CN219356220U - Reaction kettle with rectification structure - Google Patents
Reaction kettle with rectification structure Download PDFInfo
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- CN219356220U CN219356220U CN202320168637.6U CN202320168637U CN219356220U CN 219356220 U CN219356220 U CN 219356220U CN 202320168637 U CN202320168637 U CN 202320168637U CN 219356220 U CN219356220 U CN 219356220U
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- separation disc
- kettle body
- stirring block
- stirring
- kettle
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model provides a reaction kettle with a rectification structure, which comprises a kettle body, wherein an evaporator is arranged at the bottom end inside the kettle body, a motor is arranged at the top end inside the kettle body, a condenser is arranged at one side of the motor, a stirring rod is arranged at the bottom of the motor, an auxiliary contact assembly is arranged at the outer side of the stirring rod, and an auxiliary mixing assembly is arranged inside the auxiliary contact assembly; the auxiliary contact assembly comprises a first separation disc, a second separation disc and a connecting block, wherein a communication port is formed in the middle of the first separation disc, and a plurality of connecting blocks are arranged on the inner side of the communication port. According to the utility model, through the arrangement of the evaporator and the condenser, the reactants in the kettle body can be evaporated and discharged, volatile substances of the reactants can be conveniently collected or the concentration of the reactants in the reactants can be conveniently changed, and meanwhile, the first separation disc and the second separation disc which are sequentially distributed can improve the flowing length of the volatile substances, and the contact time of evaporation gas and liquid can be improved, so that the rectification efficiency of the reaction kettle can be conveniently improved.
Description
Technical Field
The utility model relates to the technical field of chemical equipment, in particular to a reaction kettle with a rectification structure.
Background
Corrosion inhibitors are chemical substances or compounds that, when present in an environment (medium) in a suitable concentration and form, can prevent or slow down the corrosion of materials, and thus can also be referred to as corrosion inhibitors. The dosage of the composition is small (0.1% -1%), but the effect is obvious; this method of protecting metals is known as corrosion inhibitor protection;
during processing, the corrosion inhibitor is generally prepared by putting reactants into a reaction kettle, carrying out chemical reaction on materials in the reaction kettle in a heating process, and mixing and stirring the reacted materials by a stirring mechanism in the reaction kettle; however, in the chemical reaction process of the mixture in the reaction kettle, it is difficult for a worker to change the concentration of the reactant in the reaction kettle or obtain volatile substances in the reactant, the purity of the obtained substances by simple distillation is insufficient, the production requirement cannot be met, and a multistage distillation tank needs to be arranged, so that the cost is high; in addition, in production, repeated reaction treatment is required to be carried out after the reactant to be reacted in the reaction kettle is reacted, and the material reaction is not convenient and sufficient.
In summary, there is a need for a reactor that can rectify internal reactants.
Disclosure of Invention
Aiming at the defects of the prior art, the utility model provides a reaction kettle with a rectification structure, and solves the problems in the background art.
In order to achieve the above purpose, the utility model is realized by the following technical scheme:
the reaction kettle with the rectification structure comprises a kettle body, wherein an evaporator is arranged at the bottom end inside the kettle body, a motor is arranged at the top end inside the kettle body, a condenser is arranged on one side of the motor, a stirring rod is arranged at the bottom of the motor, an auxiliary contact assembly is arranged outside the stirring rod, an auxiliary mixing assembly is arranged inside the auxiliary contact assembly, and the evaporator and the condenser together form a rectification structure for circulating distillation;
the auxiliary contact assembly comprises a first separation disc, a second separation disc and a connecting block, wherein a communication port is formed in the middle of the first separation disc, a plurality of connecting blocks are arranged on the inner side of the communication port, the inner end of each connecting block is connected with the outer side of the stirring rod, and the second separation disc is arranged on the outer side of the stirring rod.
Further, the first separation disc and the second separation disc are arranged in a plurality, and the first separation disc and the second separation disc are distributed and arranged at equal intervals in sequence.
Further, the outer side of the second separation disc is spaced from the inner wall of the kettle body, and the outer side of the first separation disc is in contact fit with the inner wall of the kettle body.
Further, a feeding pipe is arranged on one side of the top end of the kettle body, a liquid discharge pipe is arranged on the other side of the top end of the kettle body, the liquid discharge pipe is arranged on the side face of the condenser, an L-shaped return pipe is arranged at the bottom of the liquid discharge pipe, the return pipe is communicated with the inside of the kettle body, an air inlet pipe is arranged at the bottom of the condenser, and a liquid discharge pipe is arranged on one side of the bottom end of the kettle body.
Further, the stirring rod is rotationally connected with the kettle body with the first separation disc and the second separation disc, and the auxiliary mixing assembly is positioned at the intervals of the first separation disc and the second separation disc.
Further, the auxiliary mixing assembly is provided with a plurality of groups in the first separation disc and the second separation disc, the auxiliary mixing assembly comprises a first stirring block and a second stirring block, the first stirring block and the second stirring block are correspondingly arranged, the first stirring block and the second stirring block are contacted with the top surface or the bottom surface of the first separation disc and the top surface of the second separation disc, the distribution angles of the first stirring block and the second stirring block are different, and the first stirring block and the second stirring block are distributed in an annular shape.
Further, the auxiliary mixing assembly further comprises a heating rod, wherein the heating rod is arranged inside the first stirring block and the second stirring block, and the heating rod is arranged in the plurality of stirring blocks.
The utility model provides a reaction kettle with a rectification structure. Compared with the prior art, the method has the following beneficial effects:
through the setting of evaporimeter and condenser, can evaporate the discharge to the reactant of the internal portion of cauldron, be convenient for collect the volatile material of reactant or change the inside reactant concentration of reactant, the first separation dish that distributes in proper order simultaneously separates the dish with the second and can improve the length that volatile material flows, improves the duration of evaporating gas and liquid contact to improve the efficiency of reation kettle rectification.
Drawings
In order to more clearly illustrate the embodiments of the utility model or the technical solutions in the prior art, the drawings that are required in the embodiments or the description of the prior art will be briefly described, it being obvious that the drawings in the following description are only some embodiments of the utility model, and that other drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 shows a schematic structural view of a reaction vessel having a rectification structure of the present utility model;
FIG. 2 shows a schematic representation of a flattened side-view cross-section of the present utility model;
FIG. 3 shows a schematic structural view of a first spacer disk and a second spacer disk of the present utility model;
FIG. 4 shows a schematic structural view of the auxiliary mixing assembly of the present utility model;
the figure shows: 1. a kettle body; 11. a feed pipe; 12. a discharge pipe; 2. a motor; 21. a stirring rod; 3. a condenser; 31. a liquid discharge pipe; 32. a return pipe; 33. an air inlet pipe; 4. an evaporator; 5. an auxiliary contact assembly; 51. a first spacer; 511. a communication port; 52. a second spacer; 53. a connecting block; 6. an auxiliary mixing assembly; 61. a first stirring block; 62. a second stirring block; 63. and a heating rod.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the embodiments of the present utility model more clear, the technical solutions in the embodiments of the present utility model are clearly and completely described, and it is obvious that the described embodiments are some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Example 1
In order to solve the technical problems in the background technology, a reaction kettle with a rectification structure is provided as follows:
referring to fig. 1-3, the reaction kettle with the rectification structure provided by the utility model comprises a kettle body 1, wherein an evaporator 4 is arranged at the bottom end inside the kettle body 1, a motor 2 is arranged at the top end inside the kettle body 1, a condenser 3 is arranged at one side of the motor 2, a stirring rod 21 is arranged at the bottom of the motor 2, an auxiliary contact assembly 5 is arranged at the outer side of the stirring rod 21, an auxiliary mixing assembly 6 is arranged inside the auxiliary contact assembly 5, and the evaporator 4 and the condenser 3 together form a rectification structure for circulating distillation; the evaporator 4 and the condenser 3 are used for evaporating and condensing gas of the mixture in the kettle body 1;
the auxiliary contact assembly 5 comprises a first separation disc 51, a second separation disc 52 and a connecting block 53, wherein a communication port 511 is formed in the middle of the first separation disc 51, a plurality of connecting blocks 53 are arranged on the inner side of the communication port 511, the inner ends of the connecting blocks 53 are connected with the outer side of the stirring rod 21, the second separation disc 52 is arranged on the outer side of the stirring rod 21, a plurality of first separation discs 51 and second separation discs 52 are arranged in a sequential equidistant distribution manner, a space is reserved between the outer side of the second separation disc 52 and the inner wall of the kettle body 1, and the outer side of the first separation disc 51 is in contact fit with the inner side of the kettle body 1; the first separation discs 51 and the second separation discs 52 which are distributed at equal intervals can improve the flowing length of the reactant to be reacted and the evaporating gas in the kettle body 1;
a feed pipe 11 is arranged on one side of the top end of the kettle body 1, a liquid discharge pipe 31 is arranged on the other side of the top end of the kettle body 1, the liquid discharge pipe 31 is arranged on the side face of the condenser 3, an L-shaped return pipe 32 is arranged at the bottom of the liquid discharge pipe 31, the return pipe 32 is communicated with the inside of the kettle body 1, an air inlet pipe 33 is arranged at the bottom of the condenser 3, and a liquid discharge pipe 12 is arranged on one side of the bottom end of the kettle body 1; the arrangement of the liquid discharge pipe 31 and the return pipe 32 is convenient for controlling the volatile matters evaporated in the reaction kettle to be discharged or flow back into the kettle body 1;
when the reaction kettle is used, firstly reactants to be reacted are put into the kettle body 1 through the feed pipe 11, the reactants entering the kettle body 1 can carry out chemical reaction, at the moment, the evaporator 4 can evaporate materials in the kettle body 1, and evaporated gas can pass through the first partition plate 51 and the second partition plate 52 which are arranged, enter the condenser 3 through the air inlet pipe 33 and are discharged or flow back into the kettle body 1;
through the arrangement of the evaporator 4 and the condenser 3, the reactants in the kettle body 1 can be evaporated and discharged, volatile matters of the reactants can be collected conveniently or the concentration of the reactants in the reactants can be changed, meanwhile, the flowing length of the volatile matters can be increased through the first separation disc 51 and the second separation disc 52 which are distributed in sequence, the contact time of evaporation gas and liquid can be increased, and the rectification efficiency of the reaction kettle can be improved conveniently;
in this embodiment, the stirring rod 21, the first separation disc 51 and the second separation disc 52 are both rotatably connected with the kettle body 1, and the auxiliary mixing assembly 6 is located at the interval between the first separation disc 51 and the second separation disc 52; through the rotation connection of first separating disk 51, second separating disk 52 and cauldron body 1, be convenient for drive supplementary mixing assembly 6 and mix the stirring to the inside reactant of cauldron body 1, improve reaction efficiency.
Example two
As shown in fig. 1 to 4, on the basis of the above embodiment, the present embodiment further provides the following:
the auxiliary mixing assembly 6 is provided with a plurality of groups in the first separation disc 51 and the second separation disc 52, the auxiliary mixing assembly 6 comprises a first stirring block 61 and a second stirring block 62, the first stirring block 61 and the second stirring block 62 are correspondingly arranged, the first stirring block 61 and the second stirring block 62 are contacted with the top surface or the bottom surface of the first separation disc 51 and the second separation disc 52, the distribution angles of the first stirring block 61 and the second stirring block 62 are different, and the first stirring block 61 and the second stirring block 62 are distributed in a ring shape; through the first stirring block 61 and the second stirring block 62 with different distribution angles, when the stirring rod 21 drives the first separation disc 51 and the second separation disc 52 to rotate in the kettle body 1, the first stirring block 61 and the second stirring block 62 which move along with the stirring rod 21 can mix reactants in the kettle body 1;
in this embodiment, the auxiliary mixing assembly 6 further includes a heating rod 63, the heating rod 63 is disposed inside the first stirring block 61 and the second stirring block 62, and the heating rods 63 are disposed in a plurality of the stirring blocks; through the heating rod 63, when the first stirring block 61 and the second stirring block 62 are stirred with the reaction kettle, the temperature of the first stirring block 61 and the second stirring block 62 can be increased, so that the first stirring block 61 and the second stirring block 62 can uniformly heat reactants in the kettle body 1;
when the inside reactant of this reation kettle stirs the reaction, first stirring piece 61 and second stirring piece 62 can follow puddler 21 at the internal rotation of cauldron after heating rod 63 heats, heats the intensification to the reactant when stirring, and then makes the heating of the inside reactant of this reation kettle more even to the reaction effect and the reaction efficiency of the inside reactant of this reation kettle improve.
The working principle and the using flow of the utility model are as follows:
when in use:
firstly, reactants to be subjected to chemical reaction are put into a kettle body 1 through a feed pipe 11, then a motor 2 drives a stirring rod 21, a first separation disc 51 and a second separation disc 52 to rotate, and at the moment, the first separation disc 51 and the second separation disc 52 can drive a first stirring block 61 and a second stirring block 62 to mix and stir the reactants, so that the reactants react rapidly;
then the heating rods 63 in the first stirring block 61 and the second stirring block 62 heat the first stirring block 61 and the second stirring block 62, and the continuously rotating first stirring block 61 and the continuously rotating second stirring block 62 can uniformly heat the contacted reactant, so that the stirring and heating of the reactant by the reaction kettle can be more uniform and rapid;
in the reaction process;
the reactant continuously reacts in the reaction kettle, at this time, the evaporator 4 can be started to evaporate the material in the kettle body 1, then the volatile matters in the reactant can flow upwards along the distribution paths of the first separation disc 51 and the second separation disc 52 in a gas state, so that the contact area of the gas and the reactant can be increased, the content of the volatile matters in the gas is increased, and then the volatile matters can enter the condenser 3 through the air inlet pipe 33 to be cooled and discharged or flow back to the kettle body 1, and rectification processing is realized.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising one … …" does not exclude the presence of other like elements in a process, method, article, or apparatus that comprises the element.
The above embodiments are only for illustrating the technical solution of the present utility model, and are not limiting; although the utility model has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical scheme described in the foregoing embodiments can be modified or some technical features thereof can be replaced by equivalents; such modifications and substitutions do not depart from the spirit and scope of the technical solutions of the embodiments of the present utility model.
Claims (7)
1. Reaction kettle with rectification structure, its characterized in that: the novel circulating distillation kettle comprises a kettle body (1), wherein an evaporator (4) is arranged at the bottom end inside the kettle body (1), a motor (2) is arranged at the top end inside the kettle body (1), a condenser (3) is arranged on one side of the motor (2), a stirring rod (21) is arranged at the bottom of the motor (2), an auxiliary contact assembly (5) is arranged outside the stirring rod (21), an auxiliary mixing assembly (6) is arranged inside the auxiliary contact assembly (5), and the evaporator (4) and the condenser (3) jointly form a distillation structure for circulating distillation;
the auxiliary contact assembly (5) comprises a first separation disc (51), a second separation disc (52) and a connecting block (53), a communication port (511) is formed in the middle of the first separation disc (51), a plurality of connecting blocks (53) are arranged on the inner side of the communication port (511), the inner end of each connecting block (53) is connected with the outer side of the stirring rod (21), and the second separation disc (52) is arranged on the outer side of the stirring rod (21).
2. The reaction kettle with a rectification structure as claimed in claim 1, wherein: the first separation discs (51) and the second separation discs (52) are arranged in a plurality, and the first separation discs (51) and the second separation discs (52) are distributed and arranged at equal intervals in sequence.
3. The reaction kettle with a rectification structure as claimed in claim 2, wherein: the outer side of the second separation disc (52) is spaced from the inner wall of the kettle body (1), and the outer side of the first separation disc (51) is in contact fit with the inner side of the kettle body (1).
4. The reaction kettle with a rectification structure as claimed in claim 1, wherein: the novel kettle is characterized in that a feeding pipe (11) is arranged on one side of the top end of the kettle body (1), a liquid discharge pipe (31) is arranged on the other side of the top end of the kettle body (1), the liquid discharge pipe (31) is arranged on the side face of the condenser (3), an L-shaped return pipe (32) is arranged at the bottom of the liquid discharge pipe (31), the return pipe (32) is communicated with the inside of the kettle body (1), an air inlet pipe (33) is arranged at the bottom of the condenser (3), and a liquid discharge pipe (12) is arranged on one side of the bottom end of the kettle body (1).
5. The reaction kettle with a rectification structure as claimed in claim 4, wherein: the stirring rod (21) is rotationally connected with the first separation disc (51) and the second separation disc (52) and the kettle body (1), and the auxiliary mixing assembly (6) is positioned at the interval between the first separation disc (51) and the second separation disc (52).
6. The reaction kettle with a rectification structure as claimed in claim 5, wherein: the auxiliary mixing assembly (6) is internally provided with a plurality of groups at the first separation disc (51) and the second separation disc (52), the auxiliary mixing assembly (6) comprises a first stirring block (61) and a second stirring block (62), the first stirring block (61) and the second stirring block (62) are correspondingly arranged, the first stirring block (61) and the second stirring block (62) are contacted with the top surface or the bottom surface of the first separation disc (51) and the top surface or the bottom surface of the second separation disc (52), the distribution angles of the first stirring block (61) and the second stirring block (62) are different, and the first stirring block (61) and the second stirring block (62) are annularly distributed.
7. The reaction kettle with a rectification structure as claimed in claim 6, wherein: the auxiliary mixing assembly (6) further comprises heating rods (63), the heating rods (63) are arranged inside the first stirring block (61) and the second stirring block (62), and the heating rods (63) are arranged in a plurality of parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320168637.6U CN219356220U (en) | 2023-02-09 | 2023-02-09 | Reaction kettle with rectification structure |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320168637.6U CN219356220U (en) | 2023-02-09 | 2023-02-09 | Reaction kettle with rectification structure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219356220U true CN219356220U (en) | 2023-07-18 |
Family
ID=87138376
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320168637.6U Active CN219356220U (en) | 2023-02-09 | 2023-02-09 | Reaction kettle with rectification structure |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219356220U (en) |
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2023
- 2023-02-09 CN CN202320168637.6U patent/CN219356220U/en active Active
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