CN219231460U - Crude butylphenol rectifying device - Google Patents
Crude butylphenol rectifying device Download PDFInfo
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- CN219231460U CN219231460U CN202320893082.1U CN202320893082U CN219231460U CN 219231460 U CN219231460 U CN 219231460U CN 202320893082 U CN202320893082 U CN 202320893082U CN 219231460 U CN219231460 U CN 219231460U
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Abstract
The utility model provides a crude butylphenol rectifying device, which relates to the technical field of crude butylphenol and comprises a reaction kettle body and a purifying box, wherein a water storage tank is fixedly connected to the upper surface of the purifying box, a water pump is arranged at the inner bottom of the water storage tank, a water suction pipe is fixedly connected to the output end of the water pump, and one end of the water suction pipe, which is far away from the water pump, penetrates through the upper surface of the purifying box and extends to the other side. According to the utility model, after the gas enters the purifying box, the water pump is started, the water pump and the water suction pipe are matched for use, the water in the water storage box is pumped into the purifying box, then the water is uniformly sprayed through the spray head, the harmful gas in the gas is adsorbed through the water, then the sprayed water flows into the water storage tank, the collection is convenient, the gas is secondarily adsorbed and purified through the activated carbon filter plate, and then the gas is discharged through the exhaust pipe, so that the purifying effect on the gas is good, and the environment and the human health are protected, and the practicability is high.
Description
Technical Field
The utility model relates to the technical field of crude butylphenol, in particular to a crude butylphenol rectifying device.
Background
The rectification of crude butylphenol is a chemical separation technology, which is used for separating crude butylphenol from a mixture, adding the mixture into a heater, heating to a certain temperature, then sending the mixture into a reaction kettle, adding a catalyst for catalytic reaction, allowing the reacted product to enter a separation tower, separating the crude butylphenol product by distillation at different temperatures, cooling and condensing the crude butylphenol product by a condenser, and collecting the crude butylphenol product in a collector to finish rectification.
In the prior art, a large amount of waste gas generated in the rectification process of crude butylphenol generally contains volatile organic compounds, hydrogen sulfide and other harmful gases, and if the waste gas is not treated and is directly discharged into the atmosphere, the environment and the human health can be influenced, so the crude butylphenol rectification device is provided.
Disclosure of Invention
The utility model aims to solve the problem that the prior art has a large amount of waste gas generated in the rectification process of crude butylphenol, which generally contains volatile organic compounds, hydrogen sulfide and other harmful gases, and the waste gas is directly discharged into the atmosphere without being treated, so that the environment and the human health are influenced.
In order to achieve the above purpose, the present utility model adopts the following technical scheme: the utility model provides a crude butyl phenol rectifier unit, includes reation kettle body and purifying box, the last fixedly connected with water storage tank of purifying box, the interior bottom of water storage tank is provided with the water pump, the output fixedly connected with drinking-water pipe of water pump, the one end that the water pump was kept away from to the drinking-water pipe runs through the upper surface of purifying box and extends to the opposite side, the one end fixedly connected with shower nozzle that the water pump was kept away from to the drinking-water pipe, the ponding groove has been seted up to the interior bottom of purifying box, be provided with the active carbon filter plate between the inner wall of purifying box, the right surface intercommunication of purifying box is provided with the blast pipe.
Preferably, the upper surface of the reaction kettle body is fixedly connected with an air outlet pipe, and the outer surface of the air outlet pipe is provided with a valve.
Preferably, the outer surface of outlet duct is provided with the air pump in the position of keeping away from the valve, the one end fixedly connected with circulation water tank that the outlet duct kept away from the reation kettle body extends to the inboard.
Preferably, the inner surface of the circulating water tank is provided with a heat exchange tube, the end face of the air outlet tube is fixedly connected with the upper end face of the heat exchange tube, and the other end of the heat exchange tube penetrates through the inner surface of the circulating water tank and extends to the outer side.
Preferably, the upper surface of the circulating water tank is fixedly connected with a water adding pipe, and the front surface of the circulating water tank is fixedly connected with a water outlet pipe.
Preferably, the end face of the heat exchange tube is fixedly connected with the outer surface of the purifying box.
Compared with the prior art, the utility model has the advantages and positive effects that,
1. according to the utility model, after the gas enters the purifying box, the water pump is started, the water pump and the water suction pipe are matched for use, the water in the water storage box is pumped into the purifying box, then the water is uniformly sprayed through the spray head, the harmful gas in the gas is adsorbed through the water, then the sprayed water flows into the water storage tank, the collection is convenient, the gas is secondarily adsorbed and purified through the activated carbon filter plate, and then the gas is discharged through the exhaust pipe, so that the purifying effect on the gas is good, and the environment and the human health are protected, and the practicability is high.
2. According to the utility model, after sufficient water is added into the circulating water tank through the water adding pipe, gas in the reaction kettle body enters the heat exchange pipe through the gas outlet pipe, the heat exchange reaction is carried out through the heat exchange pipe and the water in the circulating water tank, the water in the circulating water tank is heated, finally the gas losing heat is discharged into the purifying box for purification, and the hot water in the circulating water tank can be discharged through the water outlet pipe, so that the waste heat of the reaction kettle body is fully utilized, the energy utilization efficiency is improved, and the energy consumption is reduced.
Drawings
FIG. 1 is a perspective view of a crude butylphenol rectification apparatus according to the present utility model;
FIG. 2 is a perspective view of a crude butylphenol rectification apparatus according to the present utility model;
fig. 3 is a perspective view of a crude butylphenol rectification device according to the present utility model.
Legend description: 1. a reaction kettle body; 2. an air outlet pipe; 3. an air pump; 4. a valve; 5. a circulation water tank; 6. a water supply pipe; 7. a water pumping pipe; 8. a water storage tank; 9. a water outlet pipe; 10. a purifying box; 11. a heat exchange tube; 12. an exhaust pipe; 13. a water pump; 14. a spray head; 15. an activated carbon filter plate; 16. a water accumulation tank.
Detailed Description
In order that the above objects, features and advantages of the utility model will be more clearly understood, a further description of the utility model will be rendered by reference to the appended drawings and examples. It should be noted that, in the case of no conflict, the embodiments of the present application and the features in the embodiments may be combined with each other.
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present utility model, however, the present utility model may be practiced otherwise than as described herein, and therefore the present utility model is not limited to the specific embodiments of the disclosure that follow.
1-3, the utility model provides a crude butylphenol rectifying device, which comprises a reaction kettle body 1 and a purifying box 10, wherein a water storage box 8 is fixedly connected to the upper surface of the purifying box 10, a water pump 13 is arranged at the inner bottom of the water storage box 8, a water suction pipe 7 is fixedly connected to the output end of the water pump 13, one end, far away from the water pump 13, of the water suction pipe 7 penetrates through the upper surface of the purifying box 10 and extends to the other side, a spray head 14 is fixedly connected to one end, far away from the water pump 13, of the water suction pipe 7, a water storage tank 16 is arranged at the inner bottom of the purifying box 10, an activated carbon filter plate 15 is arranged between the inner walls of the purifying box 10, an exhaust pipe 12 is arranged on the right surface of the purifying box 10 in a communicating manner, an air outlet pipe 2 is fixedly connected to the upper surface of the reaction kettle body 1, a valve 4 is arranged on the outer surface of the air outlet pipe 2, and the end surface of the heat exchange pipe 11 is fixedly connected with the outer surface of the purifying box 10.
The effect that its whole embodiment 1 reached is, after reflection cauldron body 1 reflection work was over, open valve 4, make the inside gas of reflection cauldron body 1 discharge through outlet duct 2, through opening air pump 3, can accelerate the inside gas discharge rate of reflection cauldron body 1, then utilize the heat of gas through circulation tank 5, then the gas is discharged into purifying box 10, fill water in water storage tank 8, then start water pump 13, thereby use through water pump 13 and drinking-water pipe 7 cooperation, take the water in the water storage tank 8 to purifying box 10, then evenly spray water through shower nozzle 14, adsorb harmful gas in the gas through water, then the water that sprays can flow to the ponding groove 16, be convenient for collect, then the gas carries out secondary adsorption through active carbon filter plate 15 and purifies, afterwards discharge through blast pipe 12, purifying effect to the gas is good, thereby environmental protection and human health, the practicality is high.
The effect that its whole embodiment 2 reached is, after adding sufficient water in with circulation tank 5 through water pipe 6, the gas in the reation kettle body 1 gets into heat exchange tube 11 through outlet duct 2, carries out heat exchange reaction through the water in heat exchange tube 11 and the circulation tank 5, heats the water in the circulation tank 5, and the gas that loses the heat finally is discharged into purifying box 10 and is purified, can discharge the hot water in the circulation tank 5 through outlet pipe 9, has fully utilized the waste heat of reation kettle body 1, has improved the utilization efficiency of the energy, reduces the energy consumption.
Working principle: after the reaction of the reaction kettle body 1 is finished, after enough water is added into the circulating water tank 5 through the water adding pipe 6, then the valve 4 is opened, gas in the reaction kettle body 1 is discharged through the gas outlet pipe 2, the gas discharging speed in the reaction kettle body 1 can be accelerated by opening the gas pump 3, after the gas enters the heat exchange pipe 11, the heat exchange reaction is carried out through the heat exchange pipe 11 and the water in the circulating water tank 5, the water in the circulating water tank 5 is heated, then the gas losing heat is discharged into the purifying box 10, the water storage tank 8 is filled with water, then the water pump 13 is started, so that the water in the water storage tank 8 is pumped into the purifying box 10 through the water pump 13 and the water pumping pipe 7, then the water is uniformly sprayed, harmful gas in the gas is adsorbed through the water, then the sprayed water flows into the water accumulating tank 16, the gas is convenient to collect, then the gas is subjected to secondary adsorption and purification through the activated carbon 15, and then the gas is discharged through the gas exhaust pipe 12, the purifying effect on the gas is good, and the environment and the human health is protected, and the practicability is high.
The wiring diagrams of the air pump 3 and the water pump 13 in the present utility model are common knowledge in the art, the working principle thereof is a known technology, and the model thereof is selected to be a proper model according to actual use, so the control mode and wiring arrangement of the air pump 3 and the water pump 13 are not explained in detail.
The present utility model is not limited to the above-mentioned embodiments, and any equivalent embodiments which can be changed or modified by the technical content disclosed above can be applied to other fields, but any simple modification, equivalent changes and modification made to the above-mentioned embodiments according to the technical substance of the present utility model will still fall within the protection scope of the technical solution of the present utility model.
Claims (6)
1. The utility model provides a crude butylphenol rectifying device, includes reation kettle body (1) and purifying box (10), its characterized in that: the utility model discloses a purifying box, including purifying box (10), water storage tank (8) is connected with to the upper surface of purifying box (10), the interior bottom of water storage tank (8) is provided with water pump (13), the output fixedly connected with drinking-water pipe (7) of water pump (13), the one end that drinking-water pipe (7) were kept away from water pump (13) runs through the upper surface of purifying box (10) and extends to the opposite side, the one end fixedly connected with shower nozzle (14) that water pump (13) was kept away from to drinking-water pipe (7), water storage tank (16) have been seted up to the interior bottom of purifying box (10), be provided with active carbon filter plate (15) between the inner wall of purifying box (10), the right surface intercommunication of purifying box (10) is provided with blast pipe (12).
2. The crude butylphenol rectification apparatus of claim 1, wherein: the upper surface fixedly connected with outlet duct (2) of reation kettle body (1), the surface of outlet duct (2) is provided with valve (4).
3. The crude butylphenol rectification apparatus of claim 2, wherein: the outer surface of outlet duct (2) is kept away from the position of valve (4) and is provided with air pump (3), the one end fixedly connected with circulation water tank (5) that reaction kettle body (1) was kept away from to outlet duct (2) extends to the inboard.
4. A crude butylphenol rectification apparatus as claimed in claim 3, wherein: the inner surface of the circulating water tank (5) is provided with a heat exchange tube (11), the end face of the air outlet tube (2) is fixedly connected with the upper end face of the heat exchange tube (11), and the other end of the heat exchange tube (11) penetrates through the inner surface of the circulating water tank (5) and extends to the outer side.
5. A crude butylphenol rectification apparatus as claimed in claim 3, wherein: the upper surface of the circulating water tank (5) is fixedly connected with a water adding pipe (6), and the front surface of the circulating water tank (5) is fixedly connected with a water outlet pipe (9).
6. The crude butylphenol rectification apparatus of claim 4, wherein: the end face of the heat exchange tube (11) is fixedly connected with the outer surface of the purifying box (10).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320893082.1U CN219231460U (en) | 2023-04-20 | 2023-04-20 | Crude butylphenol rectifying device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320893082.1U CN219231460U (en) | 2023-04-20 | 2023-04-20 | Crude butylphenol rectifying device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219231460U true CN219231460U (en) | 2023-06-23 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320893082.1U Active CN219231460U (en) | 2023-04-20 | 2023-04-20 | Crude butylphenol rectifying device |
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| Country | Link |
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| CN (1) | CN219231460U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118491131A (en) * | 2024-07-16 | 2024-08-16 | 烟台丰鲁精细化工有限责任公司 | Benzene liquid separation and collection device |
-
2023
- 2023-04-20 CN CN202320893082.1U patent/CN219231460U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118491131A (en) * | 2024-07-16 | 2024-08-16 | 烟台丰鲁精细化工有限责任公司 | Benzene liquid separation and collection device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A crude butylphenol distillation device Effective date of registration: 20230727 Granted publication date: 20230623 Pledgee: Shandong Linzi Rural Commercial Bank Co.,Ltd. Pledgor: ZIBO XUJIA CHEMICAL Co.,Ltd. Registration number: Y2023980049856 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |