wall, and fluid-discharge tube (3) fixed connection is provided with the solenoid valve in second fixed orifices inner wall on fluid-discharge tube (3).
3. The multi-stage molecular distillation apparatus according to claim 1, wherein: a rotating shaft (7), a main stirring fan blade (8) and an auxiliary stirring fan blade (10) are arranged in the stirring mechanism.
4. A multi-stage molecular distillation apparatus according to claim 3, wherein: the rotary shaft (7) is rotationally connected to the inner wall of the bottom of the distillation flask body (1) through a motor, the main stirring fan blades (8) are circumferentially arranged on the outer wall of the rotary shaft (7), the rotary rod I (9) is rotationally connected to the main stirring fan blades (8), and the auxiliary stirring fan blades (10) are circumferentially arranged at two ends of the outer wall of the rotary rod I (9).
5. The multi-stage molecular distillation apparatus according to claim 4, wherein: the inner wall of the bottom of the rotating shaft (7) is provided with a through hole, the inner wall of the top of the rotating shaft (7) is rotationally connected with a fixing rod (11), the bottom of the fixing rod (11) penetrates through the through hole and is fixedly connected with the inner wall of the distillation flask body (1), and the outer wall of the fixing rod (11) is fixedly connected with a bevel gear I (12).
6. The multi-stage molecular distillation apparatus according to claim 5, wherein: the main stirring fan blade (8) is far away from the inner wall at one side of the rotating shaft (7) and is rotationally connected with a connecting rotating rod (14), the connecting rotating rod (14) extends to the inner wall of the rotating shaft (7), and one end, close to the fixed rod (11), of the connecting rotating rod (14) is provided with a bevel gear II (13), and the bevel gear II (13) is meshed with the outer wall of the bevel gear I (12).
7. The multi-stage molecular distillation apparatus according to claim 6, wherein: a second rotating rod (16) and a membrane breaker (18) are arranged in the membrane breaking mechanism, a plurality of linearly arranged rotating holes are formed in the outer wall of the main stirring fan blade (8), the second rotating rod (16) is rotationally connected to the inner wall of the rotating holes, and the membrane breaker (18) is arranged at two ends of the second rotating rod (16).
8. The multi-stage molecular distillation apparatus according to claim 7, wherein: the outer wall of the connecting rotating rod (14) is fixedly connected with a plurality of linearly arranged worms (15), the outer walls of the first rotating rod (9) and the second rotating rod (16) are fixedly connected with worm wheels (17), and the worm wheels (17) are meshed with the outer wall of the second rotating rod (16).
9. The multi-stage molecular distillation apparatus according to claim 8, wherein: the membrane breaker (18) is conical, and a spiral thread groove (19) is formed in the outer wall of the membrane breaker (18).
CN202320584201.5U 2023-03-23 2023-03-23 Multistage molecular distillation equipment Active CN219595887U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202320584201.5U CN219595887U (en) 2023-03-23 2023-03-23 Multistage molecular distillation equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202320584201.5U CN219595887U (en) 2023-03-23 2023-03-23 Multistage molecular distillation equipment

Publications (1)

Publication Number Publication Date
CN219595887U true CN219595887U (en) 2023-08-29

Family

ID=87739434

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202320584201.5U Active CN219595887U (en) 2023-03-23 2023-03-23 Multistage molecular distillation equipment

Country Status (1)

Country Link
CN (1) CN219595887U (en)

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