CN219377143U - Reaction device for preparing P-204 phosphate - Google Patents
Reaction device for preparing P-204 phosphate Download PDFInfo
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- CN219377143U CN219377143U CN202320686100.9U CN202320686100U CN219377143U CN 219377143 U CN219377143 U CN 219377143U CN 202320686100 U CN202320686100 U CN 202320686100U CN 219377143 U CN219377143 U CN 219377143U
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- alkalizing
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Abstract
The reaction device for preparing the P-204 phosphate comprises an alkalizing tank for carrying out reaction, a feeding pump arranged on a transfusion tube, a discharging tube arranged at one side of the bottom end of the alkalizing tank, a stirring motor, a stirring shaft, an auxiliary heating component and a flow dividing piece, wherein the auxiliary heating component is arranged at one side of the alkalizing tank, and the flow dividing piece connected with a feeding tube is arranged at the top of the inner side of the alkalizing tank; the auxiliary heating assembly comprises a liquid suction pipe, a control valve, a return pipe and a return pump, wherein the liquid suction pipe is arranged at the bottom of the alkalization tank, the control valve is arranged on the liquid suction pipe, one end of the liquid suction pipe is connected with a vertical pipe, and the circulating pump is arranged on the vertical pipe.
Description
Technical Field
The utility model relates to a reaction device, in particular to a reaction device for preparing P-204 phosphate.
Background
The preparation of P-204 phosphate, first, requires the alkalization of the mixed octyl esters, the process is:
1. the mixed octyl ester is pumped into a metering tank (a sealed tank with a weight sensor) for weight metering, and the metered mixed octyl ester is pumped from the metering tank into a sealed alkalization tank.
2. According to the concentration and weight of the mixed octyl ester, the weight of the alkali liquor required is calculated, the alkali liquor is pumped into a metering tank from an alkali liquor tank, the alkali liquor is pumped into an alkalization tank from the metering tank after the alkali liquor with the required weight is weighed out by the metering tank, the mixed liquor of the mixed octyl ester and the alkali liquor in the alkalization tank is heated and stirred by a stirring assembly, and after the alkali liquor tank is kept warm for a period of time, the alkalization process can generate gas to raise the pressure in the tank, the alkalization reaction is completed, and the solution is pressed into a hydration tank communicated with the alkalization tank through a pipeline by the pressure in the tank.
When the existing reaction device for preparing the P-204 phosphate is used, the added alkali liquor enters into contact with the mixed octyl ester at a charging port, so that the contact uniformity is poor, the mixing efficiency is reduced, meanwhile, when the mixed liquor is subjected to heating reaction, only the side wall is heated, the heating efficiency in the middle of the mixed liquor is low, the reaction efficiency is influenced, and the use is not facilitated.
Disclosure of Invention
Aiming at the situation, in order to overcome the defects of the prior art, the utility model provides the reaction device for preparing the P-204 phosphate, which effectively solves the problems that when the existing reaction device for preparing the P-204 phosphate is used, the added alkali liquor enters into contact with the mixed octyl ester at a charging port, the contact uniformity is poor, the mixing efficiency is reduced, and meanwhile, when the mixed liquor is heated for reaction, the side wall is heated, the heating efficiency in the middle part of the mixed liquor is low, the reaction efficiency is influenced, and the use is not facilitated.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model comprises an alkalizing tank for reaction, a feeding pipe arranged at the top end of the alkalizing tank, a metering tank connected with the feeding pipe through a transfusion pipe, a feeding pump arranged on the transfusion pipe, a discharging pipe arranged at one side of the bottom end of the alkalizing tank, a stirring motor, a stirring shaft, an auxiliary heating component and a flow dividing piece, wherein the auxiliary heating component is arranged at one side of the alkalizing tank, and the flow dividing piece connected with the feeding pipe is arranged at the top of the inner side of the alkalizing tank;
the auxiliary heating subassembly includes liquid suction pipe, control valve, standpipe, circulating pump, heating inner box, heating outer box, heating liquid, heater strip, back flow and backwash pump, and the liquid suction pipe sets up in the bottom of alkalization jar, installs the control valve on the liquid suction pipe, and the one end of liquid suction pipe is connected with the standpipe, installs the circulating pump on the standpipe, and the one end of standpipe is connected with the heating inner box, and the externally mounted of heating inner box has the heating outer box, and the inside of heating outer box is filled with the heating liquid, and the heater strip is installed to the bottom of heating outer box inboard, and the opposite side of heating inner box is connected with the back flow, installs the backwash pump on the back flow.
Preferably, one end of the return pipe is spliced at the top of the alkalizing tank.
Preferably, a heat insulation sleeve is arranged outside the alkalizing tank, and a spiral heating wire is embedded and installed in the inner wall of the alkalizing tank.
Preferably, the middle part at the top end of the alkalizing tank is provided with a stirring motor, and the bottom end of the stirring motor is provided with a stirring shaft positioned in the alkalizing tank.
Preferably, the shunt piece includes shunt tubes, arc portion, shunt ports and connector, and the shunt tubes is fixed at the inboard top of alkalization jar, and the middle part of shunt tubes is provided with arc portion, and the bottom of shunt tubes and arc portion evenly is provided with a plurality of shunt ports, and the one end of shunt tubes is provided with the connector of being connected with the inlet pipe.
Preferably, the discharge pipe is connected to an external hydration tank by a pipe.
The beneficial effects are that: when the alkali liquor mixing device is used, mixed octyl ester is pumped into the metering tank, after the weight is measured, the mixed octyl ester is fed into the alkalization tank through the feeding pump, the weight of alkali liquor required is calculated according to the concentration and the weight of the mixed octyl ester, alkali liquor is pumped into the metering tank from the alkali liquor tank, after the alkali liquor with the required weight is weighed out by the metering tank, the alkali liquor entering the alkalization tank through the feeding pipe is pumped into the alkalization tank through the feeding pump of the metering tank, finally the alkali liquor is discharged through the shunt pipe and the shunt port on the arc-shaped part, so that the alkali liquor can be uniformly added into the mixed octyl ester solution in the alkalization tank, the mixing efficiency of the mixed octyl ester and the alkali liquor is improved, when the mixed octyl ester and the alkali liquor are mixed and heated, a control valve is opened, the circulating pump works to convey the mixed liquor in the middle part of the inner bottom end of the alkalization tank into the heating inner tank through the standpipe, the heating liquor in the heating outer tank is heated by the heating wire arranged at the bottom, the mixed octyl ester and the alkali liquor in the heating inner tank is heated through the heating wire, the heated mixed octyl ester and the alkali liquor in the heating tank is returned into the alkalization tank through the heating tank after the heating, and the mixed octyl ester and the mixed liquor is heated into the alkalization tank. The utility model has novel structure and ingenious conception, ensures that the alkali liquor can be uniformly added into the mixed octyl ester solution in the alkalizing tank, improves the mixing efficiency of the mixed octyl ester and the alkali liquor, and can circularly heat the outer side and the middle part of the mixed liquor during heating so as to accelerate the mixing heating efficiency of the mixed octyl ester and the alkali liquor in the alkalizing tank.
Drawings
The accompanying drawings are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate the utility model and together with the embodiments of the utility model, serve to explain the utility model. In the drawings:
FIG. 1 is a schematic view of the overall structure of the present utility model;
FIG. 2 is a schematic view of the internal structure of the heating outer box of the present utility model;
FIG. 3 is a schematic view of the diverter according to the present utility model;
reference numerals in the drawings: 1. an alkalizing tank; 2. a feed pipe; 3. a feed pump; 4. a metering tank; 5. a discharge pipe; 6. a stirring motor; 7. a stirring shaft; 8. an auxiliary heating assembly; 9. a shunt; 801. a liquid suction pipe; 802. a control valve; 803. a standpipe; 804. a circulation pump; 805. heating the inner box; 806. heating the outer box; 807. heating the liquid; 808. a heating wire; 809. a return pipe; 810. a reflux pump; 91. a shunt; 92. an arc-shaped portion; 93. a shunt port; 94. and (5) a connector.
Detailed Description
The following describes embodiments of the present utility model in further detail with reference to FIGS. 1-3.
1-3, the utility model provides a reaction device for preparing P-204 phosphate, which comprises an alkalizing tank 1 for reaction, a feed pipe 2 arranged at the top end of the alkalizing tank 1, a metering tank 4 connected with the feed pipe 2 through a transfusion pipe, a feed pump 3 arranged on the transfusion pipe, a discharge pipe 5 arranged at one side of the bottom end of the alkalizing tank 1, a stirring motor 6, a stirring shaft 7, an auxiliary heating component 8, a flow dividing component 9, a liquid suction pipe 801, a control valve 802, a vertical pipe 803, a circulating pump 804, a heating inner tank 805, a heating outer tank 806, heating liquid 807, a heating wire 808, a return pipe 809, a return pump 810, a flow dividing pipe 91, an arc-shaped part 92, a flow dividing port 93 and a connector 94, wherein the auxiliary heating component 8 arranged at one side of the alkalizing tank 1, and the flow dividing component 9 connected with the feed pipe 2 is arranged at the top of the inner side of the alkalizing tank 1;
the auxiliary heating assembly 8 comprises a liquid extracting pipe 801, a control valve 802, a vertical pipe 803, a circulating pump 804, a heating inner box 805, a heating outer box 806, heating liquid 807, a heating wire 808, a return pipe 809 and a return pump 810, wherein the liquid extracting pipe 801 is arranged at the bottom of the alkalizing tank 1, the control valve 802 is arranged on the liquid extracting pipe 801, one end of the liquid extracting pipe 801 is connected with the vertical pipe 803, the circulating pump 804 is arranged on the vertical pipe 803, one end of the vertical pipe 803 is connected with the heating inner box 805, the heating outer box 806 is arranged outside the heating inner box 805, the heating liquid 807 is filled in the heating outer box 806, the heating wire 808 is arranged at the bottom of the inner side of the heating outer box 806, the return pipe 809 is connected with the other side of the heating inner box 805, and the return pump 810 is arranged on the return pipe 809.
One end of the return pipe 809 is inserted into the top of the alkalizing tank 1, so that the return pipe 809 is convenient to connect and use.
The outside of the alkalization tank 1 is provided with a heat preservation sleeve, and a spiral heating wire is embedded and installed in the inner wall of the alkalization tank 1, so that the alkalization tank 1 is conveniently heated.
The middle part at the top of the alkalization tank 1 is provided with a stirring motor 6, and the bottom end of the stirring motor 6 is provided with a stirring shaft 7 positioned inside the alkalization tank 1, so that the inside of the alkalization tank 1 is conveniently stirred.
The shunt piece 9 includes shunt tubes 91, arc portion 92, shunt ports 93 and connector 94, shunt tubes 91 fix at the inboard top of alkalization jar 1, the middle part of shunt tubes 91 is provided with arc portion 92, the bottom of shunt tubes 91 and arc portion 92 evenly is provided with a plurality of shunt ports 93, the one end of shunt tubes 91 is provided with the connector 94 of being connected with inlet pipe 2, during the use, the alkali lye that will enter into in the alkalization jar 1 through inlet pipe 2 enters into the inside of shunt tubes 91 through connector 94, finally the alkali lye is discharged through shunt tubes 91 and shunt ports 93 on arc portion 92 for the mixed octyl ester solution in the alkalization jar 1 is added to the alkali lye that can be comparatively even, the mixing efficiency of mixed octyl ester and alkali lye is improved.
The discharging pipe 5 is connected with an external hydration tank through a pipeline, so that the use is convenient.
Working principle: when the mixed octyl ester is used, the mixed octyl ester is pumped into the metering tank 4, after the weight is measured, the mixed octyl ester is fed into the alkalization tank 1 through the feeding pump 3, the weight of the alkali liquor required is calculated according to the concentration and the weight of the mixed octyl ester, the alkali liquor is pumped into the metering tank 4 from the alkali liquor tank, the alkali liquor with the required weight is weighed out by the metering tank 4, the alkali liquor is pumped into the alkalization tank 1 through the feeding pump 3 of the metering tank 4, the alkali liquor entering the alkalization tank 1 through the feeding pipe 2 enters the inside of the shunt tube 91 through the connector 94, finally the alkali liquor is discharged through the shunt tube 91 and the shunt opening 93 on the arc-shaped part 92, so that the alkali liquor can be uniformly added into the mixed octyl ester solution in the alkalization tank 1, the mixing efficiency of the mixed octyl ester and the alkali liquor is improved, when the mixed octyl ester and the alkali liquor are mixed and heated, the control valve 802 is opened, the circulating pump 804 works to convey the mixed liquor in the middle of the bottom end of the alkalization tank 1 into the heating inner tank 805 through the liquid pumping pipe 801, the heating liquid 807 is heated by the heating wire 808 installed at the bottom, the heating liquid in the heating tank 807, the mixed liquor in the heating tank mixed octyl ester and the mixed liquor is returned into the alkalization tank 1 through the heating tank 803, and mixed liquor is heated by the mixed liquor in the heating tank 803 after the mixed liquor.
The beneficial effects are that: the utility model has novel structure and ingenious conception, ensures that the alkali liquor can be uniformly added into the mixed octyl ester solution in the alkalizing tank 1, improves the mixing efficiency of the mixed octyl ester and the alkali liquor, and can circularly heat the outer side and the middle part of the mixed liquor during heating so as to accelerate the mixing heating efficiency of the mixed octyl ester and the alkali liquor in the alkalizing tank 1.
All electric parts and the adaptive power supply are connected through wires by the person skilled in the art, and a proper controller and encoder should be selected according to actual conditions so as to meet control requirements, specific connection and control sequence, and the electric connection is completed by referring to the following working principles in the working sequence among the electric parts, and the detailed connection means are known in the art, and mainly introduce the working principles and processes as follows, and do not describe the electric control.
Finally, it should be noted that: the foregoing description is only a preferred embodiment of the present utility model, and the present utility model is not limited thereto, but it is to be understood that modifications and equivalents of some of the technical features described in the foregoing embodiments may be made by those skilled in the art, although the present utility model has been described in detail with reference to the foregoing embodiments. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present utility model should be included in the protection scope of the present utility model.
Claims (6)
1. The utility model provides a reaction unit for preparing P-204 phosphate, is including being used for carrying out the alkalization jar (1) of reaction, inlet pipe (2) that alkalization jar (1) top set up, metering tank (4) that pass through the transfer line connection on inlet pipe (2), feeding pump (3) of installation on the transfer line and discharging pipe (5) that alkalization jar (1) bottom one side set up, its characterized in that: the device is characterized by further comprising a stirring motor (6), a stirring shaft (7), an auxiliary heating component (8) and a flow dividing component (9), wherein the auxiliary heating component (8) is arranged on one side of the alkalizing tank (1), and the flow dividing component (9) connected with the feeding pipe (2) is arranged at the top of the inner side of the alkalizing tank (1);
auxiliary heating subassembly (8) are including drawing liquid pipe (801), control valve (802), standpipe (803), circulating pump (804), heating inner box (805), heating outer box (806), heating liquid (807), heater strip (808), back flow (809) and backwash pump (810), drawing liquid pipe (801) set up in the bottom of alkalization jar (1), install control valve (802) on drawing liquid pipe (801), the one end of drawing liquid pipe (801) is connected with standpipe (803), install circulating pump (804) on standpipe (803), the one end of standpipe (803) is connected with heating inner box (805), the externally mounted of heating inner box (805) has heating outer box (806), the inside packing of heating outer box (806) has heating liquid (807), heating wire (808) are installed to the bottom of heating outer box (806) inboard, the opposite side of heating inner box (805) is connected with back flow (809), install backwash pump (810) on back flow (809).
2. A reaction apparatus for producing P-204 phosphate as claimed in claim 1, wherein: one end of the return pipe (809) is inserted into the top of the alkalizing tank (1).
3. A reaction apparatus for producing P-204 phosphate as claimed in claim 1, wherein: the outside of alkalization jar (1) is provided with the insulation cover, inserts in the inner wall of alkalization jar (1) and installs spiral heater strip.
4. A reaction apparatus for producing P-204 phosphate as claimed in claim 1, wherein: the middle part at the top of the alkalizing tank (1) is provided with a stirring motor (6), and the bottom of the stirring motor (6) is provided with a stirring shaft (7) positioned in the alkalizing tank (1).
5. A reaction apparatus for producing P-204 phosphate as claimed in claim 1, wherein: the shunt piece (9) comprises a shunt tube (91), an arc-shaped part (92), a shunt opening (93) and a connector (94), wherein the shunt tube (91) is fixed at the top of the inner side of the alkalization tank (1), the arc-shaped part (92) is arranged in the middle of the shunt tube (91), a plurality of shunt openings (93) are uniformly arranged at the bottom ends of the shunt tube (91) and the arc-shaped part (92), and the connector (94) connected with the feeding pipe (2) is arranged at one end of the shunt tube (91).
6. A reaction apparatus for producing P-204 phosphate as claimed in claim 1, wherein: the discharging pipe (5) is connected with an external hydration tank through a pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320686100.9U CN219377143U (en) | 2023-03-31 | 2023-03-31 | Reaction device for preparing P-204 phosphate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320686100.9U CN219377143U (en) | 2023-03-31 | 2023-03-31 | Reaction device for preparing P-204 phosphate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219377143U true CN219377143U (en) | 2023-07-21 |
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ID=87200126
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320686100.9U Active CN219377143U (en) | 2023-03-31 | 2023-03-31 | Reaction device for preparing P-204 phosphate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219377143U (en) |
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2023
- 2023-03-31 CN CN202320686100.9U patent/CN219377143U/en active Active
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