CN219441611U - Acetylene furnace reaction chamber with adjustable reaction time - Google Patents

Acetylene furnace reaction chamber with adjustable reaction time Download PDF

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Publication number
CN219441611U
CN219441611U CN202220061218.8U CN202220061218U CN219441611U CN 219441611 U CN219441611 U CN 219441611U CN 202220061218 U CN202220061218 U CN 202220061218U CN 219441611 U CN219441611 U CN 219441611U
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reaction chamber
reaction
wall
acetylene
adjustable
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王金福
丰秀珍
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Huafeng Chemical Co ltd
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Abstract

The utility model belongs to the field of natural gas chemical industry in general, and provides an acetylene furnace reaction chamber with adjustable reaction time, which comprises an upper part (101) and a lower part (102); the top of the upper part (101) of the reaction chamber is connected with an acetylene furnace burner plate, and the lower part of the lower part (102) of the reaction chamber is connected with a quenching system; the upper part (101) of the reaction chamber is separated from the lower part (102) of the reaction chamber; a height adjusting component (5) is arranged on the upper part (101) or the lower part (102) of the reaction chamber; the height adjusting component (5) is used for enabling the upper part (101) or the lower part (102) of the reaction chamber to move in the vertical direction, so that the distance between the lower part (102) of the reaction chamber and the upper part (101) of the reaction chamber is controlled and adjusted, and the purpose of adjusting the reaction time of the internal gas is achieved by adjusting the height of the reaction chamber of the acetylene furnace.

Description

Acetylene furnace reaction chamber with adjustable reaction time
Technical Field
The utility model belongs to the field of natural gas chemical industry in general, and particularly relates to an acetylene furnace reaction chamber with adjustable reaction time.
Background
The partial oxidative cleavage of natural gas to acetylene is typically a reaction sequence and the intermediate product is the target product acetylene. The oxidation reaction process takes a very short time, and is a millisecond-scale transient reaction. Therefore, the control requirement on the reaction process is very strict, and problems are brought to too short or too long reaction time, such as insufficient reaction caused by too short reaction time, and further cracking of the intermediate product acetylene into hydrogen and carbon black caused by too long reaction time.
Because of the volume, height and other parameters of the reaction chamber, the residence time of the reaction gas in the reaction chamber is directly related. Therefore, when designing the reaction chamber of the acetylene furnace, the size of the reaction chamber needs to be combined with the air inflow, air speed, proportion and the like of the raw material gas to carry out strict experimental measurement and simulation accounting of dynamics and thermodynamic parameters.
Therefore, in order to ensure the optimization of the oxidation-cracking reaction time, for the acetylene reaction device with a solidified structure, on one hand, the optimized oxidation reaction time can be ensured only by keeping stable and unchanged process parameters including the raw material gas grade composition, the oxygen ratio, the speed, the temperature and the like, and on the other hand, the productivity is fixed and cannot be changed at will.
For the reaction chamber with a variable structural size, the reaction time can be controlled through structural change, so that the production load of the device can be flexibly adjusted and the device can adapt to the change of other process conditions.
Disclosure of Invention
The inventor of the application considers through research analysis summary that: in the process of preparing acetylene from natural gas, once the size of the reaction chamber of the acetylene furnace is solidified, the optimized oxidative cracking time can be ensured only according to the preset air inlet parameter, so that the productivity or the production load of the reaction chamber of the acetylene furnace can not be adjusted, if the acetylene reaction furnace with adjustable size can be designed, parameters such as air inlet and the like and the size of the acetylene reaction furnace can be adjusted and changed according to the planned change of the production load, so that the time adjustment of the gas in the reaction chamber of the acetylene furnace is controlled within the optimized time, thereby realizing the variable production load of the reaction chamber of the acetylene furnace and optimal oxidative cracking yield. Therefore, the utility model aims to provide an acetylene furnace reaction chamber with adjustable reaction time, which is characterized in that the acetylene furnace reaction chamber is designed into an upper reaction chamber and a lower reaction chamber, the lower reaction chamber can move relative to the upper reaction chamber, the overall height of the reaction chamber is changed, the total height of the reaction chamber is regulated to a reasonable value according to the size, the proportion, the speed, the productivity and the like of the air inflow in actual production, the residence time of gas in the reaction chamber is regulated to be within the optimal reaction time interval, the yield of the reaction product is ensured, and the device can flexibly regulate the production load and the productivity of the device, adapt to the change of the process parameters of raw gas and the like and simultaneously ensure the maximization of the yield by changing the height of the reaction chamber.
The technical scheme of the utility model is that the reaction chamber of the acetylene furnace with adjustable reaction time comprises the upper part of the reaction chamber and the lower part of the reaction chamber; the top end of the upper part of the reaction chamber is connected with an acetylene furnace burner plate, and the lower part of the reaction chamber is connected with a quenching system; the upper part of the reaction chamber is separated from the lower part of the reaction chamber; the upper part or the lower part of the reaction chamber is provided with a height adjusting component; the height adjusting component is used for enabling the upper part of the reaction chamber or the lower part of the reaction chamber to move in parallel in the vertical direction, so that the distance between the lower part of the reaction chamber and the upper part of the reaction chamber is controlled and adjusted, and the regulation and control of the gas reaction time are realized through the height adjustment of the reaction chamber of the acetylene furnace; the reaction chamber of the acetylene furnace with adjustable reaction time is arranged in a closed cavity structure.
The utility model separates the height direction of the reaction chamber into two parts which are relatively independent from each other, namely the upper part of the reaction chamber and the lower part of the reaction chamber, and realizes the movement of the lower part of the reaction chamber in the vertical direction through the height adjusting part arranged on the upper part of the reaction chamber or the lower part of the reaction chamber, thereby realizing the regulation and control of the overall height of the upper part of the reaction chamber and the lower part of the reaction chamber (namely the height of the reaction chamber or the distance of the reaction gas passing through a reaction zone), and reasonably presuming the residence time requirement of the reaction gas in the reaction chamber according to the parameters under the condition that the air inflow amount, the air inflow proportion, the air inflow flow rate and the like of the reaction chamber are changed, and further, the upper part of the reaction chamber and the lower part of the reaction chamber are far away from or close to each other through the height adjusting part on the upper part of the reaction chamber or the lower part of the reaction chamber, thereby changing the height of the reaction chamber (gas reaction zone) formed jointly with the lower part of the reaction chamber, and realizing the control of the residence time of the gas in the reaction chamber within the optimal reaction time interval through the height adjustment of the reaction chamber;
the utility model provides an acetylene furnace reaction chamber, which belongs to a part of components in an acetylene furnace reactor for preparing acetylene from natural gas. Therefore, the design of the airtight connection between the upper part of the reaction chamber and the lower part of the reaction chamber may not be considered, because even if the lower part of the reaction chamber needs a certain distance from the upper part of the reaction chamber because of the height adjustment, part of the reaction gas escaping from the connection part of the two is still in the cavity structure.
Further, the upper part and the lower part of the reaction chamber comprise an inner wall and an outer wall; the separation arrangement of the upper part of the reaction chamber and the lower part of the reaction chamber comprises an inner wall separation arrangement and an outer wall separation arrangement; the inner wall and the outer wall are made of carbon steel, and a cavity structure is arranged between the inner wall and the outer wall and is used for introducing cooling circulating water.
The cavity structure on the reaction chamber wall is used for loading cooling circulating water, so that the cooling wall structure of the reaction chamber is realized, the wall temperature of the reaction furnace is controlled in a lower temperature range, and hidden danger caused by overhigh temperature of the furnace wall is avoided. Only the inner wall and the outer wall of the upper part of the reaction chamber and the inner wall and the outer wall of the lower part of the reaction chamber are separated and arranged at the same time, so that the lower part of the reaction chamber can vertically and vertically move relative to the upper part in a regulating manner.
Furthermore, the height of the reaction chamber of the acetylene furnace with adjustable reaction time is 400+/-50 mm, and the inscribed circle size of the upper part of the reaction chamber is phi 600+/-50 mm.
The upper part and the lower part of the reaction chamber are arranged in a separated mode in the height direction, namely reaction gas enters from an acetylene furnace burner plate connected with the upper part of the reaction chamber, flows downwards along the axial direction of the reaction chamber, enters the lower part of the reaction chamber, enters a quenching system from the bottom end of the lower part of the reaction chamber, and the height of the reaction chamber is the height of the whole reaction chamber under the normal state of the upper part and the lower part of the reaction chamber (before the lower part of the reaction chamber moves in the vertical direction). The height of the reaction chamber is combined with the size of an inscribed circle at the upper part of the reaction chamber, and the height of the reaction chamber can be used as preliminary data of ventilation capacity of the reaction chamber and used for calculating productivity and the like.
Furthermore, the inner wall of the upper part of the reaction chamber and the inner wall of the lower part of the reaction chamber are downward closing structures with the cross section area of the upper part being more than or equal to that of the lower part; the angle between the inner wall of the upper part of the reaction chamber and the inner wall of the lower part of the reaction chamber and the perpendicular bisector of the reaction chamber is preferably designed to be 0-9 °, more preferably 7±2°.
The closing-in structure is provided with a cold extraction device which utilizes gas to concentrate into the lower part, so that the utility model designs angles and preferred angles for closing-in.
Further, the cross section of the inner wall of the reaction chamber is regular hexagon or round.
Further, the lower part of the reaction chamber and the upper part of the reaction chamber are respectively and independently provided with a cooling circulating water inlet and a cooling circulating water outlet; the cooling circulating water outlet at the lower part of the reaction chamber is connected with the cooling circulating water inlet at the upper part of the reaction chamber.
The utility model also provides application of the reaction time-adjustable acetylene furnace reaction chamber in a natural gas acetylene production process, wherein the acetylene furnace reaction chamber, an acetylene furnace burner plate and a quenching system are jointly arranged in a closed cavity structure, the upper part of the closed cavity structure is connected with a gas mixing device, and the lower part of the closed cavity structure is provided with a pyrolysis gas outlet.
The reaction pressure of the reaction chamber is 0-0.1 MPa, and the reaction temperature is 1300-1500 ℃.
It can be seen that the acetylene furnace reaction chamber provided by the utility model belongs to a part of components in the acetylene furnace reactor for preparing acetylene from natural gas. Therefore, the design of airtight connection between the upper part of the reaction chamber and the lower part of the reaction chamber can be omitted, because even if the lower part of the reaction chamber needs a certain distance from the upper part of the reaction chamber because of height adjustment, part of the reaction gas escaping from the connection part of the reaction chamber and the reaction chamber is still in the cavity structure, and the gas is discharged from a cracking gas outlet after the reaction.
Compared with the prior art, the utility model has the advantages that:
according to the utility model, the reaction chamber of the acetylene furnace is designed into an upper part and a lower part, and the distance between the upper part and the lower part is changed through relative fixation and movement, so that the overall height of the reaction chamber is adjustable, thus the total height of the reaction chamber can be regulated and controlled to be a reasonable value according to the requirements of the air inflow in the reaction chamber, such as the proportion, the speed, the productivity and the like, the residence time of the gas in the reaction chamber is always controlled in an optimal reaction time interval, the maximum acetylene yield in the partial oxidation process of natural gas is ensured, and the problems of acetylene yield reduction and the like caused by insufficient reaction time or overlong reaction time are solved.
Drawings
These and/or other aspects and advantages of the present utility model will become more apparent and more readily appreciated from the following detailed description of the embodiments of the utility model, taken in conjunction with the accompanying drawings, wherein:
FIG. 1 is a schematic diagram of the front view of an acetylene furnace reaction chamber with adjustable reaction time according to an embodiment of the present utility model; wherein, the upper part of the 101-reaction chamber, the lower part of the 102-reaction chamber, the water inlet of the lower part of the 1-reaction chamber, the water outlet of the lower part of the 2-reaction chamber, the water inlet of the upper part of the 3-reaction chamber, the water outlet of the upper part of the 4-reaction chamber and the 5-height adjusting part.
Fig. 2 is a schematic top view of a reaction chamber of an acetylene furnace with adjustable reaction time according to an embodiment of the present utility model, that is, a top view corresponding to the front view shown in fig. 1.
Detailed Description
The present utility model will be described in further detail below with reference to the drawings and detailed description for the purpose of enabling those skilled in the art to understand the utility model better.
Example 1
The structure of the reaction chamber of the acetylene furnace with adjustable reaction time is shown in figure 1, the reaction chamber is divided into an upper part and a lower part, the lower part is provided with a height adjusting part, preferably an adjustable fixing part such as a bolt, and the reaction chamber specifically comprises: a reaction chamber upper portion 101 and a reaction chamber lower portion 102. The cross section of the reaction chamber is regular hexagon, the inner wall is of a downward closing structure in the vertical direction, the inclination angle is 7 degrees, namely the included angle between the inner wall and the vertical line is 7 degrees.
The upper part of the reaction chamber upper part 101 is adjacent to an acetylene reaction furnace mixing zone which is used for realizing uniform mixing of hydrocarbon and oxygen, and then enters the reaction chamber (comprising the reaction chamber upper part 101 and the reaction chamber lower part 102) through a burner plate with n regular triangle burners uniformly distributed, and oxidation reaction occurs in the reaction chamber, so that acetylene and other byproducts are generated. The pyrolysis gas rapidly passes through the reaction chamber along the common central axis direction of the upper part 101 and the lower part 102 of the reaction chamber, and is cooled down by the extraction cooling medium in the extraction cooling zone, so as to terminate the reaction. The outer walls of the extraction cooling areas adjacent to the lower part 102 of the reaction chamber are provided with nozzles, extraction cooling medium is axially sprayed into the center of the furnace from the nozzles, and pyrolysis gas is uniformly contacted with the extraction cooling medium to be cooled.
The reaction chamber comprising the upper part 101 and the lower part 102 adopts a cold wall structure, circulating water enters the circulating jacket from the water inlet 1 at the lower part of the reaction chamber, then leaves the circulating jacket from the water outlet 2 at the lower part of the reaction chamber, and part of heat in the acetylene furnace is taken away, so that the furnace wall is maintained in a low-temperature state. The circulating water enters the upper water inlet 3 of the reaction chamber through a hose connected with the lower water outlet 2 of the reaction chamber, and leaves the circulating jacket from the upper water outlet 4 of the reaction chamber after part of heat at the upper part of the reaction chamber is circularly taken away.
When the capacity of the apparatus was designed to be 1 ten thousand tons/year and the production load was 100%, the height of the reaction chamber was 400mm, and the inscribed circle in the upper portion 101 of the reaction chamber had a size of Φ600mm. In this case, the optimum oxidation time is 20ms, and the highest acetylene yield can be obtained.
Further, the reaction chamber lower part 102 may be adjusted in the up-down position by a height adjusting member 5 such as a bolt. Specifically, when the production load of the apparatus is increased to 120%, the amount of the corresponding reaction furnace gas (including natural gas and oxygen) is increased, the gas velocity is increased, and the residence time of the gas, i.e., the oxidation reaction time, is too short, which may cause insufficient reaction progress and decrease in acetylene yield. At this time, the lower part 102 of the reaction chamber is moved downward away from the upper part of the reaction chamber by adjusting the height adjusting part 5, such as a bolt, so that the overall height of the reaction chamber is increased by 10%, and the extraction cooling zone immediately adjacent to the bottom of the lower part 102 of the reaction chamber is correspondingly translated downward, thereby increasing the time of passing the pyrolysis gas through the reaction chamber and maintaining the optimal reaction time of 20ms and product yield.
Further, when the production load of the device is reduced to 80%, the air inflow (comprising natural gas and oxygen) of the corresponding reaction furnace is reduced, the air speed is reduced, the residence time of the gas, namely the oxidation reaction time, is too long, so that the reaction is not terminated timely, the acetylene product is further cracked into hydrogen and carbon black, and the acetylene yield is reduced. At this time, the lower part 102 of the reaction chamber is closed to the upper part of the reaction chamber by adjusting the height adjusting part 5 such as a bolt, the overall height of the reaction chamber is reduced by 10%, and the extraction cooling zone immediately adjacent to the bottom of the lower part 102 of the reaction chamber is correspondingly translated upwards, so that the time for the pyrolysis gas to pass through the reaction chamber is shortened, and the optimal reaction time of 20ms and the product yield are maintained.
In another embodiment of the utility model, the cross section of the reaction chamber is circular, the inclination angle of the inner wall is 0 degrees, i.e. the inner wall is vertical.
Example 2
The structure of the reaction chamber of the acetylene furnace with adjustable reaction time is shown in figure 1, and the reaction chamber is divided into an upper part and a lower part, and specifically comprises: the bottom ends of the reaction chamber lower part 102 and the reaction chamber upper part 101 are provided with bolts for fixing the reaction chamber lower part 102 away from or near the reaction chamber upper part 101. The cross section of the reaction chamber is regular hexagon, the inner wall is of a downward closing structure in the vertical direction, the inclination angle is 7 degrees, namely the included angle between the inner wall and the vertical line is 7 degrees.
The upper part of the reaction chamber upper part 101 is adjacent to an acetylene reaction furnace mixing zone which is used for realizing uniform mixing of hydrocarbon and oxygen, and then the mixture enters the reaction chamber (comprising the reaction chamber upper part 101 and the reaction chamber lower part 102) through a burner plate with n regular triangle burners uniformly distributed, and oxidation reaction occurs in the reaction chamber to generate acetylene and other byproducts. The pyrolysis gas rapidly passes through the reaction chamber along the common central axis direction of the upper part 101 and the lower part 102 of the reaction chamber, and is cooled down by the extraction cooling medium in the extraction cooling zone, so as to terminate the reaction. The outer wall of the extraction cooling zone adjacent to the lower part of the reaction chamber is provided with a nozzle, the extraction cooling medium is axially sprayed into the center of the furnace from the nozzle, and the pyrolysis gas is uniformly contacted with the extraction cooling medium to cool.
The reaction chamber comprising the upper part 101 and the lower part 102 adopts a cold wall structure, circulating water enters the circulating jacket from the water inlet 1 at the lower part of the reaction chamber, then leaves the circulating jacket from the water outlet 2 at the lower part of the reaction chamber, and part of heat in the acetylene furnace is taken away, so that the furnace wall is maintained in a low-temperature state. The circulating water enters the upper water inlet 3 of the reaction chamber through a hose connected with the lower water outlet 2 of the reaction chamber, and leaves the circulating jacket from the upper water outlet 4 of the reaction chamber after part of heat at the upper part of the reaction chamber is circularly taken away.
When the production load of the device is 1 ten thousand tons/year, the height of the reaction chamber is 400mm, and the inscribed circle in the upper part 101 of the reaction chamber has a dimension phi 600mm. At this time, the content of C2-type gas (e.g., ethane) in the raw natural gas was 0.5%. In this case, the oxidation reaction time was set to an optimum value of 20ms, and the highest acetylene yield was obtained.
When the content of C2 gas (such as ethane) in the raw natural gas is increased to 2.8%, the retention time of the gas required, namely the oxidation reaction time, is shortened because the cracking difficulty is reduced. At this time, the lower part 102 of the reaction chamber is close to the upper part 101 of the reaction chamber by adjusting the height adjusting part, the overall height of the reaction chamber is reduced by about 2%, and the extraction cooling zone adjacent to the bottom of the lower part 102 of the reaction chamber is correspondingly translated upwards, so that the time for the pyrolysis gas to pass through the reaction chamber is shortened, and the optimal reaction time and product yield are maintained.
The foregoing description of embodiments of the utility model has been presented for purposes of illustration and description, and is not intended to be exhaustive or limited to the embodiments disclosed. Many modifications and variations will be apparent to those of ordinary skill in the art without departing from the scope and spirit of the various embodiments described. Therefore, the protection scope of the present utility model should be subject to the protection scope of the claims.

Claims (8)

1. The reaction chamber of the acetylene furnace with adjustable reaction time is characterized by comprising an upper part (101) and a lower part (102) of the reaction chamber;
the top end of the upper part (101) of the reaction chamber is connected with an acetylene furnace burner plate, and the lower end of the lower part (102) of the reaction chamber is connected with a quenching system; the upper part (101) of the reaction chamber is separated from the lower part (102) of the reaction chamber;
a height adjusting component (5) is arranged on one of the upper part (101) and the lower part (102) of the reaction chamber; the height adjusting component (5) is an adjustable fixing component and is used for enabling the upper part (101) or the lower part (102) of the reaction chamber to move in the vertical direction, so that the distance between the upper part (101) and the lower part (102) of the reaction chamber is controlled and adjusted, and the reaction time of the gas in the reaction chamber is controlled and controlled by adjusting the height of the reaction chamber of the acetylene furnace;
the reaction chamber of the acetylene furnace with adjustable reaction time is arranged in a closed cavity structure.
2. The reaction chamber of the acetylene furnace with adjustable reaction time according to claim 1, wherein the upper part (101) and the lower part (102) of the reaction chamber comprise an inner wall and an outer wall;
the separation arrangement of the upper part (101) of the reaction chamber and the lower part (102) of the reaction chamber comprises an inner wall separation arrangement and an outer wall separation arrangement;
the inner wall and the outer wall are made of carbon steel;
and a cavity structure is arranged between the inner wall and the outer wall and is used for introducing cooling circulating water.
3. The reaction chamber of an acetylene furnace with adjustable reaction time according to claim 1, wherein the height of the reaction chamber of the acetylene furnace with adjustable reaction time is 400 + -50 mm, and the inscribed circle of the upper part (101) of the reaction chamber has a dimension phi 600 + -50 mm.
4. The reaction chamber of the acetylene furnace with adjustable reaction time according to claim 2, wherein the inner walls of the upper part (101) and the lower part (102) of the reaction chamber are downward closing structures with the upper cross-sectional area being larger than or equal to the lower cross-sectional area.
5. The reaction chamber of the acetylene furnace with adjustable reaction time according to claim 4, wherein the angle between the inner wall of the upper part (101) of the reaction chamber and the inner wall of the lower part (102) of the reaction chamber and the perpendicular bisector of the reaction chamber is 0-9 degrees.
6. The reaction chamber of an acetylene furnace with adjustable reaction time according to claim 5, wherein the angle between the inner wall of the upper part (101) and the inner wall of the lower part (102) of the reaction chamber and the perpendicular bisector of the reaction chamber is 7+ -2 °.
7. The reaction chamber of an acetylene furnace with adjustable reaction time according to claim 1, wherein the cross section of the inner wall of the reaction chamber is regular hexagon or circle.
8. The reaction chamber of the acetylene furnace with adjustable reaction time according to claim 2, wherein a cooling circulating water inlet and a cooling circulating water outlet are respectively and independently arranged on the lower part (102) and the upper part (101) of the reaction chamber; the cooling circulating water outlet of the lower part (102) of the reaction chamber is connected with the cooling circulating water inlet of the upper part (101) of the reaction chamber.
CN202220061218.8U 2021-04-14 2022-01-11 Acetylene furnace reaction chamber with adjustable reaction time Active CN219441611U (en)

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CN202120757701 2021-04-14
CN2021207577015 2021-04-14

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Effective date of registration: 20240611

Address after: No. 1788, Development Zone Avenue, Ruian Dongshan Economic Development Zone, Wenzhou City, Zhejiang Province, 325200

Patentee after: Huafeng Chemical Co.,Ltd.

Country or region after: China

Address before: 100080 room 1701, unit 1, building 22, shuangqingyuan, Haidian District, Beijing

Patentee before: Wang Jinfu

Country or region before: China